LEADER 03861nam 2200625 a 450 001 9910815320103321 005 20240401195951.0 010 $a1-118-68192-4 010 $a1-118-68190-8 010 $a1-118-68188-6 035 $a(CKB)2550000001111872 035 $a(EBL)1441762 035 $a(OCoLC)856625651 035 $a(MiAaPQ)EBC1441762 035 $a(DLC) 2013023483 035 $a(Au-PeEL)EBL1441762 035 $a(CaPaEBR)ebr10748735 035 $a(CaONFJC)MIL511764 035 $a(PPN)189849231 035 $a(EXLCZ)992550000001111872 100 $a20130607d2014 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $2rdacontent 182 $2rdamedia 183 $2rdacarrier 200 00$aLocal structural characterisation /$fedited by Duncan W. Bruce, Dermot O'Hare, Richard I. Walton 205 $a1st ed. 210 $aChichester, West Sussex, U.K. $cJohn Wiley & Sons Inc.$d2014 215 $a1 online resource (474 p.) 225 0$aInorganic materials series 300 $aDescription based upon print version of record. 311 $a1-119-95320-0 311 $a1-299-80513-2 320 $aIncludes bibliographical references and index. 327 $aCover; Series Page; Title Page; Copyright; Inorganic Materials Series Preface; Preface; List of Contributors; Chapter 1: Solid-State Nuclear Magnetic Resonance Spectroscopy; 1.1 Overview; 1.2 Theoretical Background; 1.3 Basic Experimental Methods; 1.4 Calculation of NMR Parameters; 1.5 Applications of Solid-State NMR Spectroscopy; 1.6 Commonly Studied Nuclei; 1.7 NMR of Materials; 1.8 Conclusion; References; Chapter 2: X-ray Absorption and Emission Spectroscopy; 2.1 Introduction: What is Photon Spectroscopy?; 2.2 Electronic Structure and Spectroscopy; 2.3 Calculation of Inner-shell Spectra 327 $a2.4 Experimental Techniques2.5 Experimental Considerations; 2.6 Conclusion; Acknowledgements; REFERENCES; Chapter 3: Neutrons and Neutron Spectroscopy; 3.1 The Neutron and How it is Scattered; 3.2 Why Neutrons?; 3.3 Molecular Hydrogen (Dihydrogen) in Porous Materials; 3.4 Ins and Catalysis; 3.5 CO2 and SO2 Capture; 3.6 What Could be Next?; 3.7 Conclusion; References; Chapter 4: Electron Paramagnetic Resonance Spectroscopy of Inorganic Materials; 4.1 Introduction; 4.2 Electron Spin in a Magnetic Field; 4.3 Spin Hamiltonian and symmetry 327 $a4.4 Principal Types of EPR Spectrum and Their Characteristic Features4.5 Advanced EMR Techniques; REFERENCES; Chapter 5: Analysis of Functional Materials by X-ray Photoelectron Spectroscopy; 5.1 Introduction; 5.2 Imaging XPS; 5.3 Time-resolved High-resolution XPS; 5.4 High- or Ambient-pressure XPS; 5.5 Applications to Inorganic Materials; 5.6 Conclusion; References; Index 330 $a Inorganic materials are at the heart of many contemporary real-world applications, in electronic devices, drug delivery, bio-inspired materials and energy storage and transport. In order to underpin novel synthesis strategies both to facilitate these applications and to encourage new ones, a thorough review of current and emerging techniques for materials characterisation is needed. Examining important techniques that allow investigation of the structures of inorganic materials on the local atomic scale, Local Structural Characterisation discusses: Solid-State NMR S 410 0$aInorganic Materials Series 606 $aChemical structure 606 $aMaterials 615 0$aChemical structure. 615 0$aMaterials. 676 $a543/.5 701 $aBruce$b Duncan W$0861136 701 $aO'Hare$b Dermot$0861137 701 $aWalton$b Richard I$0107204 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910815320103321 996 $aLocal structural characterisation$94005159 997 $aUNINA