LEADER 01862nam 22005774a 450 001 9910454606003321 005 20200520144314.0 035 $a(CKB)1000000000522959 035 $a(SSID)ssj0000281693 035 $a(PQKBManifestationID)11223579 035 $a(PQKBTitleCode)TC0000281693 035 $a(PQKBWorkID)10307864 035 $a(PQKB)11154526 035 $a(MiAaPQ)EBC3306560 035 $a(Au-PeEL)EBL3306560 035 $a(CaPaEBR)ebr10112571 035 $a(OCoLC)560313270 035 $a(EXLCZ)991000000000522959 100 $a20030319d2002 uy 0 101 0 $aeng 135 $aurcn||||||||| 181 $ctxt 182 $cc 183 $acr 200 00$aManaging IBM e-server Cluster 1600$b[electronic resource] $epower recipes for PSSP 3.4 /$f[Christian A. Schmidt ... [et al.]] 205 $a1st ed. 210 $aPoughkeepsie, NY $cIBM International Technical Support Organization$d2002 215 $axviii, 278 p. $cill 225 1 $aRedbooks 300 $a"SG24-6603-00." 300 $a"June 2002." 311 $a0-7384-2341-6 320 $aIncludes bibliographical references (p. 267-268) and index. 410 0$aIBM redbooks. 606 $aParallel computers 606 $aIBM RISC System/6000 computers 606 $aFile organization (Computer science) 608 $aElectronic books. 615 0$aParallel computers. 615 0$aIBM RISC System/6000 computers. 615 0$aFile organization (Computer science) 676 $a004/.35 701 $aSchmidt$b Christian A$0884839 712 02$aInternational Business Machines Corporation.$bInternational Technical Support Organization. 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910454606003321 996 $aManaging IBM e-server Cluster 1600$91975794 997 $aUNINA LEADER 04755nam 2200649 450 001 9910144406903321 005 20190715152939.0 010 $a1-282-02171-0 010 $a9786612021718 010 $a3-527-62521-6 010 $a3-527-62522-4 035 $a(CKB)1000000000577977 035 $a(EBL)482075 035 $a(OCoLC)609855520 035 $a(SSID)ssj0000298178 035 $a(PQKBManifestationID)11223412 035 $a(PQKBTitleCode)TC0000298178 035 $a(PQKBWorkID)10361737 035 $a(PQKB)10431107 035 $a(MiAaPQ)EBC482075 035 $a(PPN)15233999X 035 $a(EXLCZ)991000000000577977 100 $a20160815h20092009 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 10$aHandbook of GC/MS $efundamentals and applications /$fHans-Joachim Hu?bschmann 205 $a2nd ed. 210 1$aWeinheim, [Germany] :$cWiley-VCH Verlag GmbH & Co. KGaA,$d2009. 210 4$d©2009 215 $a1 online resource (739 p.) 300 $aDescription based upon print version of record. 311 $a3-527-31427-X 320 $aIncludes bibliographical references at the end of each chapters and index. 327 $aHandbook of GC/MS; Foreword; Preface to the Second Edition; Preface to the First Edition; Contents; 1 Introduction; 2 Fundamentals; 2.1 Sample Preparation; 2.1.1 Solid Phase Extraction; 2.1.1.1 Solid Phase Microextraction; 2.1.2 Supercritical Fluid Extraction; 2.1.3 Pressurized Fluid Extraction; 2.1.4 Online Liquid Chromatography Clean-up; 2.1.5 Headspace Techniques; 2.1.5.1 Static Headspace Technique; 2.1.5.2 Dynamic Headspace Technique (Purge and Trap); 2.1.5.3 Headspace versus Purge and Trap; 2.1.6 Adsorptive Enrichment and Thermodesorption; 2.1.6.1 Sample Collection; 2.1.6.2 Calibration 327 $a2.2.3.4 Cold Injection Systems2.2.3.5 Injection Volumes; 2.2.3.6 On-column Injection; 2.2.3.7 Cryofocusing; 2.2.4 Capillary Columns; 2.2.4.1 Sample Capacity; 2.2.4.2 Internal Diameter; 2.2.4.3 Film Thickness; 2.2.4.4 Column Length; 2.2.4.5 Adjusting the Carrier Gas Flow; 2.2.4.6 Properties of Stationary Phases; 2.2.5 Chromatography Parameters; 2.2.5.1 The Chromatogram and its Meaning; 2.2.5.2 Capacity Factor k ?; 2.2.5.3 Chromatographic Resolution; 2.2.5.4 Factors Affecting the Resolution; 2.2.5.5 Maximum Sample Capacity; 2.2.5.6 Peak Symmetry; 2.2.5.7 Optimisation of Flow 327 $a2.2.6 Classical Detectors for GC/MS Systems2.2.6.1 FID; 2.2.6.2 NPD; 2.2.6.3 ECD; 2.2.6.4 PID; 2.2.6.5 ELCD; 2.2.6.6 FPD; 2.2.6.7 PDD; 2.2.6.8 Connection of Classical Detectors Parallel to the Mass Spectrometer; 2.3 Mass Spectrometry; 2.3.1 Resolving Power and Resolution in Mass Spectrometry; 2.3.1.1 High Resolution; 2.3.1.2 Unit Mass Resolution; 2.3.1.3 High and Low Resolution in the Case of Dioxin Analysis; 2.3.2 Time-of-Flight Analyser; 2.3.3 Isotope Ratio Monitoring GC/MS; 2.3.4 Ionisation Procedures; 2.3.4.1 Electron Impact Ionisation; 2.3.4.2 Chemical Ionisation 327 $a2.3.5 Measuring Techniques in GC/MS2.3.5.1 Detection of the Complete Spectrum (Full Scan); 2.3.5.2 Recording Individual Masses (SIM/MID); 2.3.5.3 High Resolution Accurate Mass MID Data Acquisition; 2.3.6 MS/MS -Tandem Mass Spectrometry; 2.3.7 Mass Calibration; 2.4 Special Aspects of GC/MS Coupling; 2.4.1 Vacuum Systems; 2.4.2 GC/MS Interface Solutions; 2.4.2.1 Open Split Coupling; 2.4.2.2 Direct Coupling; 2.4.2.3 Separator Techniques; References for Chapter 2; 3 Evaluation of GC/MS Analyses; 3.1 Display of Chromatograms; 3.1.1 Total Ion Current Chromatograms; 3.1.2 Mass Chromatograms 327 $a3.2 Substance Identification 330 $aThis is the first comprehensive reference work for GC/MS now in its second edition.It offers broad coverage, from sample preparation to the evaluation of MS-Data, including library searches. Fundamentals, techniques, and applications are described.A large part of the book is devoted to numerous examples for GC/MS-applications in environmental, food, pharmaceutical and clinical analysis. 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These fields of specific attention are high-Mn TWIP steels, high-Cr heat resistant steels, aluminum alloys, ultrafine grained materials including those developed by severe plastic deformation, and high-entropy alloys. The major portion of the collected papers is focused on the mechanisms of microstructure evolution and the mechanical properties of metallic materials subjected to various thermo-mechanical, deformation or heat treatments. Another large portion of the studies is aimed on the elaboration of alloying design of advanced steels and alloys. 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