LEADER 04717nam 2200625 450 001 9910830943003321 005 20230421044621.0 010 $a1-282-01031-X 010 $a9786612010316 010 $a3-527-61235-1 010 $a3-527-61232-7 035 $a(CKB)1000000000376844 035 $a(EBL)481828 035 $a(OCoLC)310370261 035 $a(SSID)ssj0000211485 035 $a(PQKBManifestationID)11198391 035 $a(PQKBTitleCode)TC0000211485 035 $a(PQKBWorkID)10311340 035 $a(PQKB)10020119 035 $a(MiAaPQ)EBC481828 035 $a(EXLCZ)991000000000376844 100 $a20160816h19981998 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 10$aNMR spectroscopy $emodern spectral analysis /$fUrsula Weber, Herbert Thiele 210 1$aWeinheim, [Germany] :$cWiley-VCH,$d1998. 210 4$dİ1998 215 $a1 online resource (411 p.) 225 1 $aSpectroscopic Techniques: An Interactive Course 300 $aDescription based upon print version of record. 311 $a3-527-28828-7 320 $aIncludes bibliographical references at the end of each chapters and index. 327 $aNMR Spectroscopy: Modern Spectral Analysis; Table of Contents; 1 Introduction; 1.1 Scope and Audience; 1.2 Organisation; 1.3 Personal Qualifications; 1.4 Contents; 1.5 Technical Requirements; 1.6 Software; 1.6.1 General Remarks; 1.6.2 Installation; 1.6.3 Basic Program Knowledge; 1.6.4 Book Formatting; 1.7 Recommended Reading and References; 2 General Characteristics of Spin Systems; 2.1 The Chemical Shift; 2.1.1 Spin Systems Without Coupling; 2.1.2 The NMR Resonance Frequency; 2.1.2.1 The NMR Transition Frequency; 2.1.2.2 The NMR Transition Intensity; 2.1.2.3 The NMR Lineshape 327 $a2.1.3 Two Non-Coupled Spins2.1.3.1 Two Isochronous Spins; 2.1.3.2 Two Non-Isochronous Spins Without Coupling; 2.1.4 Basic Notation of Spin Systems; 2.1.5 Summary and Examples; 2.2 First Order Spin Systems; 2.2.1 Introduction to Spin-Spin Coupling; 2.2.2 The AX Spin System; 2.2.2.1 Heteronuclear AX Spin Systems; 2.2.2.2 Homonuclear AX Spin Systems; 2.2.2.3 Summary; 2.2.3 The AMX Spin System; 2.2.4 Extended First Order Spin Systems; 2.2.4.1 AMRX Spin Svstems; 2.2.4.2 Fragmentation of Spin Systems; 2.3 Second Order Spin Systems; 2.3.1 Notational Aspects; 2.3.2 The AB Spin System 327 $a2.3.2.1 The Graphical Spectrum Analysis2.3.2.2 Suppression of Particular Transitions; 2.3.3 The ABX Spin System; 2.3.3.1 Analytical Solution for the ABX Spin System; 2.3.3.2 First Order Based ABX Solution; 2.3.4 Extended Spin Systems; 2.3.4.1 Taking Advantage of Field Effects; 2.4 Magnetic Equivalence; 2.4.1 Notational Aspects; 2.4.2 The Coupled A2 Spin System; 2.4.3 The Composite Particle Approach; 2.4.4 The A n Spin Systems; 2.4.5 First Order Spin Systems; 2.4.5.1 The A2X Spin System; 2.4.5.2 The AX3 Spin System; 2.4.5.3 AnXm Spin Systems 327 $a2.4.5.4 First Order Spin Systems with more than one Coupling2.4.6 Second Order Spin Systems; 2.4.6.1 The A2B Spin System; 2.5 References; 3 Structure and Spin System Parameters; 3.1 Symmetry Effects; 3.1.1 Structural and Notational Aspects; 3.1.2 The [AX1]2 Spin System; 3.1.3 The [AB]2 spin system; 3.2 Configuration Isomers in NMR; 3.2.1 Cis/trans Isomerism; 3.2.1.1 Determination of the Signs of Coupling Constants; 3.2.1.2 Extended Spin Systems; 3.2.2 Enantiomers and Diastereomers; 3.3 Conformation and NMR; 3.3.1 Taking Advantage of Field and Solvent Effects; 3.3.1.1 Linewidths 327 $a4.2.3 Spin Systems Containing 29Si 330 $aThe state-of-the-art in NMR spectral analysis.This interactive tutorial provides readers with a comprehensive range of software tools and techniques, as well as the necessary theoretical knowledge required to analyze their spectra and obtain the correct NMR parameters.Modern Spectral Analysis provides expert guidance, by presenting efficient strategies to extract NMR parameters from measured spectra. A database of selected spectra and modern, powerful WIN-NMR software designed by Bruker are provided on the enclosed CD-ROM. The programs provided are 1 D WIN-NMR, WIN-DAISY, WIN-DR and WI 410 0$aSpectroscopic techniques. 606 $aNuclear magnetic resonance spectroscopy$xData processing 615 0$aNuclear magnetic resonance spectroscopy$xData processing. 676 $a543.0877 676 $a547.128 700 $aWeber$b Ursula$0447554 702 $aThiele$b Herbert 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910830943003321 996 $aNMR spectroscopy$94098949 997 $aUNINA