LEADER 05287nam 2200625Ia 450 001 9910146269003321 005 20170816142740.0 010 $a1-281-31169-3 010 $a9786611311698 010 $a3-527-61197-5 010 $a3-527-61199-1 035 $a(CKB)1000000000441537 035 $a(EBL)482133 035 $a(OCoLC)609855541 035 $a(SSID)ssj0000299045 035 $a(PQKBManifestationID)11254046 035 $a(PQKBTitleCode)TC0000299045 035 $a(PQKBWorkID)10240357 035 $a(PQKB)10315277 035 $a(MiAaPQ)EBC482133 035 $a(EXLCZ)991000000000441537 100 $a20050624d2006 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 00$aHPLC made to measure$b[electronic resource] $ea practical handbook for optimization /$fedited by Stavros Kromidas 210 $aWeinheim $cWiley-VCH ;$a[Chichester $cJohn Wiley, distributor]$dc2006 215 $a1 online resource (789 p.) 300 $aDescription based upon print version of record. 311 $a3-527-31377-X 320 $aIncludes bibliographical references and index. 327 $aHPLC Made to Measure; Foreword; Preface; Contents; List of Contributors; Structure of the Book; 1 Fundamentals of Optimization; 1.1 Principles of the Optimization of HPLC Illustrated by RP-Chromatography; 1.1.1 Before the First Steps of Optimization; 1.1.2 What Exactly Do We Mean By "Optimization"?; 1.1.3 Improvement of Resolution ("Separate Better"); 1.1.3.1 Principal Possibilities for Improving Resolution; 1.1.3.2 What has the Greatest Effect on Resolution?; 1.1.3.3 Which Sequence of Steps is Most Logical When Attempting an Optimization?; 1.1.3.4 How to Change k, ?, and N 327 $a1.1.3.4.1 Isocratic Mode1.1.3.4.2 Gradient Mode; 1.1.3.4.3 Acetonitrile or Methanol?; 1.1.4 Testing of the Peak Homogeneity; 1.1.5 Unknown Samples: "How Can I Start?"; Strategies and Concepts; 1.1.5.1 The "Two Days Method"; 1.1.5.2 "The 5-Step Model"; 1.1.6 Shortening of the Run Time ("Faster Separation"); 1.1.7 Improvement of the Sensitivity ("To See More", i.e. Lowering of the Detection Limit); 1.1.8 Economics in HPLC ("Cheaper Separation"); 1.1.9 Final Remarks and Outlook; References; 1.2 Fast Gradient Separations; 1.2.1 Introduction; 1.2.2 Main Part; 1.2.2.1 Theory; 1.2.2.2 Results 327 $a1.2.2.2.1 General Relationships1.2.2.2.2 Short Columns, Small Particles; 1.2.2.2.3 An Actual Example; 1.2.2.3 Optimal Operating Conditions and Limits of Currently Available Technology; 1.2.2.4 Problems and Solutions; 1.2.2.4.1 Gradient Delay Volume; 1.2.2.4.2 Detector Sampling Rate and Time Constant; 1.2.2.4.3 Ion Suppression in Mass Spectrometry; References; 1.3 pH and Selectivity in RP-Chromatography; 1.3.1 Introduction; 1.3.2 Main Section; 1.3.2.1 Ionization and pH; 1.3.2.2 Mobile Phase and pH; 1.3.2.2.1 Buffer Capacity 327 $a1.3.2.2.2 Changes of pK and pH Value in the Presence of an Organic Solvent1.3.2.3 Buffers; 1.3.2.3.1 Classical HPLC Buffers; 1.3.2.3.2 MS-Compatible pH Control; 1.3.2.4 Influence of the Samples; 1.3.2.4.1 The Sample Type: Acids, Bases, Zwitterions; 1.3.2.4.2 Influence of the Organic Solvent on the Ionization of the Analytes; 1.3.3 Application Example; 1.3.4 Troubleshooting; 1.3.4.1 Reproducibility Problems; 1.3.4.2 Buffer Strength and Solubility; 1.3.4.3 Constant Buffer Concentration; 1.3.5 Summary; References; 1.4 Selecting the Correct pH Value for HPLC; 1.4.1 Introduction 327 $a1.4.2 Typical Approaches to pH Selection1.4.3 Initial pH Selection; 1.4.4 Basis of pK(a) Prediction; 1.4.5 Correction of pH Based on Organic Content; 1.4.6 Optimization of Mobile Phase pH Without Chemical Structures; 1.4.7 A Systematic Approach to pH Selection; 1.4.8 An Example - Separation of 1,4-Bis[(2-pyridin-2-ylethyl)thio]butane-2,3-diol from its Impurities; 1.4.9 Troubleshooting Mobile Phase pH; 1.4.10 The Future; 1.4.11 Conclusion; References; 1.5 Optimization of the Evaluation in Chromatography; 1.5.1 Evaluation of Chromatographic Data - An Introduction; 1.5.2 Working Range 327 $a1.5.3 Internal Standard 330 $aThe only topical HPLC book to focus on optimization, this volume addresses the needs of HPLC users who wish to constantly improve their methods, in particular in terms of throughput, accuracy and cost-effectiveness. This handbook features contributions from such bestselling authors as John W. Dolan, Michael McBrien, Veronika R. Meyer, Uwe D. Neue, Lloyd R. Snyder, and Klaus K. Unger, as well as from scientists working for major companies, including Agilent, AstraZeneca, Merck, Schering, Tosoh Biosep, VWR, and Waters. It covers essential aspects of optimization in general, optimization in 606 $aHigh performance liquid chromatography$xMethodology 606 $aLiquid chromatography 608 $aElectronic books. 615 0$aHigh performance liquid chromatography$xMethodology. 615 0$aLiquid chromatography. 676 $a543.0894 676 $a543.84 701 $aKromidas$b Stavros$0878029 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910146269003321 996 $aHPLC made to measure$92072092 997 $aUNINA LEADER 05627oam 2200733I 450 001 9910779258203321 005 20230802005251.0 010 $a1-136-25185-5 010 $a1-280-77674-9 010 $a9786613687135 010 $a1-136-25186-3 010 $a0-203-10499-4 024 7 $a10.4324/9780203104996 035 $a(CKB)2550000000104250 035 $a(EBL)981804 035 $a(OCoLC)804665909 035 $a(SSID)ssj0000695567 035 $a(PQKBManifestationID)11412762 035 $a(PQKBTitleCode)TC0000695567 035 $a(PQKBWorkID)10676234 035 $a(PQKB)11134665 035 $a(MiAaPQ)EBC981804 035 $a(Au-PeEL)EBL981804 035 $a(CaPaEBR)ebr10572222 035 $a(CaONFJC)MIL368713 035 $a(OCoLC)802047555 035 $a(FINmELB)ELB134927 035 $a(EXLCZ)992550000000104250 100 $a20180706e20121991 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 04$aThe future of the Arab nation $echallenges and options /$fKhair el-Din Haseeb. [et al.] ; with a new introduction by Roger Owen 210 1$aLondon :$cRoutledge,$d2012. 215 $a1 online resource (535 p.) 225 1 $aRoutledge Library Editions: The Arab Nation 300 $aFirst published in 1991 by Routledge. 311 $a0-415-75218-3 311 $a0-415-62394-4 320 $aIncludes bibliographical references (p. [496]-509) and index. 327 $aFront Cover; The Future of the Arab Nation; Copyright Page; Contents; List of figures; List of tables; Acknowledgements; Conventions; Introduction to the 2012 Edition; Introduction to the English-language edition: Professor Roger Owen; Introduction: Khair el-Din Haseeb; Part I: Analysis of the prospects of the future of the Arab world: aims and methodology; 1. The aims of the study and its relation to previous studies of the Arab world; Why study the future?; Why the Arab world?; The outcome of previous studies; The need for a new study; 2. The selected methodology 327 $aThe role of prospective analysis in future studiesThe special characteristics of prospective analysis methodology; Components and hypotheses; Part II: The basis for prospective analysis: the past, the present and the critical features of a changing world; 3. The legacy and lessons of the past; From the seventh century to the Arab country state; The colonial invasion and the rise of state nationalism; 4. The present: positive and negative aspects; The present Arab situation; The present situation of society and the state; The economic situation; The extent of political achievement 327 $a5. International horizons and entry into the twenty-firstcenturyThe economic future; Scientific and technological prospects; International cultural values and trends; The Arabs and the international power struggle; Part III: Future Arab scenarios: reality, potentiality and the ability to pay the price; 6. The true Arab potential: a look into the future; The appropriateness of the database; Human resources; Water and agricultural land; Mineral resources; 7. The scenario of division: Limited prospects and probability of fragmentation; Introduction; The international and regional orders 327 $aEconomic developments in the scenarioSocio-economic interactions; The implications of the scenario for society and the state; The end result; Policy options: a struggle for survival; Conclusion; 8. The scenario of co-ordination and co-operation: the difficulties of standing firm in the face of international circumstances; Introduction; The general outline of the scenario; Factors underlying the mounting challenges and a more effective response to them; The driving forces behind inter-Arab co-operation; Economic developments within the context of this scenario 327 $aThe international and regional contextsThe social implications of the scenario; The end result; Policies and mechanisms; Conclusion; 9. The scenario of Arab unity: a desire for change and theworld of large entities; Introduction; Preconditions for the scenario; The general features of the scenario; The implications of the scenario for society and the state; The foreign relations of the Arab federal state; The developmental prospects of the Arab federal state; Requirements; Conclusion; Part IV: Bridges to the future: a debate concerninginstruments for the conception and planningof change 327 $a10. Conclusion: What next? 330 $aWhat is the place of the Arab states as a new world order emerges? How can the Arab world respond positively to change as the new Europe emerges, political relationships are restructured, and the information revolution transforms the global economy? To what extent are the Arab states in danger of falling prey to increasing disunity and fragmentation? The book is the result of a major research programme in which Arab social scientists outline some of the paths which could be taken by the Arab world over the next 25 years. It presents a detailed analysis of resources in the Arab world 410 0$aRoutledge Library Editions: The Arab Nation 606 $aArab countries$xForecasting 607 $aArab countries$xHistory 607 $aArab countries$xForecasting 615 0$aArab countries$xForecasting. 676 $a303.49174927 676 $a320.9174927 701 $aHaseeb$b K$01515818 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910779258203321 996 $aThe future of the Arab nation$93751827 997 $aUNINA LEADER 02408nam 2200517 450 001 9910816298503321 005 20210426220929.0 010 $a1-80034-028-1 010 $a1-909821-36-5 035 $a(CKB)4100000005182568 035 $a(Au-PeEL)EBL5485069 035 $a(OCoLC)1048779321 035 $a(StDuBDS)EDZ0002316093 035 $a(MiAaPQ)EBC5485069 035 $a(EXLCZ)994100000005182568 100 $a20200724e20201998 fy| 0 101 0 $aeng 135 $aurcnu|||||||| 181 $ctxt$2rdacontent 182 $cc$2rdamedia 183 $acr$2rdacarrier 200 10$aEuropean Jewry in the age of mercantilism 1550-1750 /$fJonathan I. Israel$b[electronic resource] 205 $aThird edition. 210 1$aOxford :$cThe Littman Library of Jewish Civilization,$d2020. 215 $a1 online resource (xix, 266 pages) $cillustrations, map 225 1 $aLiverpool scholarship online 300 $aThis edition previously issued in print: 1998. 311 $a1-874774-42-0 320 $aIncludes bibliographical references and index. 330 8 $aThis survey history of Jewish life and culture in early modern Europe is the first to focus on the sixteenth and seventeenth centuries as a radically new phase in Jewish history. The volume lays particular emphasis on the reversal of trends in western and central Europe in the late sixteenth century, which was followed by a rapid increase in Jewish numbers and activity, and far-reaching reorganization of Jewish society and institutions. A major consequence of these changes was a much expanded and more varied Jewish role in European civilization as a whole. The first edition of this book was the joint winner of the Wolfson Literary Prize for History in 1986. For this third edition, the text has been updated and includes a new introduction. 410 0$aLiverpool scholarship online. 606 $aJews$zEurope$xHistory$y16th century 606 $aJews$zEurope$xHistory$y17th century 606 $aJews$xHistory$y70-1789 607 $aEurope$xEthnic relations 615 0$aJews$xHistory 615 0$aJews$xHistory 615 0$aJews$xHistory 676 $a940/.04924 700 $aIsrael$b Jonathan$f1946-$0258955 801 0$bStDuBDS 801 1$bStDuBDS 906 $aBOOK 912 $a9910816298503321 996 $aEuropean jewry in the age of mercantilism$91472908 997 $aUNINA