LEADER 06239nam 2201033z- 450 001 9910557299503321 005 20210501 035 $a(CKB)5400000000041044 035 $a(oapen)https://directory.doabooks.org/handle/20.500.12854/68970 035 $a(oapen)doab68970 035 $a(EXLCZ)995400000000041044 100 $a20202105d2020 |y 0 101 0 $aeng 135 $aurmn|---annan 181 $ctxt$2rdacontent 182 $cc$2rdamedia 183 $acr$2rdacarrier 200 00$aFive Years of Separations$eFeature Paper 2018 210 $aBasel, Switzerland$cMDPI - Multidisciplinary Digital Publishing Institute$d2020 215 $a1 online resource (152 p.) 311 08$a3-03936-924-5 311 08$a3-03936-925-3 330 $aFive years of Separations are celebrated by a collection of ten feature articles: one review and nine research articles on topics of current interest. Applications of Gas Chromatography for the Analysis of Tricyclic Antidepressants in Biological Matrices are presented focusing on novel extraction techniques and novel materials used for sample preparation due to the great demand for method development for the determination of TCAs in biofluids, especially for therapeutic drug monitoring. Original research articles include the following: 1. Insights into the Mechanism of Separation of Bisphosphonates by Zwitterionic Hydrophilic Interaction Liquid Chromatography: Application to the Quantitation of Risedronate in Pharmaceuticals. 2. A method based on micro-matrix solid-phase dispersion (?-MSPD) followed by gas-chromatography tandem mass spectrometry (GC-MS/MS), developed to analyze UV filters in personal care products. 3. The performance of a vibratory shear-enhanced process (VSEP) combined with an appropriate membrane unit for the treatment of simulated or industrial tannery wastewaters. 4. A method for the analysis of thyroid hormones by liquid chromatography-mass spectrometry that was used for the dissolution testing of single- and dual-component thyroid hormone supplements via a two-stage biorelevant dissolution procedure. 5. A method involving the collection and determination of organic and inorganic gunshot residues on hands using online in-tube solid-phase microextraction (IT-SPME) coupled to miniaturized capillary liquid chromatography with diode array detection (CapLC-DAD) and scanning electron microscopy coupled to energy dispersion X-ray (SEM-EDX), respectively, for quantifying both residues. 6. The gas chromatographic retention behavior of 16 polycyclic aromatic hydrocarbons (PAHs) and alkylated PAHs on a new ionic liquid stationary phase, 1,12-di(tripropylphosphonium) dodecane bis(trifluoromethanesulfonyl)imide (SLBŪ-ILPAH) intended for the separation of PAH mixtures, which was compared with the elution pattern on more traditional stationary phases: a non-polar phenyl arylene (DB-5ms) and a semipolar 50% phenyl dimethyl siloxane (SLB PAHms) column. 7. The Multiple-Stage Precursor Ion Separation and High Resolution Mass Spectrometry toward Structural Characterization of 2,3-Diacyltrehalose Family from Mycobacterium tuberculosis 8. The use of micellar electrokinetic chromatography (MEKC) for studying the hydrophobic character of modified Monomethyl Auristatin E derivatives, as Novel Candidates for the Design of Antibody-Drug Conjugates, which are promising state-of-the-art biopharmaceutical drugs for selective drug-delivery applications and the treatment of diseases such as cancer. 9. The use of recycled diatomaceous earth as the extraction phase in solid phase microextraction (SPME) technique for the determination of polycyclic aromatic hydrocarbons (PAHs) in river water samples, with separation/detection performed by gas chromatography-mass spectrometry (GC-MS). 517 $aFive Years of Separations 606 $aResearch & information: general$2bicssc 610 $aalkylated polycyclic aromatic hydrocarbons (alkylated PAHs) 610 $aantibody-drug conjugate 610 $abiological fluids 610 $abiopharmaceutical 610 $abisphosphonates 610 $acapillary liquid chromatography 610 $achromatographic selectivity 610 $acosmetic analysis 610 $acytotoxicity 610 $adiacyltrehalose 610 $adiphenylamine 610 $adissolution 610 $adry cotton swab 610 $afragrance allergens 610 $agas chromatography 610 $agas chromatography-mass spectrometry 610 $aGC-MS/MS 610 $aglycolipid 610 $agunshot residues 610 $ahands 610 $ahydrophobicity 610 $ain-tube solid-phase extraction 610 $aionic liquid stationary phase 610 $alinear ion trap 610 $aliquid chromatography-mass spectrometry 610 $amatrix solid-phase dispersion 610 $amembrane filtration-treatment 610 $amembrane fouling mechanism 610 $amembrane type-operation 610 $amicellar electrokinetic chromatography 610 $aminiaturized extraction technique 610 $aMycobacterium tuberculosis 610 $aPDA 610 $apersonal care products 610 $aplasticizers 610 $apolycyclic aromatic hydrocarbons 610 $apreservatives 610 $aquantitation 610 $arecycled diatomaceous earth 610 $arisedronate 610 $asample treatment 610 $aSEM-EDX 610 $asolid phase microextraction 610 $asynthetic musks 610 $atablets 610 $atandem mass spectrometry 610 $atannery industrial wastewater 610 $athyroid 610 $atiludronate 610 $atricyclic antidepressants (TCAs) 610 $aUV filters 610 $avibratory shear-enhanced process (VSEP) 610 $aZIC-HILIC 610 $azoledronate 610 $a?-MSPD 615 7$aResearch & information: general 700 $aSamanidou$b Victoria$4edt$01174648 702 $aLucena$b Rafael$4edt 702 $aSamanidou$b Victoria$4oth 702 $aLucena$b Rafael$4oth 906 $aBOOK 912 $a9910557299503321 996 $aFive Years of Separations$93029952 997 $aUNINA