LEADER 05692nam 2200757 450 001 9910810814703321 005 20210604091821.0 010 $a1-118-68284-X 010 $a1-118-68342-0 010 $a1-118-68279-3 035 $a(CKB)3460000000124166 035 $a(EBL)1650859 035 $a(SSID)ssj0001039358 035 $a(PQKBManifestationID)11992685 035 $a(PQKBTitleCode)TC0001039358 035 $a(PQKBWorkID)10985742 035 $a(PQKB)11154108 035 $a(OCoLC)852958648 035 $a(MiAaPQ)EBC1650859 035 $a(DLC) 2013028463 035 $a(MiAaPQ)EBC4037530 035 $a(Au-PeEL)EBL1650859 035 $a(CaPaEBR)ebr10849292 035 $a(CaONFJC)MIL584527 035 $a(OCoLC)874321911 035 $a(Au-PeEL)EBL4037530 035 $a(CaPaEBR)ebr11111795 035 $a(PPN)190226501 035 $a(EXLCZ)993460000000124166 100 $a20130628d2014 uy| 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 10$aEnvironmental trace analysis $etechniques and applications /$fJohn R. Dean 205 $a1st ed. 210 1$aChichester, West Sussex, United Kingdom :$cJohn Wiley & Sons Inc.,$d2014. 215 $a1 online resource (280 p.) 300 $aDescription based upon print version of record. 311 $a1-119-96271-4 311 $a1-119-96270-6 320 $aIncludes bibliographical references and index. 327 $aEnvironmental Trace Analysis: Techniques and Applications; Contents; About the Author; Preface; Acknowledgements; Acronyms and Abbreviations; 1 Basic Laboratory Procedures; 1.1 Introduction; 1.2 Health and Safety Issues; 1.3 Sample Handling: Solid Samples; 1.4 Sample Handling: Liquid Samples; 1.5 Sample Handling: Gases/Vapour Samples; 1.6 Summary; Further Reading; 2 Investigative Approach for Environmental Analysis; 2.1 Introduction; 2.2 Recording of Practical Results; 2.2.1 Useful Tips on Presenting Data in Tables; 2.2.2 Useful Tips on Presenting Data in Graphical Form 327 $a2.2.3 Useful Tips for Templates for Presenting Data in Your Notebook2.3 Significant Figures; 2.4 Units; 2.5 Summary; Appendix; Example Template A: Sample Collection; Example Template B: Sample Treatment; Example Template C: Sample Preparation for Inorganic Analysis; Example Template D: Instrumental Analysis; Example Template E: Sample Preparation for Organic Analysis; Example Template F: Instrumental Analysis; Further Reading; 3 Principles of Quantitative Environmental Analysis; 3.1 Introduction; 3.2 Preparing Solutions for Quantitative Work; 3.3 Calibration Graphs 327 $a3.4 Limits of Detection/Quantitation3.5 Calculations: Dilution or Concentration Factors; 3.6 Quality Assurance; 3.6.1 Certified Reference Materials; 3.7 Summary; References; Further Reading; 4 Environmental Sampling; 4.1 Introduction; 4.2 Sampling Soil (and Sediments); 4.3 Sampling Water; 4.4 Sampling Air; 4.5 Summary; Further Reading; 5 Storage of Samples for Analysis; 5.1 Introduction; 5.2 Choice of Storage Container for Liquid Samples; 5.3 Preservation Techniques for Liquid Samples; 5.4 Storage and Preservation of Solid Samples; 5.5 Storage and Preservation of Gaseous Samples; 5.6 Summary 327 $aFurther Reading6 Preparation of Environmental Solid Samples for Inorganic Analysis; 6.1 Introduction; 6.2 Decomposition Techniques; 6.3 Selective Extraction Methods; 6.3.1 Single Extraction Methods; 6.3.2 Sequential Extraction Method; 6.3.3 Chemometric Identification of Substrates and Element Distributions (CISED) Method; 6.4 Physiologically-Based Extraction Test or In Vitro Gastrointestinal Extraction; 6.4.1 Procedure for Gastric Extraction; 6.4.2 Procedure for Gastric + Intestinal Extraction; 6.5 Earthworms; 6.5.1 Procedure for Earthworm Bioaccumulation Studies (Sandoval et al., 2001) 327 $a6.6 SummaryAppendix A: Extraction Reagents for Single Extraction Methods; Appendix B: Extraction Reagents for Sequential Extraction Method; Appendix C: Extraction Reagents for In Vitro Gastrointestinal Extraction Using the Unified Bioaccessibility Method (and the FOREhST Method); References; Further Reading; 7 Preparation of Environmental Liquid Samples for Inorganic Analysis; 7.1 Introduction; 7.2 Liquid-Liquid Extraction of Metals; 7.2.1 Procedure for APDC Extraction into MIBK; 7.3 Ion Exchange; 7.3.1 Chelation Ion Exchange; 7.3.2 Procedure for Batch Ion Exchange Extraction 327 $a7.4 Co-precipitation 330 $a"This book covers all aspects of environmental trace analysis from sampling through to preparation of the sample to the analytical techniques used to quantify the level of trace metals or organic compounds. The book is divided into two areas: sample preparation for inorganic analysis and sample preparation for organic analysis. This allows the reader to focus on key aspects related to the preparation of samples for their subsequent analysis. Selected case studies provide the reader with the opportunity to consider how the sample preparation approach can be optimized for their own area of expertise"--$cProvided by publisher. 606 $aTrace analysis$xMethodology 606 $aEnvironmental chemistry$xMethodology 606 $aSampling 615 0$aTrace analysis$xMethodology. 615 0$aEnvironmental chemistry$xMethodology. 615 0$aSampling. 676 $a577.27028/7 686 $aSCI013040$2bisacsh 700 $aDean$b John R.$0312730 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910810814703321 996 $aEnvironmental trace analysis$9259648 997 $aUNINA