LEADER 05398nam 2200709Ia 450 001 9910144314803321 005 20200520144314.0 010 $a9786612305511 010 $a9781282305519 010 $a1282305514 010 $a9780470132449 010 $a0470132442 010 $a9780470132791 010 $a0470132795 035 $a(CKB)1000000000376275 035 $a(EBL)470039 035 $a(OCoLC)808668858 035 $a(SSID)ssj0000299779 035 $a(PQKBManifestationID)11223535 035 $a(PQKBTitleCode)TC0000299779 035 $a(PQKBWorkID)10242753 035 $a(PQKB)10046236 035 $a(MiAaPQ)EBC470039 035 $a(PPN)24312080X 035 $a(Perlego)2762150 035 $a(EXLCZ)991000000000376275 100 $a20750907d1971 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 00$aInorganic syntheses$hVolume XIII /$feditor-in-chief, F.A. Cotton 210 $aNew York $cMcGraw Hill$d1971 215 $a1 online resource (288 p.) 225 0 $aInorganic syntheses ;$v13 300 $aDescription based upon print version of record. 311 08$a9780470131725 311 08$a0470131721 320 $aIncludes bibliographical references and and index. 327 $aINORGANIC SYNTHESES; CONTENTS; Preface; Notice to Contributors; Chapter One COMPOUNDS OF THE NONTRANSITION ELEMENTS; 1. Perbromic Acid and Potassium Prebromate; 2. a-Sulfanuric Chloride-Cyclic Trimer; A. (Trichlorophosphoranylidene)sulfamoyl Chloride; B. a-Sulfanuric Chloride-Cyclic Trimer; 3. Arsine and Arsine-d3; 4. Ammonium Cyanate; 5. Phosphorus(III) Isocyanate; 6. Phosphoramidic Acid and Its Salts; A. Ammonium Hydrogen Phosphoramidate; B. Phosphoramidic Acid; C. Potassium Hydrogen Phosphoramidate; 7. Diphenyl(trimethylsilyl)phosphine and DimethyI(trimethylsilyl)phosphine 327 $aA. Diphenyl(trimethylsilyl)phosphineB. Dimethyl(trimethylsilyl)phosphine; 8. Exchange Reactions for the Syntheses of Phenylboron Chlorides and Tetrafluoromethylphosphorane; A. Dichloro(phenyl)borane, C6H5BCl2; B. Chlorodiphenylborane, (C6H5)2BCl; C. Tetrafluoromethylphosphorane, CH3PF4; 9. 2,4,6-Trichloroborazine; 10. 2,4,6-Trichloro-1,3,5-trimethylboraeine; Chapter Two ORGANOMETALLIC COMPOUNDS; 11. Cyclic-diolefin Complexes of Platinum and Palladium; A. Platinum Compounds; B. Palladium Compounds; 12. Cationic Diene Complexes of Palladiuni(II) and Platinum(II); A. Complexes of Type (I) 327 $aB. Complexes of Type (II)C. Complexes of Type (III); D. Complexes of Type (IV); 13. Trichloro-, Trimethyl-, and Trifluorosilylcobalt Tetracarbonyl; A. Tetracarbonyl(trichlorosilyl)cobalt; B. Tetracarbonyl(trimethylsilyl)cobalt; C. Tetracarbonyl(trifluorosilyl)cobalt; 14. Isoleptic Allyl Derivatives of Various Metals; A. Allyl Magnesium Chloride; B. Tetraallylstannane; C. Tetraallylsilane and Tetraallylgermane; D. Tri-h3-allylchromium; E. Di-h3-allylnickel; Chapter Three COMPOUNDS CONTAINING METAL-TO- METAL BONDS; 15. Rhenium and Molybdenum Compounds Containing Quadruple Bonds 327 $aA. Octahalodirhenate(III) AnionsB. Tetrakis(carboxylato)dihalodirhenium(III) Compounds; C. Tetrakis(carboxylato)dimolyndenum (II) Compounds; 16. Tetrakis(acetato)dirhodium(II) and Similar Carboxylato Compounds; 17. Dodecacarbonyltriruthenium and -triosmium; A. Dodecacarbonyltriruthenium; B. Dodecacarbonyltriosmiuin; 18. Dodecacarbonyltetrairidium; 19. Disodium Hexaalkoxy-octa-u3-chloro-hexamolybdates; A. Disodium Octa-u3-chloro-hexaniethoxyhexamolybdate(II); B. Disodium Octa-u3-chloro-hexaethoxyhexamolybdate(II); C. Disodium Octa-u3-chloro-hexamolybdate(II) 327 $aChapter Four PHOSPHINE AND PHOSPHITE COMPLEXES OF LOW-VALENT METALS20. Triaryl Phosphite Complexes of Cobalt, Nickel. Platinum. and Rhodium; A. Hydridotetrakis(triphenyl phosphite)cobalt(I); B. Tetrakis(triphenyl phosphite)nickel(0); C. Tetrakis(triphenyl phosphite)platinum(0); D. Hydridotetrakis(triphenyl phosphite)rhodium(I); 21. Tetrakis(triethyl phosphite)nickel(0), Palladium(0), and Platinum(0) Complexes; A. Tetrakis(triethyl phosphite)nickel(0); B. Tetrakis(triethyl phosphite)palladium(0); C. Tetrakis(triethyl phosphite)platinum(0); D. Tetrakis(triphenyl phosphite)nickel(0) 327 $a22. Low-valent Metal Complexes of Diethyl Phenylphosphonite 330 $aThe volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested. 410 0$aInorganic Syntheses 606 $aInorganic compounds$xSynthesis 606 $aChemistry, Inorganic 615 0$aInorganic compounds$xSynthesis. 615 0$aChemistry, Inorganic. 676 $a541.39 676 $a541/.39 701 $aCotton$b F. Albert$g(Frank Albert),$f1930-2007.$0528 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910144314803321 996 $aInorganic syntheses$91954837 997 $aUNINA