LEADER 05281nam 2200661 a 450 001 9910462088903321 005 20200520144314.0 010 $a1-280-77001-5 010 $a9786613680785 010 $a0-12-385541-1 035 $a(CKB)2670000000193862 035 $a(EBL)943706 035 $a(OCoLC)796466990 035 $a(SSID)ssj0000676098 035 $a(PQKBManifestationID)12229126 035 $a(PQKBTitleCode)TC0000676098 035 $a(PQKBWorkID)10677010 035 $a(PQKB)10833114 035 $a(MiAaPQ)EBC943706 035 $a(PPN)170601595 035 $a(Au-PeEL)EBL943706 035 $a(CaPaEBR)ebr10571152 035 $a(CaONFJC)MIL368078 035 $a(EXLCZ)992670000000193862 100 $a20120413d2012 uy 0 101 0 $aeng 135 $aurcn||||||||| 181 $ctxt 182 $cc 183 $acr 200 10$aGas chromatography$b[electronic resource] /$fColin F. Poole 205 $a1st ed. 210 $aAmsterdam ;$aBoston $cElsevier$d2012 215 $a1 online resource (753 p.) 300 $aDescription based upon print version of record. 311 $a0-12-385540-3 320 $aIncludes bibliographical references and index. 327 $aFront Cover; Gas Chromatography; Copyright; Contents; Contributors; Chapter 1 - Milestones in the Development of Gas Chromatography; 1.1.INTRODUCTION; 1.2.THE INVENTION OF GAS CHROMATOGRAPHY; 1.3.EARLY INSTRUMENTATION; 1.4.EARLY COLUMN DEVELOPMENTS; 1.5.INTERFACING GLASS CAPILLARY COLUMNS TO INJECTORS AND DETECTORS; 1.6.THE HINDELANG CONFERENCES AND THE FUSED-SILICA COLUMN; 1.7.INCREASING SOPHISTICATION OF INSTRUMENTATION; 1.8.DECLINE IN THE EXPERTISE OF THE AVERAGE GAS CHROMATOGRAPHER; References; Chapter 2 - Theory of Gas Chromatography; 2.1.INTRODUCTION 327 $a2.2.NOMENCLATURE AND OTHER CONVENTIONS 2.3.GENERAL DEFINITIONS; 2.4.SOLUTE-COLUMN INTERACTION; 2.5.PROPERTIES OF AN IDEAL GAS; 2.6.FLOW OF IDEAL GAS IN OPEN CIRCULAR TUBES; 2.7.MIGRATION AND ELUTION PARAMETERS OF THE SOLUTES; 2.8.PEAK SPACING AND REVERSAL OF PEAK ORDER; 2.9.PEAK WIDTH; 2.10.OPTIMIZATION; References; Chapter 3 - Column Technology: Open Tubular Columns; 3.1.INTRODUCTION; 3.2.OVERVIEW OF THE FUSED SILICA DRAWING PROCESS; 3.3.THE PREFORM - RAW MATERIAL; 3.4.SURFACE CHEMISTRY; 3.5.DRAWING OF THE CAPILLARY FROM THE PREFORM; 3.6.PROTECTIVE COATING; 3.7.ALTERNATIVE PROTECTIVE COATINGS 327 $a3.8. CLEAN ROOM ENVIRONMENT 3.9.QUALITY MONITORING; 3.10.OBSERVATIONS ON HANDLING OF FUSED-SILICA CAPILLARY TUBING; 3.11.COLUMN TECHNOLOGY - COATING THE STATIONARY PHASE; 3.12.STATIONARY PHASES; 3.13.COATING TECHNIQUES; 3.14.COLUMN TECHNOLOGY - QUALITY EVALUATION; 3.15.COLUMN TECHNOLOGY - SUMMARY; References; Chapter 4- Packed Columns for Gas-Liquid and Gas-Solid Chromatography; 4.1.INTRODUCTION; 4.2.GAS-LIQUID CHROMATOGRAPHY; 4.3.GAS-SOLID CHROMATOGRAPHY; References; Chapter 5 - Gas-Solid Chromatography (PLOT Columns); 5.1.ALUMINA ADSORBENTS; 5.2.MOLECULAR SIEVES; 5.3.POROUS POLYMERS 327 $a5.4.CARBON ADSORBENTS 5.5.OTHER ADSORBENTS; References; Chapter 6- Classification and Selection of Open-Tubular Columns for Analytical Separations; 6.1.INTRODUCTION; 6.2.STATIONARY-PHASE CLASSIFICATION; 6.3.POROUS-LAYER OPEN-TUBULAR COLUMNS; 6.4.TEMPERATURE-PROGRAMMED SEPARATIONS; 6.5.STATIONARY-PHASE SELECTIVITY TUNING; References; Chapter 7 - Multidimensional and Comprehensive Gas Chromatography; 7.1.INTRODUCTION; 7.2.A GRAPHICAL REPRESENTATION OF 2D GC SEPARATIONS; 7.3 .BACK FLUSHING 2D GC; 7.4.HEART CUTTING 2D GC; 7.5.COMPREHENSIVE 2D GC; 7.6.CONCLUSIONS; References 327 $aChapter 8 - Sample Introduction Methods 8.1.INTRODUCTION; 8.2.CHOOSING A SAMPLE INTRODUCTION SYSTEM; 8.3.SUPPORTING DEVICES; 8.4.THE COLD ON-COLUMN INJECTOR; 8.5.THE FLASH VAPORIZATION INJECTOR; 8.6.THE SPLIT/SPLITLESS INJECTOR; 8.7.THE PROGRAMMABLE TEMPERATURE VAPORIZING (PTV) INJECTOR; 8.8.THE GAS SAMPLING VALVE; 8.9.THE LIQUID SAMPLING VALVE; References; Chapter 9 - Head space-Gas Chromatography; 9.1.INTRODUCTION AND HISTORY; 9.2.FUNDAMENTALS OF HEAD SPACE EXTRACTION; 9.3.INSTRUMENTATION AND PRACTICE; 9.4.METHOD DEVELOPMENT CONSIDERATIONS; 9.5.CONCLUSIONS; References 327 $aChapter 10- Thermal Desorption for Gas Chromatography 330 $aThis title provides comprehensive coverage of modern gas chromatography including theory, instrumentation, columns, and applications addressing the needs of advanced students and professional scientists in industry and government laboratories. Chapters are written by recognized experts on each topic. Each chapter offers a complete picture with respect to its topic so researchers can move straight to the information they need without reading through a lot of background information.Individual chapters written by recognized experts The big picture of gas chromatography 606 $aGas chromatography 606 $aChromatographic analysis 608 $aElectronic books. 615 0$aGas chromatography. 615 0$aChromatographic analysis. 676 $a543/.85 700 $aPoole$b C. F$0990553 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910462088903321 996 $aGas chromatography$92270443 997 $aUNINA