LEADER 05016nam 2200673Ia 450 001 9910830157703321 005 20210223194357.0 010 $a1-280-54194-6 010 $a9786610541942 010 $a0-471-65367-5 010 $a0-471-65368-3 035 $a(CKB)111090529069414 035 $a(EBL)183854 035 $a(SSID)ssj0000179658 035 $a(PQKBManifestationID)11177655 035 $a(PQKBTitleCode)TC0000179658 035 $a(PQKBWorkID)10138030 035 $a(PQKB)10643124 035 $a(MiAaPQ)EBC183854 035 $a(OCoLC)85820551 035 $a(PPN)243218214 035 $a(EXLCZ)99111090529069414 100 $a20750907d2004 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 00$aInorganic syntheses$hVolume 34$b[electronic resource] /$feditor-in-chief John R. Shapley 210 $aNew York [etc.] $cWiley [etc.]$d2004 215 $a1 online resource (284 p.) 225 1 $aInorganic Syntheses ;$vv.68 300 $aDescription based upon print version of record. 311 $a0-471-64750-0 320 $aIncludes bibliographical references and index. 327 $aINORGANIC SYNTHESES Volume 34; PREFACE; NOTICE TO CONTRIBUTORS AND CHECKERS; TOXIC SUBSTANCES AND LABORATORY HAZARDS; CONTENTS; Chapter One MAIN GROUP COMPOUNDS; 1. Diborane(4) Compounds; A. Tetrakis(dimethylamino)diborane(4), B(2)(NMe(2))(4); B. 1,2-Dichloro-1,2-bis(dimethylamino)diborane(4), B(2)Cl(2)(NMe(2))(2); C. 2,2'-Bis(1,3,2-benzodioxaborole), B(2)(1,2-O(2)C(6)H(4))(2); 2. Sodium Tetrakis(3,5-bis(trifluoromethyl)phenyl)borate, Na[B(3,5-(CF(3))(2)C(6)H(3))(4)]; 3. Anionic Tris- and Bis(diphenylphosphinomethyl)borates 327 $aA. Tetrabutylammonium Phenyltris(diphenylphosphinomethyl)borate, [(n)Bu(4)N][PhB(CH(2)PPh(2))(3)]B. Tetrabutylammonium Diphenylbis(diphenylphosphinomethyl)borate, [(n)Bu(4)N][Ph(2)B(CH(2)PPh(2))(2)]; C. Thallium Phenyltris(diphenylphosphinomethyl)borate, [PhB(CH(2)PPh(2))(3)]Tl; 4. Six-Coordinate Aluminum Cations Based on Salen Ligands; A. Chloro-1,2-bis(2-hydroxybenzylideneimino)ethanealuminum, Al(Salen)Cl; B. Diaqua-1,2-bis(2-hydroxybenzylideneimino)ethanealuminum Chloride, [Al(Salen)(H(2)O)(2)]Cl 327 $aC. Dimethanol-1,2 bis-(2-hydroxy-3,5-bis(tert-butyl)benzylideneimino) Aluminum Chloride, [Al(Salen(t)Bu)(MeOH)(2)]ClD. Dimethanol-1,2-bis(2-hydroxy-3,5-bis(tert-butyl)benzylideneimino)ethanealuminum Tetraphenylborate, [Al((t)BuSalen)(MeOH)(2)][BPh(4)]; E. Dimethanol-1,2-bis(2-hydroxy-3,5-bis(tert-butyl)benzylideneimino)ethanealuminum para-Toluenesulfonate, [Al((t)BuSalen)(MeOH)(2)][OTs]; F. Bis(tetrahydrofuran)-1,2-bis(2-hydroxy-3,5-bis(tert-butyl)benzylideneimino)ethanealuminum Tetraphenylborate, [Al((t)BuSalen)(THF)(2)][BPh(4)]; 5. Tabular a-Alumina; 6. Para-Substituted Aryl Isocyanides 327 $aA. 1,4-Diisocyanobenzene, p-CNC(6)H(4)NCB. 1,4-Diisocyano-2,5-dimethylbenzene, p-CN(C(6)H(2)(CH(3))(2))NC; C. 1-Isocyano-4-methoxybenzene, p-CN(C(6)H(4))OCH(3); D. Bis(1,4-diisocyanobenzene)bis(1,2-bis(diphenylphosphino)ethane)tungsten(0), W(dppe)(2)(CNC(6)H(4)NC)(2); 7. Unsymmetric Tripod Ligands Related to Tris(pyrazol-1-yl)methane; A. Bis(pyrazol-1-yl)methanone, (pz)(2)C=O; B. N-Methylimidazole-2-carbaldehyde, (mim)CHO; C. Bis(pyrazol-1-yl)(pyridin-2-yl)methane, (pz)(2)(py)CH; D. Bis(pyrazol-1-yl)(N-methylimidazol-2-yl)methane, (pz)(2)(mim)CH; 8. Difluorotriphenylarsenic(V), AsF(2)Ph(3) 327 $a9. Tetramethylammonium Salts of Superoxide and PeroxynitriteA. Tetramethylammonium Superoxide, [N(CH(3))(4)]O(2); B. Tetramethylammonium Peroxynitrite, [N(CH(3))(4)][ONOO]; 10. Tellurium-Nitrogen Compounds; A. Lithium tert-Butylamide, Li[HN(t)Bu]; B. Bis(m-tert-butylimido)-bis(tert-butylimido)ditellurium, (t)BuNTe(m-N(t)Bu)(2)TeN(t)Bu; C. Bis{dilithium[tris(tert-butylimido)tellurite]}, {Li(2)[Te(N(t)Bu)(3)]}(2); Chapter Two ORGANOMETALLIC AND COORDINATION COMPLEXES; 11. Addition Compounds of Dibromodioxomolybdenum(VI); A. Stock Solution of MoO(2)Br(2)(H(2)O)(2) in Diethyl Ether 327 $aB. Diaquadibromodioxomolybdenum(VI) Diglyme Complex, MoO(2)Br(2)(H(2)O)(2)·diglyme 330 $aThis series provides inorganic chemists with detailed and foolproof procedures for the preparation of important and timely compounds. Volume 34 continues to report such procedures with an up-to-date selection of contributions by internationally-recognized researchers, including the following: 410 0$aInorganic Syntheses 606 $aInorganic compounds$xSynthesis 606 $aChemistry, Inorganic 615 0$aInorganic compounds$xSynthesis. 615 0$aChemistry, Inorganic. 676 $a541.39 676 $a541/.39 676 $a547.2 701 $aShapley$b John R$01698207 712 02$aAmerican Chemical Society. 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910830157703321 996 $aInorganic syntheses$94079508 997 $aUNINA