LEADER 05144nam 2200661Ia 450 001 9910830459403321 005 20240117174605.0 010 $a9786610271931 010 $a0-470-86800-7 010 $a0-470-32235-7 010 $a1-280-27193-0 010 $a0-470-86455-9 035 $a(CKB)1000000000411846 035 $a(EBL)158153 035 $a(OCoLC)52761947 035 $a(SSID)ssj0000102927 035 $a(PQKBManifestationID)11122488 035 $a(PQKBTitleCode)TC0000102927 035 $a(PQKBWorkID)10062121 035 $a(PQKB)11605141 035 $a(MiAaPQ)EBC158153 035 $a(EXLCZ)991000000000411846 100 $a20021118d2003 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 14$aThe analysis of controlled substances$b[electronic resource] /$fMichael D. Cole 210 $aNew York $cWiley$dc2003 215 $a1 online resource (222 p.) 225 1 $aAnalytical techniques in the sciences 300 $aDescription based upon print version of record. 311 $a0-471-49252-3 311 $a0-471-49253-1 320 $aIncludes bibliographical references and index. 327 $aTHE ANALYSIS OF CONTROLLED SUBSTANCES; Contents; Series Preface; Preface; Acronyms, Abbreviations and Symbols; About the Author; 1 Introduction to Drug Trends, Control, Legislation and Analysis; 1.1 Introductory Remarks; 1.2 International Legislation; 1.3 Controlled Substances in the United Kingdom; 1.3.1 Background to the Misuse of Drugs Act, 1971; 1.3.2 The Provisions of the Misuse of Drugs Act, 1971; 1.4 Controlled Substances in the United States; 1.5 Controlled Substances in Australia; 1.6 The Drug Chemist and Drug Analysis; 1.7 Quality Assurance in the Drugs Laboratory 327 $a1.8 Presentation of Evidence in CourtReferences; 2 Amphetamine and Related Compounds; 2.1 Introduction; 2.2 Qualitative Identification of Amphetamines; 2.2.1 Sampling and Physical Description of Amphetamines; 2.2.2 Presumptive Testing of Amphetamines; 2.2.3 Thin Layer Chromatography of Amphetamines; 2.2.4 Definitive Identification of Amphetamines; 2.3 Quantification of Amphetamines; 2.4 Comparison and Profiling of Amphetamine Samples; 2.4.1 The Leuckart Synthesis of Amphetamine; 2.4.2 The Reductive Amination of Benzyl Methyl Ketone; 2.4.3 The Nitrostyrene Synthesis 327 $a2.4.4 Impurity Extraction and Sample ComparisonReferences; 3 The Analysis of LSD; 3.1 Introduction; 3.2 Qualitative Identification of LSD; 3.2.1 Sampling and Physical Description of LSD Blotter Acid; 3.2.2 Extraction of LSD Prior to Analysis; 3.2.3 Presumptive Testing for LSD; 3.2.4 Thin Layer Chromatography of Samples Containing LSD; 3.2.5 Confirmatory Tests for the Presence of LSD; References; 4 Cannabis sativa and Products; 4.1 Introduction; 4.2 Origins, Sources and Manufacture of Cannabis; 4.3 Analytical Sequence, Bulk and Trace Sampling Procedures 327 $a4.4 Qualitative Identification of Cannabis4.4.1 Identification of Herbal Material; 4.4.2 Identification of Other Materials; 4.4.3 Comparison of Cannabis Samples; References; 5 Diamorphine and Heroin; 5.1 Introduction; 5.2 Origins, Sources and Manufacture of Diamorphine; 5.3 Appearance of Heroin and Associated Paraphernalia; 5.4 Bulk and Trace Sampling Procedures; 5.5 Identification, Quantification and Comparison of Heroin Samples; 5.5.1 Presumptive Tests for Heroin; 5.5.2 Thin Layer Chromatography of Heroin Samples; 5.5.3 Gas Chromatographic-Mass Spectroscopic Identification of Heroin 327 $a5.5.4 Quantification of Heroin Samples5.5.5 Comparison of Heroin Samples; References; 6 Cocaine; 6.1 Introduction; 6.2 Origins, Sources and Manufacture of Cocaine; 6.2.1 Extraction and Preparation of Coca Paste; 6.2.2 Synthesis of Pure Cocaine; 6.3 Qualitative Identification of Cocaine; 6.3.1 Presumptive Tests for Cocaine; 6.3.2 Thin Layer Chromatography; 6.3.3 Definitive Identification of Cocaine; 6.4 Quantification of Cocaine; 6.4.1 Quantification of Cocaine by GC-MS; 6.4.2 Quantification of Cocaine by UV Spectroscopy; 6.5 Comparison of Cocaine Samples; References 327 $a7 Products from Catha edulis and Lophophora williamsii 330 $aPresenting new developments in sampling and drug profiling, this book also provides practical information on how to carry out analysis, what the results mean and how they can be used as court evidence and for drugs intelligence purposes.* Includes case-studies with full data and spectra, helping readers to identify substances* Accessibly organized by class of compound* Contains an up-to-date list of the newest drugs 410 0$aAnalytical techniques in the sciences. 606 $aDrugs of abuse$xAnalysis 606 $aPharmacy 615 0$aDrugs of abuse$xAnalysis. 615 0$aPharmacy. 676 $a615.1901 676 $a615/.78 700 $aCole$b M. D$g(Michael D.)$01663492 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910830459403321 996 $aThe analysis of controlled substances$94020851 997 $aUNINA