LEADER 04192nam 2200709 450 001 9910818578103321 005 20200520144314.0 010 $a0-19-046388-0 010 $a0-19-756337-6 035 $a(CKB)3710000000420275 035 $a(EBL)3564608 035 $a(SSID)ssj0001498482 035 $a(PQKBManifestationID)12608319 035 $a(PQKBTitleCode)TC0001498482 035 $a(PQKBWorkID)11502285 035 $a(PQKB)11183100 035 $a(StDuBDS)EDZ0002341508 035 $a(Au-PeEL)EBL3564608 035 $a(CaPaEBR)ebr11061376 035 $a(CaONFJC)MIL795807 035 $a(OCoLC)932320843 035 $a(MiAaPQ)EBC3564608 035 $a(EXLCZ)993710000000420275 100 $a20150608h20152015 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 14$aThe assignment of the absolute configuration by NMR using chiral derivatizing agents $ea practical guide /$fJ.M. Seco, Emilio Quin?oa?, and R. Riguera 210 1$aNew York, New York :$cOxford University Press,$d2015. 210 4$d©2015 215 $a1 online resource (265 p.) 225 1 $aOxford scholarship online 300 $aPreviously issued in print: 2015. 311 $a0-19-999681-4 311 $a0-19-999680-6 320 $aIncludes bibliographical references and index. 327 $a""Cover""; ""The Assignment of the Absolute Configuration by NMR Using Chiral Derivatizing Agents""; ""Copyright""; ""Contents""; ""Preface""; ""Introduction""; ""1 The Theoretical Basis for Assignment by NMR""; ""1.1. Distinguishing Enantiomers by NMR: The Use of CDAs""; ""1.2. Structural Characteristics of the Auxiliaries and the Substrates""; ""1.3. Importance of the Conformation""; ""1.4. Importance of the Aromatic Shielding Effect""; ""1.5. Use of 13C NMR for Assignment""; ""1.6. Simplified Approaches to Assignment by NMR"" 327 $a""2.1. Instrumentation, Concentration, Solvent, and Temperature of the NMR Experiment""""2.2. Source and Preparation of the CDAs""; ""2.3. Preparation of the CDA Esters, Thioesters, and Amides""; ""2.3.1. Derivatization of Alcohols, Thiols, and Cyanohydrins Using the CDA Acid""; ""2.3.2. Derivatization of Amines Using the CDA Acid""; ""2.3.3. Preparation of the CDA Acid Chlorides""; ""2.3.4. Derivatization of Alcohols, Thiols, and Cyanohydrins Using the CDA Acid Chloride""; ""2.4. Resin-Bound CDA Derivatives (Mix-and-Shake Method)""; ""2.4.1. Preparation of Resin-Bound CDA Derivatives"" 327 $a""2.4.2. Preparation of Acid Chloride Resins""""2.4.3. Preparation of CDA-Resins""; ""2.4.4. Determination of the Loading of the CDA-Resins""; ""2.4.5. In-Tube Derivatization of Amines""; ""2.4.6. In-Tube Derivatization of Primary and Secondary Alcohols, Cyanohydrins, and Secondary Thiols""; ""2.4.7. In-Tube Derivatization of Amino Alcohols""; ""2.4.8. In-Tube Derivatization of Diols and Triols""; ""2.4.9. In-Tube Derivatization for Single-Derivatization Procedures""; ""3 Assignment of the Absolute Configuration of Monofunctional Compounds by Double Derivatization"" 330 8 $aThis guide offers a concise explanation of the theoretical aspects necessary for understanding the methodology underpinning cutting-edge research in the field of nuclear magnetic resonance (NMR) spectroscopy. 410 0$aOxford scholarship online. 606 $aNuclear magnetic resonance spectroscopy 606 $aSpectrum analysis 606 $aNuclear magnetic resonance spectroscopy$vProblems, exercises, etc 606 $aSpectrum analysis$vProblems, exercises, etc 615 0$aNuclear magnetic resonance spectroscopy. 615 0$aSpectrum analysis. 615 0$aNuclear magnetic resonance spectroscopy 615 0$aSpectrum analysis 676 $a543/.66 700 $aSeco$b J. M$g(Jose? Manuel),$01642372 702 $aQuin?oa?$b E$g(Emilio), 702 $aRiguera$b R$g(Ricardo), 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910818578103321 996 $aThe assignment of the absolute configuration by NMR using chiral derivatizing agents$93987018 997 $aUNINA LEADER 04777nam 22008655 450 001 9910300381903321 005 20200630180518.0 010 $a3-319-01192-8 024 7 $a10.1007/978-3-319-01192-9 035 $a(CKB)2670000000428545 035 $a(EBL)1466759 035 $a(SSID)ssj0001010774 035 $a(PQKBManifestationID)11551946 035 $a(PQKBTitleCode)TC0001010774 035 $a(PQKBWorkID)11000943 035 $a(PQKB)11309525 035 $a(MiAaPQ)EBC1466759 035 $a(DE-He213)978-3-319-01192-9 035 $a(PPN)172423651 035 $a(EXLCZ)992670000000428545 100 $a20130912d2014 u| 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 10$aCharge Dynamics in 122 Iron-Based Superconductors /$fby Aliaksei Charnukha 205 $a1st ed. 2014. 210 1$aCham :$cSpringer International Publishing :$cImprint: Springer,$d2014. 215 $a1 online resource (139 p.) 225 1 $aSpringer Theses, Recognizing Outstanding Ph.D. Research,$x2190-5053 300 $aDescription based upon print version of record. 311 $a3-319-01191-X 320 $aIncludes bibliographical references. 327 $aIntroduction -- Iron-based superconductors -- Experimental and theoretical methods -- Results and discussion -- Summary. 330 $aThis thesis combines highly accurate optical spectroscopy data on the recently discovered iron-based high-temperature superconductors with an incisive theoretical analysis. Three outstanding results are reported: (1) The superconductivity-induced modification of the far-infrared conductivity of an iron arsenide with minimal chemical disorder is quantitatively described by means of a strong-coupling theory for spin fluctuation mediated Cooper pairing. The formalism developed in this thesis also describes prior spectroscopic data on more disordered compounds. (2) The same materials exhibit a sharp superconductivity-induced anomaly for photon energies around 2.5 eV, two orders of magnitude larger than the superconducting energy gap. The author provides a qualitative interpretation of this unprecedented observation, which is based on the multiband nature of the superconducting state. (3) The thesis also develops a comprehensive description of a superconducting, yet optically transparent iron chalcogenide compound. The author shows that this highly unusual behavior can be explained as a result of the nanoscopic coexistence of insulating and superconducting phases, and he uses a combination of two complementary experimental methods - scanning near-field optical microscopy and low-energy muon spin rotation - to directly image the phase coexistence and quantitatively determine the phase composition. These data have important implications for the interpretation of data from other experimental probes. 410 0$aSpringer Theses, Recognizing Outstanding Ph.D. Research,$x2190-5053 606 $aSuperconductivity 606 $aSuperconductors 606 $aSpectroscopy 606 $aMicroscopy 606 $aOptical materials 606 $aElectronic materials 606 $aNanoscale science 606 $aNanoscience 606 $aNanostructures 606 $aNanotechnology 606 $aStrongly Correlated Systems, Superconductivity$3https://scigraph.springernature.com/ontologies/product-market-codes/P25064 606 $aSpectroscopy and Microscopy$3https://scigraph.springernature.com/ontologies/product-market-codes/P31090 606 $aOptical and Electronic Materials$3https://scigraph.springernature.com/ontologies/product-market-codes/Z12000 606 $aNanoscale Science and Technology$3https://scigraph.springernature.com/ontologies/product-market-codes/P25140 606 $aNanotechnology$3https://scigraph.springernature.com/ontologies/product-market-codes/Z14000 615 0$aSuperconductivity. 615 0$aSuperconductors. 615 0$aSpectroscopy. 615 0$aMicroscopy. 615 0$aOptical materials. 615 0$aElectronic materials. 615 0$aNanoscale science. 615 0$aNanoscience. 615 0$aNanostructures. 615 0$aNanotechnology. 615 14$aStrongly Correlated Systems, Superconductivity. 615 24$aSpectroscopy and Microscopy. 615 24$aOptical and Electronic Materials. 615 24$aNanoscale Science and Technology. 615 24$aNanotechnology. 676 $a530.41 676 $a537.6 676 $a537.6233 700 $aCharnukha$b Aliaksei$4aut$4http://id.loc.gov/vocabulary/relators/aut$0791352 906 $aBOOK 912 $a9910300381903321 996 $aCharge Dynamics in 122 Iron-Based Superconductors$91768732 997 $aUNINA LEADER 01571nam0 2200373 i 450 001 RMG0016712 005 20251003044335.0 010 $a8821707776 020 $aIT$b95-9112 100 $a19990521d1995 ||||0itac50 ba 101 | $aita 102 $ait 181 1$6z01$ai $bxxxe 182 1$6z01$an 200 1 $aBilancio, societą e contratti$fdi Francesco Mazzarelli 210 $a[Milanofiori, Assago]$cIPSOA$d1995 215 $a247 p.$d23 cm. 225 | $aGuide fiscali$v3(1995) 410 0$1001BVE0064723$12001 $aGuide fiscali$v3(1995) 606 $aAziende$xRedditi$xTributi$xGuide pratiche$2FIR$3CFIC036043$9I 606 $aBilancio fiscale$xGuide pratiche$2FIR$3CFIC036044$9I 676 $a343.4505268$9IMPOSTA SUL REDDITO DELLE IMPRESE. ITALIA$v20 696 $aImprese$aReddito 699 $aAziende$yImprese 699 $aRedditi$zReddito 700 1$aMazzarelli$b, Francesco$3CFIV001071$4070$035845 801 3$aIT$bIT-000000$c19990521 850 $aIT-BN0095 901 $bNAP 01$cPOZZO LIB.$nVi sono collocati fondi di economia, periodici di ingegneria e scienze, periodici di economia e statistica e altri fondi comprendenti documenti di economia pervenuti in dono. 912 $aRMG0016712 950 0$aBiblioteca Centralizzata di Ateneo$c1 v.$d 01POZZO LIB.ECON MON 9507$e 0101 0000104755E VMA 1 v. (precedente collocazione: GUERRAZZI B 412)$fB $h20071025$i20071025 977 $a 01 996 $aBilancio, Societą e Contratti$9192062 997 $aUNISANNIO