LEADER 05678nam 2200745Ia 450 001 9910139078003321 005 20200520144314.0 010 $a9786613905482 010 $a9781283593038 010 $a1283593033 010 $a9781118520918 010 $a1118520912 010 $a9781118520994 010 $a1118520998 010 $a9781118520925 010 $a1118520920 035 $a(CKB)2560000000092791 035 $a(EBL)1016650 035 $a(SSID)ssj0000711463 035 $a(PQKBManifestationID)11444688 035 $a(PQKBTitleCode)TC0000711463 035 $a(PQKBWorkID)10693319 035 $a(PQKB)10399618 035 $a(MiAaPQ)EBC1016650 035 $a(OCoLC)676862591 035 $a(Perlego)1010357 035 $a(EXLCZ)992560000000092791 100 $a19960312d1996 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 10$aIntroduction to X-ray powder diffractometry /$fRon Jenkins, Robert L. Snyder 210 $aNew York $cWiley$dc1996 215 $a1 online resource (428 p.) 225 0$aChemical analysis ;$vv. 138 300 $a"A Wiley-Interscience publication." 311 08$a9780471513391 311 08$a0471513393 320 $aIncludes bibliographical references and index. 327 $aIntroduction to X-ray Powder Diffractometry; CONTENTS; PREFACE; CUMULATIVE LISTING OF VOLUMES IN SERIES; CHAPTER 1. CHARACTERISTICS OF X-RADIATION; 1.1. Early Development of X-ray Diffraction; 1.2. Origin of X-radiation; 1.3. Continuous Radiation; 1.4. Characteristic Radiation; 1.4.1. The Photoelectric Effect; 1.4.2. The Auger Effect; 1.4.3. Fluorescent Yield; 1.4.4. Selection Rules; 1.4.5. Nondiagram Lines; 1.4.6. Practical Form of the Copper K Spectrum; 1.5. Scattering of X-rays; 1.5.1. Coherent Scatter; 1.5.2. Compton Scatter; 1.6. Absorption of X-rays; 1.7. Safety Considerations 327 $aReferencesCHAPTER 2. THE CRYSTALLINE STATE; 2.1. Introduction to the Crystalline State; 2.2. Crystallographic Symmetry; 2.2.1. Point Groups and Crystal Systems; 2.2.2. The Unit Cell and Bravais Lattices; 2.2.3. Reduced Cells; 2.2.4. Space Groups; 2.3. Space Group Notation; 2.3.1. The Triclinic or Anorthic Crystal System; 2.3.2. The Monoclinic Crystal System; 2.3.3. The Orthorhombic Crystal System; 2.3.4. The Tetragonal Crystal System; 2.3.5. The Hexagonal and Trigonal Crystal Systems; 2.3.6. The Cubic Crystal System; 2.3.7. Equivalent Positions; 2.3.8. Special Positions and Site Multiplicity 327 $a2.4. Space Group Theory2.5. Crystallographic Planes and Miller Indices; References; CHAPTER 3. DIFFRACTION THEORY; 3.1. Diffraction of X-rays; 3.2. The Reciprocal Lattice; 3.3. The Ewald Sphere of Reflection; 3.4. Origin of the Diffraction Pattern; 3.4.1. Single Crystal Diffraction; 3.4.2. The Powder Diffraction Pattern; 3.5. The Location of Diffraction Peaks; 3.6. Intensity of Diffraction Peaks; 3.6.1. Electron Scattering; 3.6.2. The Atomic Scattering Factor; 3.6.3. Anomalous Scattering; 3.6.4. Thermal Motion; 3.6.5. Scattering of X-rays by a Crystal: The Structure Factor 327 $a3.7. The Calculated Diffraction Pattern3.7.1. Factors Affecting the Relative Intensity of Bragg Reflections; 3.7.2. The Intensity Equation; 3.8. Calculation of the Powder Diffraction Pattern of KCl; 3.9. Anisotropic Distortions of the Diffraction Pattern; 3.9.1. Preferred Orientation; 3.9.2. Crystallite Size; 3.9.3. Residual Stress and Strain; References; CHAPTER 4. SOURCES FOR THE GENERATION OF X-RADIATION; 4.1. Components of the X-ray Source; 4.2. The Line-Voltage Supply; 4.3. The High-Voltage Generator; 4.3.1. Selection of Operating Conditions; 4.3.2. Source Stability 327 $a4.4. The Sealed X-ray Tube4.4.1. Typical X-ray Tube Configuration; 4.4.2. Specific Loading; 4.4.3. Care of the X-ray Tube; 4.5. Effective Line Width; 4.6. Spectral Contamination; 4.6.1. X-ray Tube Life; 4.7. The Rotating Anode X-ray Tube; References; CHAPTER 5. DETECTORS AND DETECTION ELECTRONICS; 5.1. X-ray Detectors; 5.2. Desired Properties of an X-ray Detector; 5.2.1. Quantum-Counting Efficiency; 5.2.2. Linearity; 5.2.3. Energy Proportionality; 5.2.4. Resolution; 5.3. Types of Detector; 5.3.1. The Gas Proportional Counter; 5.3.2. Position-Sensitive Detectors 327 $a5.3.3. The Scintillation Detector 330 $aWhen bombarded with X-rays, solid materials produce distinct scattering patterns similar to fingerprints. X-ray powder diffraction is a technique used to fingerprint solid samples, which are then identified and cataloged for future use-much the way the FBI keeps fingerprints on file. The current database of some 70,000 material prints has been put to a broad range of uses, from the analysis of moon rocks to testing drugs for purity.Introduction to X-ray Powder Diffractometry fully updates the achievements in the field over the past fifteen years and provides a much-needed explanation o 410 0$aChemical Analysis: A Series of Monographs on Analytical Chemistry and Its Applications 606 $aX-rays$xDiffraction$xTechnique 606 $aX-ray diffractometer 606 $aPowders$xOptical properties$xMeasurement 615 0$aX-rays$xDiffraction$xTechnique. 615 0$aX-ray diffractometer. 615 0$aPowders$xOptical properties$xMeasurement. 676 $a548/.83 700 $aJenkins$b Ron$f1932-$052234 701 $aSnyder$b R. L$g(Robert L.),$f1941-$0951592 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910139078003321 996 $aIntroduction to X-ray powder diffractometry$92151310 997 $aUNINA LEADER 04351nam 22008175 450 001 9910483022803321 005 20251107172621.0 010 $a3-540-30567-X 024 7 $a10.1007/b104761 035 $a(CKB)1000000000212678 035 $a(SSID)ssj0000186205 035 $a(PQKBManifestationID)11185378 035 $a(PQKBTitleCode)TC0000186205 035 $a(PQKBWorkID)10218066 035 $a(PQKB)10827993 035 $a(DE-He213)978-3-540-30567-5 035 $a(MiAaPQ)EBC3068378 035 $a(PPN)123090806 035 $a(EXLCZ)991000000000212678 100 $a20100704d2005 u| 0 101 0 $aeng 135 $aurnn#008mamaa 181 $ctxt 182 $cc 183 $acr 200 10$aJournal on Data Semantics II /$fedited by Stefano Spaccapietra, Elisa Bertino, Sushil Jajodia, Roger B. King, Dennis McLeod, Maria E. Orlowska, Leon Strous 205 $a1st ed. 2005. 210 1$aBerlin, Heidelberg :$cSpringer Berlin Heidelberg :$cImprint: Springer,$d2005. 215 $a1 online resource (XI, 223 p.) 225 1 $aJournal on Data Semantics ;$v3360 300 $aBibliographic Level Mode of Issuance: Monograph 311 08$a3-540-24208-2 320 $aIncludes bibliographical references and index. 327 $aInternational Conference on Ontologies, DataBases, and Applications of Semantics for Large Scale Information Systems (ODBase 2003) -- Incrementally Maintaining Materializations of Ontologies Stored in Logic Databases -- Ontology Translation on the Semantic Web -- Compound Term Composition Algebra: The Semantics -- Dynamic Pattern Mining: An Incremental Data Clustering Approach -- International Conference on Cooperative Information Systems (CoopIS 2003) -- A Knowledge Network Approach for Implementing Active Virtual Marketplaces -- Stream Integration Techniques for Grid Monitoring -- 6th IFIP TC 11 WG 11.5 Working Conference on Integrity and Internal Control in Information Systems (IICIS 2003) -- Information Release Control: A Learning-Based Architecture -- Enforcing Semantics-Aware Security in Multimedia Surveillance. 330 $aThe LNCS Journal on Data Semantics is devoted to the presentation of notable work that, in one way or another, addresses research and development on issues related to data semantics. Based on the highly visible publication platform Lecture Notes in Computer Science, this new journal is widely disseminated and available worldwide. The scope of the journal ranges from theories supporting the formal definition of semantic content to innovative domain-specific applications of semantic knowledge. The journal addresses researchers and advanced practitioners working on the semantic web, interoperability, mobile information services, data warehousing, knowledge representation and reasoning, conceptual database modeling, ontologies, and artificial intelligence. 410 0$aJournal on Data Semantics ;$v3360 606 $aData structures (Computer science) 606 $aInformation theory 606 $aDatabase management 606 $aInformation storage and retrieval systems 606 $aArtificial intelligence 606 $aApplication software 606 $aComputer networks 606 $aData Structures and Information Theory 606 $aDatabase Management 606 $aInformation Storage and Retrieval 606 $aArtificial Intelligence 606 $aComputer and Information Systems Applications 606 $aComputer Communication Networks 615 0$aData structures (Computer science) 615 0$aInformation theory. 615 0$aDatabase management. 615 0$aInformation storage and retrieval systems. 615 0$aArtificial intelligence. 615 0$aApplication software. 615 0$aComputer networks. 615 14$aData Structures and Information Theory. 615 24$aDatabase Management. 615 24$aInformation Storage and Retrieval. 615 24$aArtificial Intelligence. 615 24$aComputer and Information Systems Applications. 615 24$aComputer Communication Networks. 676 $a005.74 701 $aSpaccapietra$b S$01207652 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910483022803321 996 $aJournal on data semantics II$94202096 997 $aUNINA