LEADER 04388nam 2200661 a 450 001 9910827470903321 005 20220712133127.0 010 $a1-283-17107-4 010 $a9786613171078 010 $a0-08-092015-2 035 $a(CKB)2670000000074980 035 $a(EBL)670206 035 $a(OCoLC)727648625 035 $a(SSID)ssj0000492006 035 $a(PQKBManifestationID)12174850 035 $a(PQKBTitleCode)TC0000492006 035 $a(PQKBWorkID)10478798 035 $a(PQKB)11109751 035 $a(Au-PeEL)EBL670206 035 $a(CaPaEBR)ebr10483481 035 $a(CaONFJC)MIL317107 035 $z(PPN)182574601 035 $a(PPN)170599825 035 $a(FR-PaCSA)88812116 035 $a(MiAaPQ)EBC670206 035 $a(EXLCZ)992670000000074980 100 $a20100715d2011 uy 0 101 0 $aeng 135 $aurcn||||||||| 181 $ctxt 182 $cc 183 $acr 200 10$aGas chromatography and mass spectrometry $ea practical guide /$fO. David Sparkman, Zelda E. Penton, Fulton G. Kitson 205 $a2nd ed. 210 $aBoston $cElsevier$d2011 215 $a1 online resource (633 p.) 300 $aDescription based upon print version of record. 311 $a0-08-043801-6 311 $a0-12-373628-5 320 $aIncludes bibliographical references and index. 327 $aThe fundamentals of GC/MS -- Introduction and history -- Gas chromatography -- The gc/ms interface -- Mass spectrometry instrumentation -- Mass spectral data interpretation -- Quantitation with GC/MS -- GC conditions, derivatization, and mass spectral interpretation -- Of specific compound types -- Acids -- Alcohols -- Aldehydes -- Amides -- Amines -- Amino acid -- Common contaminants -- Drugs and their metabolites -- Esters -- Ethers -- Fluorinated compounds -- Gases -- Glycols -- Halogenated compounds (other than fluorinated) -- Hydrocarbons -- Isocyanates -- Ketones -- Nitriles -- Nitroaromatics -- Nitrogen-containing heterocyclics -- Nucleosides (TMS derivatives) -- Pesticides -- Phenols -- Phosphorus compounds -- Plasticizers and other polymer additives (including phthalates) -- Prostaglandins (MO-TMS derivatives) -- Solvents and their impurities -- Steroids -- Sugars (monosaccharides) -- Sulfur compounds -- Appendices -- A definitions of terms related to gas chromatography -- B definitions of terms related to mass spectrometry -- C atomic masses and isotope abundances -- X+1 and x+2 values for ions containing atoms of C and H based on -- Isotope contributions -- E isotope peak patterns for ions containing atoms of Cl and/or Br -- F steps to follow in the determination of an elemental composition -- Based on isotope peak intensity ratios -- G derivatization in GC/MS -- H points of comparison of LC/MS vs GC/MS -- I list of available EI mass spectral databases -- J information required for reporting a GC/MS analysis -- K third-party software for use with GC/MS -- GC installation and maintenance -- Troubleshooting common GC problems -- N maintenance, operating tips, and troubleshooting for mass spectrometers -- O mixtures for determining mass spectral resolution -- P cross-index chart for GC stationary phases -- Q ions for determining unknown structures. 330 $aThe second edition of Gas Chromatography and Mass Spectrometry: A Practical Guide follows the highly successful first edition by F.G. Kitson, B.S. Larsen, and C.N. McEwen (1996), which was designed as an indispensable resource for GC/MS practitioners regardless of whether they are a novice or well experienced. The Fundamentals section has been extensively reworked from the original edition to give more depth of an understanding of the techniques and science involved with GC/MS. Even with this expansion, the original brevity and simple didactic style has been retained. Information on 606 $aGas chromatography 606 $aMass spectrometry 615 0$aGas chromatography. 615 0$aMass spectrometry. 676 $a543/.85 676 $a543.85 700 $aSparkman$b O. David$g(Orrin David),$f1942-$0447425 701 $aPenton$b Zelda$01710861 701 $aKitson$b Fulton G$067140 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910827470903321 996 $aGas chromatography and mass spectrometry$94101783 997 $aUNINA