LEADER 05224nam 2200661Ia 450 001 9910144313703321 005 20220608154755.0 010 $a1-282-30595-6 010 $a9786612305955 010 $a0-470-13248-5 010 $a0-470-13283-3 035 $a(CKB)1000000000376279 035 $a(EBL)470043 035 $a(OCoLC)808668860 035 $a(SSID)ssj0000299783 035 $a(PQKBManifestationID)11236501 035 $a(PQKBTitleCode)TC0000299783 035 $a(PQKBWorkID)10260931 035 $a(PQKB)10674794 035 $a(MiAaPQ)EBC470043 035 $a(PPN)242932649 035 $a(EXLCZ)991000000000376279 100 $a20750907d1977 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 00$aInorganic syntheses$hVolume XVII$b[electronic resource] /$feditors, Aaron Wold, John K. Ruff 210 $aNew York $cMcGraw Hill$d1977 215 $a1 online resource (238 p.) 225 0 $aInorganic syntheses ;$v17 300 $aDescription based upon print version of record. 311 $a0-470-13179-9 320 $aIncludes bibliographical references and and index. 327 $aINORGANIC SYNTHESES Volume XVII; CONTENTS; Preface; Notice to Contributors; Chapter One METAL HYDRIDES; I. MAIN GROUP HYDRIDES (E. C. Ashby); 1. Magnesium Dihydride; 2. Zinc Dihydride; 3. Lithium Trihydridozincate(1-) and Lithium Tetrahydridozincate(2-); A. Lithium Trihydridozincate(1-); B. Lithium Tetrahydridozincate(2-); 4. Sodium Trihydridodimethyldizincate(1-) and Sodium Trihydridozincate(1-); A. Sodium Trihydridodimethyldizincate(1-); B. Sodium Trihydridozincate(1-); 5. Calcium Bis[tetrahydroborate(1-)]; 6. Quaternary Ammonium and Phosphonium Heptahydroborates 327 $aA. Methyltriphenylphosphonium Tetrahydroborate(1-)B. Tetrabutylammonium Tetrahydroborate(1-); C. Methyltriphenylphosphonium Heptahydrodiborate(1-); D. Tetrabutylammonium Heptahydrodiborate(1-); 7. Potassium Tri(sec-butyl)hydroborate(l-); 8. Bis(dimethylamino)borane; 9. Bis-u-(dimethylamino)-diborane(6); 10. u-(Dimethylamino)-diborane(6); 11. Trihydrido(trimethy1amink)aluminum and (Diethy1amino)hydridoaluminum Complexes; A. Triliydrido(trimethylamine)aluminum; B. (Diethylamino)dihydridoaluminum; C. Bis(diethylarnino)hydridoaluminum; 12. Trihydrido(trimethylarnine)galliurn 327 $a13. Lithium Tetrahydridogallate(1-)14. Sodium and Potassium Tetrahydridogallate(1-); II. TRANSITION METAL HYDRIDE COMPLEXES (Herbert D. Kaesz); 15. Hydrido Phosphine Arene Complexes of Molybdenum; A. Bis(n6-benzene)molybdenum; B. (n6-Benzene)dihydridobis(triphenylphosphine)molybdenum; C. (n6-Benzene)tris(dimethylphenylphosphine)hydridomolybdenum Hexafluorophosphate(1-); D. (n6-Benzene)tris(dimethylphenylphosphine)dihydridomolybdenum Bis[hexafluorophosphate(1-)]; 16. Bis[ethylenebis(diphenylphosphine)]hydrido(2,4-pentanedionato)molybdenum(II) 327 $a17. Tris(dimethylphenylphosphine)pentahydridorhenium(V)18. Dodecacarbonyltri-p-hydrido-triarigulo-trirhenium(I); 19. Bis[ethylenebis(diphenylphosphine)]hydridoiron Complexes; A. Chlorobis[ethylenebis(diphenylphosphine)]hydridoiron(II); B. Bis[ethylenebis(diphenylphosphine)]hydridoiron(II) Tetraphenylborate(1-); C. Bis[ethylenebis(diphenylphosphine)]hydridoiron(I); 20. Hydridonitrosyltris(triphenylphosphine)ruthenium(I); 21. Dihydridotetrakis(triphenylphosphine)ruthenium(II); 22. Hydrido[(n6-phenyl)diphenylxsphosphine]bis(triphenylphosphine)ruthenium(II) Tetrafluoroborate(1-) 327 $a23. (Acetato)hydridotris(triphenylphosphine)ruthenium(II)24. Hydridobis[(+)-dioplrhodium(1); 25. Nickel and Palladium Chlorohydridobis(phosphine) Complexes; A. trans-[Chlorohydridobis(tricyclohexylphosphine)nickel]; B. trans-[Chlorohydridobis(triisopropylphosphine)nickel]; C. trans-[Chlorohydridobis(tricyclohexylphosphine)palladium]; 26. Hydrido[tetrahydroborato(1-)] Nickel and Palladium Complexes; A. trans-[Hydrido[tetrahydroborato(1-)]bis(tricyclohexylphosphine)nickel]; B. trans-[Hydrido[tetrahydroborato(1-)]bis(tricyclohexylphosphine)palladium] 327 $a27. Bis(n5-cyclopentadienyl)[tetrahydroborato(1-)]titanium 330 $aThe volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested. 410 0$aInorganic Syntheses 606 $aInorganic compounds$xSynthesis 606 $aChemistry, Inorganic 615 0$aInorganic compounds$xSynthesis. 615 0$aChemistry, Inorganic. 676 $a541.39 676 $a541/.39 701 $aWold$b Aaron$f1927-$0975539 701 $aRuff$b John K$0975540 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910144313703321 996 $aInorganic syntheses$92221351 997 $aUNINA