LEADER 04388nam 2200661Ia 450 001 9910827538403321 005 20240416070025.0 010 $a1-281-01886-4 010 $a9786611018863 010 $a0-08-053232-2 035 $a(CKB)1000000000384413 035 $a(EBL)307127 035 $a(OCoLC)173649318 035 $a(SSID)ssj0000160780 035 $a(PQKBManifestationID)11159518 035 $a(PQKBTitleCode)TC0000160780 035 $a(PQKBWorkID)10190623 035 $a(PQKB)10479387 035 $a(MiAaPQ)EBC307127 035 $a(Au-PeEL)EBL307127 035 $a(CaPaEBR)ebr10186699 035 $a(CaONFJC)MIL101886 035 $a(PPN)182567419 035 $a(EXLCZ)991000000000384413 100 $a19951122d1996 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt$2rdacontent 182 $cc$2rdamedia 183 $acr$2rdacarrier 200 10$aGas chromatography and mass spectrometry $ea practical guide /$fFulton G. Kitson, Barbara S. Larsen, Charles N. McEwen 205 $a1st ed. 210 $aSan Diego $cAcademic Press$dc1996 215 $a1 online resource (xii, 381 pages) $cillustrations 300 $aDescription based upon print version of record. 311 $a0-12-483385-3 320 $aIncludes bibliographical references and index. 327 $aPart I: The Fundamentals of GC/MS; Chapter 1. What Is GC/MS?; Chapter 2. Interpretation of Mass Spectra; Chapter 3. Quantitative GC/MS; Part II: GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types; Chapter 4. Acids; Chapter 5. Alcohols; Chapter 6. Aldehydes; Chapter 7. Amides; Chapter 8. Amines; Chapter 9. Amino Acids; Chapter 10. Common Contaminants; Chapter 11. Drugs and Their Metabolites; Chapter 12. Esters; Chapter 13. Ethers 327 $aChapter 14. Fluorinated CompoundsChapter 15. Gases; Chapter 16. Glycols; Chapter 17. Halogenated Compounds (Other Than Fluorinated); Chapter 18. Hydrocarbons; Chapter 19. Isocyanates; Chapter 20. Ketones; Chapter 21. Nitriles; Chapter 22. Nitroaromatics; Chapter 23. Nitrogen-Containing Heterocyclics; Chapter 24. Nucleosides (TMS Derivatives); Chapter 25. Pesticides; Chapter 26. Phenols; Chapter 27. Phosphorus Compounds; Chapter 28. Plasticizers and Other Polymer Additives (Including Phthalates); Chapter 29. Prostaglandins (MO-TMS Derivatives); Chapter 30. Solvents and Their Impurities 327 $aChapter 31. SteroidsChapter 32. Sugars (Monosaccharides); Chapter 33. Sulfur Compounds; Part III: Ions for Determining Unknown Structures; Part IV: Appendices; Appendix 1. Definitions of Terms Related to Gas Chromatography; Appendix 2. Tips for Gas Chromatography; Appendix 3. Derivatives Found Useful in GC/MS; Appendix 4. Cross-Index Chart for GC Phases; Appendix 5. McReynolds' Constants; Appendix 6. Simple GC Troubleshooting; Appendix 7. Definitions of Terms Related to Mass Spectrometry; Appendix 8. Tips and Troubleshooting for Mass Spectrometers 327 $aAppendix 9. Atomic Masses and Isotope AbundancesAppendix 10. Structurally Significant McLafferty Rearrangement Ions; Appendix 11. Isotope Patterns for Chlorine and Bromine; Appendix 12. Mixtures for Determining Mass Spectral Resolution; Index 330 $aThis guide provides, under one cover, a wealth of practical information designed to facilitate the effectiveness of the GC/MS user. Separation conditions for numerous compound types are provided along with derivatized and underivatized compounds. A section on how to interpret mass spectral data, an extensive correlation of ion masses and neutral losses with possible structures, and examples of mass spectra are provided to further aid structure determination. Also included are basic information on instrumentation, ionization methods, quantitation, and tips on the operation of mass spectrometers. 606 $aGas chromatography 606 $aMass spectrometry 615 0$aGas chromatography. 615 0$aMass spectrometry. 676 $a543/.0873 676 $a543.0873 700 $aKitson$b Fulton G$067140 701 $aLarsen$b Barbara Seliger$067141 701 $aMcEwen$b Charles N.$f1942-$091299 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910827538403321 996 $aGas Chromatography and Mass Spectrometry$9377156 997 $aUNINA