LEADER 05410nam 2200661Ia 450 001 9910462512903321 005 20200520144314.0 010 $a1-283-60165-6 010 $a9786613914101 010 $a0-12-385014-2 035 $a(CKB)2670000000241864 035 $a(EBL)1023279 035 $a(OCoLC)811732271 035 $a(SSID)ssj0000711267 035 $a(PQKBManifestationID)12254808 035 $a(PQKBTitleCode)TC0000711267 035 $a(PQKBWorkID)10682592 035 $a(PQKB)10787769 035 $a(MiAaPQ)EBC1023279 035 $a(PPN)174628633 035 $a(Au-PeEL)EBL1023279 035 $a(CaPaEBR)ebr10602448 035 $a(CaONFJC)MIL391410 035 $a(EXLCZ)992670000000241864 100 $a20120607h20122013 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 10$aEssentials in modern HPLC separations$b[electronic resource] /$fSerban C. Moldoveanu, Victor David 210 $aAmsterdam $cElsevier$d2012, c2013 215 $a1 online resource (549 p.) 300 $aDescription based upon print version of record. 311 $a0-12-385013-4 320 $aIncludes bibliographical references and index. 327 $aFront Cover; Essentials In Modern HPLC Separations; Copyright; Dedication; Contents; Preface; Chapter1 - Basic Information about HPLC; 1.1.INTRODUCTION TO HPLC; 1.2.MAIN TYPES OF HPLC; 1.3.PRACTICE OF HPLC; 1.4.OVERVIEW OF HPLC INSTRUMENTATION; References; Chapter2 - Parameters that Characterize HPLC Analysis; 2.1.PARAMETERS RELATED TO HPLC SEPARATION; 2.2.EXPERIMENTAL PEAK CHARACTERISTICS IN HPLC; References; Chapter3 - Equilibrium Types in HPLC; 3.1.PARTITION EQUILIBRIUM; 3.2.ADSORPTION EQUILIBRIUM; 3.3.EQUILIBRIA INVOLVING IONS; 3.4.EQUILIBRIUM IN SIZE-EXCLUSION PROCESSES 327 $a3.5.THE INFLUENCE OF PH ON RETENTION EQUILIBRIA3.6.THE INFLUENCE OF TEMPERATURE ON RETENTION EQUILIBRIA; References; Chapter4 - Intermolecular Interactions; 4.1.FORCES BETWEEN IONS AND MOLECULES; 4.2.FORCES BETWEEN MOLECULES AND A SURFACE; References; Chapter5 - Retention Mechanisms in Different HPLC Types; 5.1.RETENTION IN REVERSED-PHASE CHROMATOGRAPHY; 5.2.RETENTION AND SEPARATION PROCESS IN ION-PAIR CHROMATOGRAPY; 5.3.RETENTION AND SEPARATION ON POLAR STATIONARY PHASES; 5.4.RETENTION PROCESS IN ION-EXCHANGE CHROMATOGRAPHY; 5.5.SEPARATION PROCESS IN CHIRAL CHROMATOGRAPHY 327 $a5.6.RETENTION PROCESS IN SIZE-EXCLUSION CHROMATOGRAPHY5.7.RETENTION PROCESS IN OTHER CHROMATOGRAPHY TYPES; References; Chapter6 - Stationary Phases and Their Performance; 6.1.SOLID SUPPORTS FOR STATIONARY PHASES; 6.2.REACTIONS USED FOR OBTAINING ACTIVE GROUPS OF STATIONARY PHASES; 6.3.PROPERTIES OF STATIONARY PHASES AND COLUMNS; 6.4.HYDROPHOBIC STATIONARY PHASES AND COLUMNS; 6.5.POLAR STATIONARY PHASES AND COLUMNS; 6.6.STATIONARY PHASES AND COLUMNS FOR ION-EXCHANGE, ION-MODERATED, AND LIGAND-EXCHANGE CHROMATOGRAPHY; 6.7.STATIONARY PHASES AND COLUMNS FOR CHIRAL CHROMATOGRAPHY 327 $a6.8.STATIONARY PHASES AND COLUMNS FOR SIZE-EXCLUSION CHROMATOGRAPHY6.9.STATIONARY PHASES AND COLUMNS IN IMMUNOAFFINITY CHROMATOGRAPHY; References; Chapter7 - Mobile Phases and Their Properties; 7.1.CHARACTERIZATION OF LIQUIDS AS SOLVENTS; 7.2.ADDITIONAL PROPERTIES OF LIQUIDS AFFECTING SEPARATION; 7.3.PROPERTIES OF THE MOBILE PHASE OF IMPORTANCE IN HPLC, NOT RELATED TO SEPARATION; 7.4.BUFFERS AND OTHER ADDITIVES IN HPLC; 7.5.GRADIENT ELUTION; 7.6.MOBILE PHASE IN REVERSED-PHASE CHROMATOGRAPHY; 7.7.MOBILE PHASE IN ION-PAIR LIQUID CHROMATOGRAPHY; 7.8.MOBILE PHASE IN HILIC AND NPC 327 $a7.9.MOBILE PHASE IN ION-EXCHANGE AND ION-MODERATED CHROMATOGRAPHY7.10.MOBILE PHASE IN CHIRAL CHROMATOGRAPHY; 7.11.MOBILE PHASE FOR SIZE-EXCLUSION SEPARATIONS; References; Chapter8 - Solutes in HPLC; 8.1.NATURE OF THE SOLUTE; 8.2.PARAMETERS FOR SOLUTE CHARACTERIZATION IN THE SEPARATION PROCESS; 8.3.OTHER PARAMETERS FOR SOLUTE CHARACTERIZATION; References; Chapter9 - HPLC Analysis; 9.1.CHEMICAL NATURE OF THE ANALYTES AND THE CHOICE OF HPLC TYPE; 9.2.THE QUANTITY OF SAMPLE INJECTED FOR HPLC ANALYSIS; 9.3.ESTIMATION OF PARAMETERS DESCRIBING THE SEPARATION 327 $a9.4.STEPS IN DEVELOPMENT AND IMPLEMENTATION OF AN HPLC SEPARATION 330 $a Essentials in Modern HPLC Separations discusses the role of separation in high performance liquid chromatography (HPLC). This up-to-date reference systematically covers new developments in types and characteristics of stationary phases, mobile phases, and other factors of this technique that influence separation of compounds being analyzed. The volume also considers the selection process for stationary and mobile phases in relation to the molecules being separated and examined, as well as their matrices. The book includes a section on the contemporary applications of HPLC, p 606 $aSeparation (Technology) 606 $aHigh performance liquid chromatography 608 $aElectronic books. 615 0$aSeparation (Technology) 615 0$aHigh performance liquid chromatography. 676 $a660/.2842 700 $aMoldoveanu$b S?erban$0939186 701 $aDavid$b Victor$f1955-$0995959 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910462512903321 996 $aEssentials in modern HPLC separations$92282196 997 $aUNINA