LEADER 05341nam 2200697Ia 450 001 9910826151103321 005 20240513103840.0 010 $a1-282-95543-8 010 $a9786612955433 010 $a0-444-53600-0 035 $a(CKB)2670000000051605 035 $a(EBL)630009 035 $a(OCoLC)699475034 035 $a(SSID)ssj0000471413 035 $a(PQKBManifestationID)12123767 035 $a(PQKBTitleCode)TC0000471413 035 $a(PQKBWorkID)10427463 035 $a(PQKB)11504101 035 $a(Au-PeEL)EBL630009 035 $a(CaPaEBR)ebr10562138 035 $a(CaONFJC)MIL295543 035 $a(PPN)170607607 035 $a(FR-PaCSA)88812057 035 $a(MiAaPQ)EBC630009 035 $a(EXLCZ)992670000000051605 100 $a20110322d2011 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 00$aModern inorganic synthetic chemistry /$fedited by Ruren Xu, Wenqin Pang, Qisheng Huo 205 $a1st ed. 210 $aAmsterdam ;$aBoston $cElsevier$dc2011 215 $a1 online resource (611 p.) 300 $aDescription based upon print version of record. 311 $a0-444-53599-3 320 $aIncludes bibliographical references and index. 327 $aFront Cover; Modern Inorganic Synthetic Chemistry; Copyright; Contents; Foreword; Preface; Contributors; Chapter 1 Introduction - Frontiers in Modern InorganicSynthetic Chemistry; 1.1Development Of New Synthetic Reactions, Synthetic Routes, Technologies And Associated Basic Scientific Studies; 1.2 Basic Research in Support of Green Synthesis; 1.3 Basic Research on Synthetic and Preparative Routes Under Extreme Conditions; 1.4 Biomimetic Synthesis and Applications of Biotechnology in Inorganic Synthesis 327 $a1.5 Rational Synthesis and Molecular Engineering of Inorganic Compounds with Specific Structures and FunctionsReferences; Chapter 2 High-temperature Synthesis; 2.1 Attainment of high temperature-laboratory furnaces [1] and related techniques [2-6]; 2.2 Types of high-temperature synthetic reactions and routes; 2.3 High-temperature solid-state reaction [11-14]; 2.4 Preparation Of Rare Earthcontaining Materials; 2.5 Sol-gel process and precursors in high-temperature solid synthesis [45-47]; 2.6 Self-Propagating Hightemperature Synthesis (Shs) [51-60] 327 $a2.7 High-Temperature Preparation Of Metal Vapors And Active Molecules For Use In Cryosynthesis [70-72]2.8 High-temperature electrolysis in molten salt system [73-79]; References; Chapter 3 Synthesis and Purification at Low Temperature; 3.1 Attainment And Measurement Of Low And Ultralow Temperatures; 3.2 Vacuum Technique and its Application in Inorganic Synthesis; 3.3 Purification and Separation of Inorganics at Low Temperature; 3.4 The Synthesis of Volatile Inorganic Compounds at Low Temperature; 3.5 Formation of Rare-gas Molecules at Cryogenic Condition 327 $a3.6 Inorganic Synthesis in Liquid Ammonia3.7 Cryosynthesis of Unusual Inorganic Compounds [52-55]; References; Chapter 4 Hydrothermal and Solvothermal Syntheses; 4.1 Foundation of Hydrothermal and Solvothermal Syntheses [1]; 4.2 Functional Materials from Hydrothermal and Solvothermal Systems; 4.3 Hydrothermal Biochemistry; 4.4 Supercritical Water-a Novel Reaction System [106-110]; 4.5 Techniques and Methods; 4.6 Ionothermal Synthesis; References; Chapter 5 High Pressure Synthesis and Preparationof Inorganic Materials; 5.1 Experimental Methods Of Inorganic Synthesis Under High Pressure 327 $a5.2 Effects Of High Pressure On Basic States Of Matters5.3 Effects Of High Pressure On Inorganic Chemical Reactions; 5.4 Effects Of High Pressure On Crystal And Electronic Structures Of Inorganic Compounds; 5.5 Major Roles Of High Pressure Method In Inorganic Synthesis; 5.6 Some Important Inorganic Compounds Synthesized Under High Pressure; References; Chapter 6 Inorganic Photochemical Synthesis; 6.1 The Basic Concepts; 6.2 Experimental Techniques; 6.3 Photochemical Synthesis Of Organometallic Complexes; 6.4 Photochemical Synthesis Of Inorganic Compounds 327 $a6.5 Synthesis Of Inorganic Thin Films Via Photochemical Reactions 330 $a The book has four main parts. In the first part the discussion centers on inorganic synthesis reactions, dealing with inorganic synthesis and preparative chemistry under specific conditions: high temperature, low temperature and cryogenic, hydrothermal and solvothermal, high pressure and super-high pressure, photochemical, microwave irradiation and plasma conditions. The second part systematically describes the synthesis, preparation and assembly of six important categories of compounds with wide coverage of distinct synthetic chemistry systems: coordination compounds, coordination polymers 606 $aInorganic compounds$xSynthesis 606 $aChemistry, Inorganic 615 0$aInorganic compounds$xSynthesis. 615 0$aChemistry, Inorganic. 676 $a541.39 20 676 $a546 701 $aXu$b Ruren$0902284 701 $aPang$b Wenqin$01619111 701 $aHuo$b Qisheng$01619112 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910826151103321 996 $aModern inorganic synthetic chemistry$93951203 997 $aUNINA