LEADER 04997nam 2200445 450 001 9910830002703321 005 20230511083852.0 010 $a3-527-83111-8 010 $a3-527-83110-X 035 $a(MiAaPQ)EBC7192099 035 $a(Au-PeEL)EBL7192099 035 $a(CKB)26094843200041 035 $a(EXLCZ)9926094843200041 100 $a20230511d2023 uy 0 101 0 $aeng 135 $aurcnu|||||||| 181 $ctxt$2rdacontent 182 $cc$2rdamedia 183 $acr$2rdacarrier 200 10$aCalibration in analytical science $emethods and procedures /$fPawe? Kos?cielniak 210 1$aWeinheim, Germany :$cWiley-VCH,$d[2023] 210 4$dİ2023 215 $a1 online resource (387 pages) 311 08$aPrint version: Ko?cielniak, Pawe? Calibration in Analytical Science Newark : John Wiley & Sons, Incorporated,c2023 9783527348466 320 $aIncludes bibliographical references and index. 327 $aCover -- Title Page -- Copyright -- Contents -- Preface -- Chapter 1 Calibration Fundamentals -- 1.1 Analytical Context -- 1.2 Principles of Analytical Calibration -- 1.3 Calibration Standards and Models -- 1.4 Calibration Procedures and Methods -- 1.5 Calibration in the Context of Measurement Errors -- 1.5.1 Uncontrolled Analytical Effects -- 1.5.2 Elimination and Compensation of Uncontrolled Effects -- 1.6 Calibration in Qualitative Analysis -- 1.7 Calibration in Quantitative Analysis -- 1.8 General Rules for Correct Calibration -- References -- Chapter 2 "Calibration?Free" Analysis -- 2.1 Novel Approach -- 2.2 Empirical Calibration -- 2.3 Theoretical Calibration -- 2.3.1 Fixed Models -- 2.3.2 Flexible Models -- References -- Chapter 3 Calibration Methods in Qualitative Analysis -- 3.1 Classification -- 3.2 External Calibration Methods -- 3.2.1 External Standard Method -- 3.2.2 Reference Sample Method -- 3.3 Internal Calibration Methods -- 3.3.1 Internal Standard Method -- 3.3.2 Indirect Method -- 3.4 Standard Addition Method -- References -- Chapter 4 Introduction to Empirical Calibration in Quantitative Analysis -- 4.1 Classification -- 4.2 Formulation of Model Functions -- 4.3 Examination of Interference Effect -- 4.4 Mathematical Modeling of Real Function -- References -- Chapter 5 Comparative Calibration Methods -- 5.1 External Calibration Methods -- 5.1.1 External Standard Method -- 5.1.1.1 Modified Procedures -- 5.1.2 Dilution Method -- 5.2 Internal Calibration Methods -- 5.2.1 Internal Standard Method -- 5.2.2 Indirect Method -- References -- Chapter 6 Additive Calibration Methods -- 6.1 Basic Aspects -- 6.2 Standard Addition Method -- 6.2.1 Extrapolative Variant -- 6.2.1.1 Modified Procedures -- 6.2.2 Interpolative Variants -- 6.2.3 Indicative Variant -- 6.3 Titration -- 6.4 Isotope Dilution Method -- 6.4.1 Radiometric Isotope Dilution. 327 $a6.4.2 Isotope Dilution Mass Spectrometry -- 6.4.2.1 Modified Procedures -- References -- Chapter 7 Calibration in Nonequilibrium Conditions -- 7.1 Flow Injection Analysis -- 7.1.1 Manipulation Techniques -- 7.1.2 Gradient Technique -- 7.2 Kinetic Analysis -- References -- Chapter 8 Complex Calibration Approaches -- 8.1 Extrapolative Methods -- 8.1.1 Extrapolative Indirect Method -- 8.1.2 Extrapolative Internal Standard Method -- 8.1.3 Extrapolative Dilution Method -- 8.2 Mixed Methods -- 8.3 Combined Methods -- 8.3.1 Integrated Calibration Methods -- 8.3.1.1 Simple Integrated Method -- 8.3.1.2 Complementary Dilution Method -- 8.3.2 Generalized Calibration Strategy -- 8.3.2.1 Versatile Flow Injection Calibration Module -- 8.3.3 Standard Dilution Analysis -- References -- Chapter 9 Calibration Approaches for Detection and Examination of Interference Effects -- 9.1 Introduction -- 9.2 Simple Procedures for Detection and Examination of Interference Effects -- 9.3 Detection and Compensation of Additive Interference Effect -- 9.3.1 Interpolative Procedure -- 9.3.2 Extrapolative Procedure -- 9.3.3 Integrated Procedure -- References -- Chapter 10 Calibration?Based Procedures for Correction of Preparative Effects -- 10.1 Introduction -- 10.2 Specific Procedures -- 10.3 Surrogate Recovery Method -- 10.3.1 Reliability of the Method -- 10.3.2 Interpretations of the Method -- 10.3.3 Recovery vs. Interference Effect -- 10.3.4 Recovery vs. Speciation Effect -- References -- Chapter 11 Calibration?Related Applications of Experimental Plans -- 11.1 Introduction -- 11.2 Examination of Interference Effects -- 11.3 Modeling of Real Functions -- 11.4 Multicomponent Analysis -- References -- Chapter 12 Final Remarks -- References -- Index -- EULA. 606 $aAnalytical chemistry 606 $aCalibration 615 0$aAnalytical chemistry. 615 0$aCalibration. 676 $a543 700 $aKos?cielniak$b Pawe?$01612212 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910830002703321 996 $aCalibration in analytical science$93940886 997 $aUNINA