LEADER 05166nam 2200709Ia 450 001 9910145957403321 005 20170814180600.0 010 $a1-118-99599-6 010 $a1-282-11303-8 010 $a9786612113031 010 $a0-470-42383-8 010 $a0-470-42377-3 035 $a(CKB)1000000000719482 035 $a(EBL)427633 035 $a(OCoLC)476269592 035 $a(SSID)ssj0000258416 035 $a(PQKBManifestationID)11939503 035 $a(PQKBTitleCode)TC0000258416 035 $a(PQKBWorkID)10256519 035 $a(PQKB)10154744 035 $a(MiAaPQ)EBC427633 035 $a(PPN)13987545X 035 $a(EXLCZ)991000000000719482 100 $a20080530d2009 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 00$aThermal analysis of polymers$b[electronic resource] $efundamentals and applications /$fedited by Joseph D. Menczel, R. Bruce Prime 210 $aHoboken, NJ $cJohn Wiley$dc2009 215 $a1 online resource (700 p.) 300 $aDescription based upon print version of record. 311 $a0-471-76917-7 320 $aIncludes bibliographical references and index. 327 $aTHERMAL ANALYSIS OF POLYMERS; CONTENTS; PREFACE; 1 INTRODUCTION; 2 DIFFERENTIAL SCANNING CALORIMETRY (DSC); 2.1. Introduction; 2.2. Elements of Thermodynamics in DSC; 2.3. The Basics of Differential Scanning Calorimetry; 2.4. Purity Determination of Low-Molecular-Mass Compounds by DSC; 2.5. Calibration of Differential Scanning Calorimeters; 2.6. Measurement of Heat Capacity; 2.7. Phase Transitions in Amorphous and Crystalline Polymers; 2.8. Fibers; 2.9. Films; 2.10. Thermosets; 2.11. Differential Photocalorimetry (DPC); 2.12. Fast-Scan DSC 327 $a2.13. Modulated Temperature Differential Scanning Calorimetry (MTDSC)2.14. How to Perform DSC Measurements; 2.15. Instrumentation; Appendix; Abbreviations; References; 3 THERMOGRAVIMETRIC ANALYSIS (TGA); 3.1. Introduction; 3.2. Background Principles and Measurement Modes; 3.3. Calibration and Reference Materials; 3.4. Measurements and Analyses; 3.5. Kinetics; 3.6. Selected Applications; 3.7. Instrumentation; Appendix; Abbreviations; References; 4 THERMOMECHANICAL ANALYSIS (TMA) AND THERMODILATOMETRY (TD); 4.1. Introduction; 4.2. Principles and Theory; 4.3. Instrumental; 4.4. Calibration 327 $a4.5. How to Perform a TMA Experiment4.6. Key Applications; 4.7. Selected Industrial Applications (with Details of Experimental Conditions); Appendix; Abbreviations; References; 5 DYNAMIC MECHANICAL ANALYSIS (DMA); 5.1. Introduction; 5.2. Characterization of Viscoelastic Behavior; 5.3. The Relationship between Time, Temperature, and Frequency; 5.4. Applications of Dynamic Mechanical Analysis; 5.5. Examples of DMA Characterization for Thermoplastics; 5.6. Characteristics of Fibers and Thin Films; 5.7. DMA Characterization of Crosslinked Polymers 327 $a5.8. Practical Aspects of Conducting DMA Experiments5.9. Commercial DMA Instrumentation; Appendix; Abbreviations; References; 6 DIELECTRIC ANALYSIS (DEA); 6.1. Introduction; 6.2. Theory and Background of Dielectric Analysis; 6.3. Dielectric Techniques; 6.4. Performing Dielectric Experiments; 6.5. Typical Measurements on Poly(Methyl Methacrylate) (PMMA); 6.6. Dielectric Analysis of Thermoplastics; 6.7. Dielectric Analysis of Thermosets; 6.8. Instrumentation; Appendix; Abbreviations; References; 7 MICRO- AND NANOSCALE LOCAL THERMAL ANALYSIS; 7.1. Introduction; 7.2. The Atomic Force Microscope 327 $a7.3. Scanning Thermal Microscopy7.4. Thermal Probe Design and Spatial Resolution; 7.5. Measuring Thermal Conductivity and Thermal Force-Distance Curves; 7.6. Local Thermal Analysis; 7.7. Performing a Micro/Nanoscale Thermal Analysis Experiment; 7.8. Examples of Micro/Nanoscale Thermal Analysis Applications; 7.9. Overview of Local Thermal Analysis; Abbreviations; References; INDEX 330 $aPresents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background.Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applicationsTopics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Ana 606 $aPolymers$xAnalysis 606 $aThermal analysis 615 0$aPolymers$xAnalysis. 615 0$aThermal analysis. 676 $a543 676 $a547 676 $a547.7 676 $a547/.7046 686 $aVE 8000$2rvk 686 $aVG 7100$2rvk 686 $aVN 5520$2rvk 686 $aZM 5100$2rvk 701 $aMenczel$b Joseph D$0855569 701 $aPrime$b R. Bruce$0855570 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910145957403321 996 $aThermal analysis of polymers$91910011 997 $aUNINA