LEADER 00996nam0-22003251i-450- 001 990004390650403321 005 20050114123534.0 010 $a0-521-81013-2 035 $a000439065 035 $aFED01000439065 035 $a(Aleph)000439065FED01 035 $a000439065 100 $a19990604d2002----km-y0itay50------ba 101 0 $aeng 102 $aGB 105 $aa-------001yy 200 1 $a<>origins of roman historical commemoration in the visual arts$fPeter J. Holliday 210 $aCambridge$cCambridge University press$d2002 215 $aXXV, 283 p.$c111 ill.$d26 cm 610 0 $aArte romana 676 $a704.94$v21$zita 700 1$aHolliday,$bPeter J.$0176670 801 0$aIT$bUNINA$gRICA$2UNIMARC 901 $aBK 912 $a990004390650403321 952 $a704.94 HOL 1$bBibl.47191$fFLFBC 952 $a704.94 HOL 1 BIS$bBibl.46460$fFLFBC 959 $aFLFBC 996 $aOrigins of roman historical commemoration in the visual arts$9542204 997 $aUNINA LEADER 00881nam0-22003011i-450- 001 990004177560403321 005 20071011122639.0 010 $a84-7039-236-0 035 $a000417756 035 $aFED01000417756 035 $a(Aleph)000417756FED01 035 $a000417756 100 $a19990604d1993----km-y0itay50------ba 101 0 $aspa 105 $aa-------00-g- 200 1 $aRimas$fGustavo Adolfo Bécquer$gedición introducción y notas de José Carlos De Torres 210 $aMadrid$cCastalia$d1993 215 $a242 p.$cill.$d18 cm 225 1 $aClásicos Castalia$v74 700 1$aBécquer,$bGustavo Adolfo$f<1836-1870>$0384820 702 1$aTorres,$bJosé Carlos de 801 0$aIT$bUNINA$gRICA$2UNIMARC 901 $aBK 912 $a990004177560403321 952 $aCOLL.350(74)$bDip.f.m.7933$fFLFBC 959 $aFLFBC 996 $aRimas$920099 997 $aUNINA LEADER 05636nam 2200721 450 001 9910815220103321 005 20230803072441.0 010 $a1-119-07000-7 010 $a1-119-07077-5 035 $a(CKB)2670000000616819 035 $a(EBL)1896043 035 $a(SSID)ssj0001482359 035 $a(PQKBManifestationID)11904142 035 $a(PQKBTitleCode)TC0001482359 035 $a(PQKBWorkID)11432066 035 $a(PQKB)10987042 035 $a(MiAaPQ)EBC1896043 035 $a(Au-PeEL)EBL1896043 035 $a(CaPaEBR)ebr11055106 035 $a(CaONFJC)MIL785575 035 $a(OCoLC)900278010 035 $a(PPN)191886475 035 $a(EXLCZ)992670000000616819 100 $a20150527h20152015 uy 0 101 0 $aeng 135 $aurcnu|||||||| 181 $ctxt 182 $cc 183 $acr 200 00$aMass spectrometry for the analysis of pesticide residues and their metabolites /$fedited by Despina Tsipi, Helen Botitsi, Anastasios Economou 210 1$aHoboken, New Jersey :$cJohn Wiley & Sons, Inc.,$d2015. 210 4$d©2015 215 $a1 online resource (291 p.) 225 1 $aWiley Series on Mass Spectrometry 225 1 $aTHEi Wiley ebooks 300 $aDescription based upon print version of record. 311 $a1-119-06998-X 311 $a1-118-50017-2 320 $aIncludes bibliographical references and index. 327 $aTitle Page; Copyright Page; Contents; List of Contributors; Foreword; Preface; Chapter 1 Pesticide Chemistry and Risk Assessment; 1.1 INTRODUCTION; 1.2 PESTICIDE CHEMISTRY; 1.2.1 Historical Perspective; 1.2.2 Identity and Physicochemical Properties of Pesticides; 1.2.3 Pesticide Classification; 1.2.4 Modes of Action (MoA); 1.3 PESTICIDE METABOLITES AND TRANSFORMATION PRODUCTS; 1.3.1 Biotransformation; 1.3.2 Environmental Fate; 1.4 RISK ASSESSMENT; 1.4.1 Safety Factors; 1.4.2 Ecological Risk Assessment for Pesticides; 1.5 DIETARY EXPOSURE TO PESTICIDES 327 $a1.5.1 Acute Exposure or Short-Term Intake 1.5.2 Chronic Exposure or Long-Term Intake; 1.5.3 Cumulative Exposure to Multiple Substances; 1.6 PESTICIDE RESIDUES IN FOOD; 1.6.1 Maximum Residue Limits; 1.6.2 Residue Definition; 1.6.3 Reporting of Results; 1.6.4 Residue Analysis; REFERENCES; Chapter 2 Legislation, Monitoring, and Analytical Quality Control for Pesticide Residues; 2.1 INTRODUCTION; 2.2 FOOD SAFETY; 2.2.1 CAC of Food and Agriculture Organization/World Health Organization; 2.2.2 EU Legislation; 2.2.3 US Food Regulations; 2.3 WATER QUALITY; 2.3.1 WHO; 2.3.2 EU Water Framework Directive 327 $a2.3.3 US EPA Legislation 2.4 METHOD VALIDATION AND QUALITY CONTROL PROCEDURES FOR PESTICIDE RESIDUES ANALYSIS; 2.4.1 CAC Guidelines; 2.4.2 EU Guidelines: SANCO Document; 2.4.3 FDA and EPA Guidelines; REFERENCES; Chapter 3 Advanced Sample Preparation Techniques for MS Analysis; 3.1 INTRODUCTION; 3.2 CONVENTIONAL EXTRACTION AND CLEANUP PROCEDURES; 3.2.1 LLE; 3.2.2 SPE; 3.2.3 MSPD; 3.2.4 QuEChERS; 3.3 MICROEXTRACTION TECHNIQUES; 3.3.1 Sorbent-Based Microextraction Techniques; 3.3.2 Liquid-Based Microextraction Techniques; 3.4 ALTERNATIVE EXTRACTION AND CLEANUP PROCEDURES 327 $a3.4.1 Alternative Energy Sources to Enhance the Extraction 3.4.2 Coupled-Column Liquid Chromatography (LC/PC, LC/LC Techniques); 3.4.3 Direct Analysis in Real Time; 3.5 CONCLUSIONS; ACKNOWLEDGMENTS; REFERENCES; Chapter 4 Recent Developments in Gas Chromatography-Mass Spectrometry; 4.1 INTRODUCTION; 4.2 ADVANCES IN GC SEPARATIONS; 4.2.1 Multidimensional and Comprehensive Two-Dimensional Gas Chromatography; 4.2.2 Fast GC; 4.2.3 LPGC; 4.3 MASS SPECTROMETRIC IONIZATION TECHNIQUES; 4.3.1 Electron Impact Ionization (EI); 4.3.2 CI (Positive/Negative Modes); 4.3.3 Atmospheric Pressure GC-MS 327 $a4.4 MASS ANALYZERS INTERFACED TO GC 4.4.1 Quadrupole Mass Analyzer; 4.4.2 Ion Trap Mass Analyzer; 4.4.3 QqQ; 4.4.4 TOF; 4.5 MASS SPECTRAL LIBRARIES AND SOFTWARE APPROACHES IN GC-MS ANALYSIS; 4.6. MATRIX EFFECTS IN GC-MS ANALYSIS; 4.7 CONCLUSIONS AND PERSPECTIVES; REFERENCES; Chapter 5 Recent Developments in Liquid Chromatography-Mass Spectrometry: Advances in Liquid Chromatographic Separations and Ionization Techniques/Interfaces; 5.1 INTRODUCTION; 5.2 ADVANCES IN LIQUID CHROMATOGRAPHIC SEPARATIONS; 5.2.1 Ultraperformance Liquid Chromatography 327 $a5.2.2 Hydrophilic Interaction Liquid Chromatography 330 $aProvides an overview of the use of mass spectrometry (MS) for the analysis of pesticide residues and their metabolites. Presents state of the-art MS techniques for the identification of pesticides and their transformation products in food and environment Covers important advances in MS techniques including MS instrumentation and chromatographic separations (e.g. UPLC, HILIC, comprehensive GCxGC) and applications Illustrates the main sample preparation techniques (SPE, QuEChERS, microextraction) used in combination with MS for the analysis of pesticides Describes various established and new 410 0$aWiley-Interscience series on mass spectrometry. 410 0$aTHEi Wiley ebooks. 606 $aPesticides$xAnalysis 606 $aMass spectrometry 615 0$aPesticides$xAnalysis. 615 0$aMass spectrometry. 676 $a632/.95 702 $aTsipi$b Despina 702 $aBotitsi$b Helen 702 $aEconomou$b Anastassios 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910815220103321 996 $aMass spectrometry for the analysis of pesticide residues and their metabolites$93933366 997 $aUNINA