LEADER 04970nam 22005173u 450 001 9910782657703321 005 20230829000758.0 010 $a1-282-16718-9 010 $a9786612167188 010 $a0-08-051873-7 035 $a(CKB)1000000000707198 035 $a(EBL)428602 035 $a(OCoLC)437112422 035 $a(MiAaPQ)EBC428602 035 $a(EXLCZ)991000000000707198 100 $a20130701d2006|||| u|| | 101 0 $aeng 135 $aur|n|---||||| 200 10$aMicrowave-assisted Organic Synthesis$b[electronic resource] $eOne Hundred Reaction Procedures 210 $aBurlington $cElsevier Science$d2006 215 $a1 online resource (215 p.) 225 1 $aTetrahedron organic chemistry series ;$vv.25 300 $aDescription based upon print version of record. 311 $a0-08-044624-8 327 $aCover Page; Title Page; Copyright Page; Table of Contents; Preface; Acknowledgements; Chapter 1 Interaction of microwaves with different materials; Chapter 2 Microwave effect vs. thermal effect; 2.1 Thermal activation during microwave irradiation; 2.2 Non-thermal activation during microwave irradiation; Chapter 3 Microwave equipment; 3.1 Microwave generators; 3.2 Transmission lines (waveguides); 3.3 Microwave applicators (cavities); 3.4 Microwave reactors; 3.5 Temperature monitoring; Chapter 4 Reaction vessels and glassware 327 $aChapter 5 Techniques for conducting chemical reactions under microwave irradiationChapter 6 Safety precautions on the application of microwaves in laboratory; Chapter 7 Reactions under microwave conditions; 7.1 Reactions in homogenous media and solvent; 7.1.1 2,6-Dimethyl-4-phenyl-l,4-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester; 7.1.2 6-Methyl-2-oxo-4-phenyl-l,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester; 7.1.3 Biphenyl; 7.1.4 l-Nitro-4-phenylethynyl-benzene; 7.1.5 3-(4-Nitro-phenyl)-acrylic acid ethyl ester; 7.1.6 2-Carbazol-9-yl-ethanol 327 $a7.1.7 2-Imidazol-1-yl-ethanol7.1.8 Pyridine N-oxide; 7.1.9 Cyclohexanon; 7.1.10 4-Iodo-N,N-dimethylaniline; 7.1.11 2-Iodo-4-nitroaniline; 7.1.12 3-Bromocarbazole; 7.1.13 3,6-Dichlorocarbazole; 7.1.14 3-Iodocarbazole; 7.1.15 l,1'-Bi-2-naphthol; 7.1.16 9,10-Dihydroanthraceno-9,10-alpha,beta-succinic anhydride; 7.1.17 2,4-Dihydroxybenzaldehyde; 7.1.18 4-Diethylaminosalicylaldehyde; 7.1.19 9-(2-Chloroethyl)carbazole-3-carbaldehyde; 7.1.20 8-Hydraxy-l,l,7,7-tetramethyljulolidine -9-carboxaldehyde; 7.1.21 7-Diethylamino-2-oxo-2H-chromene-3-carboxylic acid; 7.1.22 1-Iododecane 327 $a7.2 Reactions of reagents supported on mineral supports7.2.1 Diphenylbutadiyne; 7.2.2 2,4,5-Triphenylimidazole; 7.2.3 1-(4-Nitro-phenyl)-piperidine; 7.2.4 2-Nitro-1-phenyl-propan-1-ol; 7.2.5 Phenyl-[1-phenyl-methylidene]amine; 7.2.6 N,N-Diphenylacetamide; 7.2.7 Dibenzyl-(3-phenyl-prop-2-ynyl)amine; 7.2.8 l,2-Diphenyl-ethane-l,2-dione (benzil); 7.2.9 3-Methyl-2-propyl-1H-indole; 7.2.10 Azepan-2-one (e-caprolactam); 7.2.11 Octyl acetate; 7.2.12 Octanal; 7.2.13 Octan-2-one; 7.2.14 Anthraquinone; 7.2.15 9-Fluorenone; 7.2.16 2-(4-Nitrophenyl)-6-phenoxyhexanoic acid ethyl ester 327 $a7.2.17 2-(4-Nitrophenyl)-10-phenylsulfanyl-decanoic acid ethyl ester7.2.18 l-Phenethylindole-2-carboxylic acid ethyl ester; 7.2.19 5-Phenyl-2-((1-phenylmethylidene)amino)pentanoic acid methyl ester; 7.2.20 N-Benzylphenylacetamide; 7.3 Solvent-free phase transfer catalysis (PTC) reactions; 7.3.1 trans-l,2-Diphenylethylene (trans-stilbene); 7.3.2 1-Phenyl-naphthalene; 7.3.3 Benzofuran-2-carboxylic acid ethyl ester; 7.3.4 6-Diethylamino-benzofuran-2-carboxylic acid ethyl ester; 7.3.5 Naphtho[2,1-b]furan-2-carboxylic acid ethyl ester; 7.3.6 Dioctyl ether; 7.3.7 Octanoic acid 327 $a7.3.8 Octan-2-one 330 $aMicrowave-assisted Organic Synthesis - One Hundred Reaction Procedures provides readers with a broad overview of microwave assisted Organic Synthesis, enabling students and researchers alike to produce more efficient and high yield syntheses while saving time and resources. The work addresses key problems faced by chemistry laboratories in academia and in industry, that of an ever increasing need for procedures which are low-waste, energy efficient, high yield, occur over a short reaction period, and use environmentally friendly solvents. All these factors play an important role in the 410 0$aTetrahedron organic chemistry series 606 $aOrganic compounds 606 $aOrganic compounds --Synthesis. Microwaves 615 4$aOrganic compounds. 615 4$aOrganic compounds --Synthesis. Microwaves. 676 $a547.2 676 $a547.2 22 700 $aBogdal$b Dariusz$0905991 801 0$bAU-PeEL 801 1$bAU-PeEL 801 2$bAU-PeEL 906 $aBOOK 912 $a9910782657703321 996 $aMicrowave-assisted Organic Synthesis$93857790 997 $aUNINA