LEADER 05144nam 2200649Ia 450 001 996202924503316 005 20230213211433.0 010 $a1-282-30711-8 010 $a9786612307119 010 $a0-470-18691-7 010 $a0-470-18839-1 035 $a(CKB)1000000000376547 035 $a(EBL)469198 035 $a(OCoLC)814414287 035 $a(SSID)ssj0000360398 035 $a(PQKBManifestationID)11305256 035 $a(PQKBTitleCode)TC0000360398 035 $a(PQKBWorkID)10326439 035 $a(PQKB)11706259 035 $a(MiAaPQ)EBC469198 035 $a(EXLCZ)991000000000376547 100 $a20710404d1967 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 10$aFused pyrimidines$hPart I$iQuinazolines$b[electronic resource] /$fW.L.F. Armarego; edited by D.J. Brown 205 $a99th ed. 210 $aNew York $cInterscience Publishers$d1967 215 $a1 online resource (564 p.) 225 1 $aThe chemistry of heterocyclic compounds ;$v24/1 300 $aDescription based upon print version of record. 311 $a0-470-38203-1 320 $aIncludes bibliographies and indexes. 327 $aQUINAZOLINES; Contents; Tables; I. Introduction; 1. History; 2. Nomenclature; 3. The Dual Character of Quinazolines; 4. General Summary of Quinazoline Chemistry; A. Syntheses; a. Primary Syntheses; b. Secondary Syntheses; B. The Heightened Reactivity of 2- and 4-Alkyl Groups; C. Addition and Substitution Reactions, and Nucleophilic Metathesis; D. N-Oxides; E. Tautomerism; F. Oxidation and Reduction; G. Rearrangements; H. Biological Activity in Quinazolines; 5. Tables; Introduction; 6. References; II. Quinazoline; 1. Synthesis of Quinazoline; 2. Physical Properties 327 $aII.1. Quinazoline and 3-Alkyl Derivatives A. Theoretical Aspects; B. Spectra; a. Ultraviolet Spectra; b. Phosphorescence Spectra; c. Infrared Spectra; d. Proton Magnetic Resonance Spectra; e. Mass Spectra; C. Covalent Hydration; a. Covalent Hydration in Quinazoline; b. Effect of Substituents in the Pyrimidine Ring on Covalent Hydration; (i) Effect of substituents in position 4; (ii) Effect of saubstituenta in position 2; c. Effect Substituents in the Benzene Ring on Covalent Hydration; II.2. Electronic Effects and Hydration in 2-Substituted Quinazoline Cations 327 $aII.3. Ionization and Covalent Hydration of Quinazolines in Water at 20°II.4. Ionization Constants of Substituted Quinazolines in Water at 20°; D. Polarography; 3. Chemical Reactivity of Quinazoline; A. Hydrolysis, Oxidation, and Reduction; B. Electrophilic and Nucleophilic Substitution, and Alkylation; C. Addition Reactions; 4. References; III. C-Alkyl- and C-Arylquinazolines; 1. Methods of Preparation; A. Bischler's Synthesis; B. Oxidation of 3, 4-Dihydroquinazolines; C. Decarboxylation of Acids; D. From N'-ToIuene-p-sulphonylydrazino Derivatives; E. From Imidoyl Chlorides and Nitriles 327 $aF. From Aryl Diazonium Salts and NitrilesG. From 4-Chloro or 4-cyanoquinazolines and Grignard Reagents; H. From Chloro- or Cyanoquinazolines and Substances with an Active Methylene Group; I. Reidel's Synthesis; J. Miscellaneous; 2. Properties; A. Physical Properties; B. Chemical Properties; a. The Heightened Reactivity of 2- and 4-Methyl Groups; b. Oxidation and Reduction; c. Electrophilic Substitution; d. Alkylation; e. Reactivity of the Substituted Carbon Atoms Attached to C(2)and C(4); 3. Tables; III.1. 2-Alkyl- and Aryl- (including Heteroaryl-) quinazolines 327 $aIII.2. 4-Alkyl- and Aryl- (including Heteroaryl-) quinazolineaIII.3. 2,4-Disubstituted Alkyl- and Arylquinazolines; III.4. Alkylquinazolines Substituted in the Benzene Ring; III.5. Alkyl- and Arylquinazolines Substituted in Both Rings; III.6. Miscellaneous Alkyl- and Arylquinazolines (including Quina-zolinium Salts}; 4. References; IV. Oxoquinazolines and 5-, 6-, 7-, and 8-Hydroxyquinazolines; 1. 2-Oxoquinazolines; A. Preparation; B. Properties; 2. 3,4- and 1,4-Dihydro-4-oxoquinasolines; A. Preparation of 3,4-Dihydro-4-oxoquinszolines; a. Niementowski's Synthesis 327 $ab. Cyclization of o-Amidobenzamides 330 $aChemistry of Heterocyclic Compounds publishes articles, letters to the Editor, reviews, and minireviews on the synthesis, structure, reactivity, and biological activity of heterocyclic compounds including natural products. The journal covers investigations in heterocyclic chemistry taking place in scientific centers of all over the world, including extensively the scientific institutions in Russia, Ukraine, Latvia, Lithuania and Belarus. 410 0$aChemistry of heterocyclic compounds ;$vv. 24/1. 606 $aQuinazoline 606 $aHeterocyclic compounds 615 0$aQuinazoline. 615 0$aHeterocyclic compounds. 676 $a547/.59/05 700 $aArmarego$b W. L. F$0440089 701 $aBrown$b D. 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