LEADER 05151nam 2200649Ia 450 001 9910144313403321 005 20170810192827.0 010 $a1-282-30559-X 010 $a9786612305597 010 $a0-470-13249-3 010 $a0-470-13284-1 035 $a(CKB)1000000000376280 035 $a(EBL)469354 035 $a(OCoLC)808668866 035 $a(SSID)ssj0000299761 035 $a(PQKBManifestationID)11947457 035 $a(PQKBTitleCode)TC0000299761 035 $a(PQKBWorkID)10241577 035 $a(PQKB)10927561 035 $a(MiAaPQ)EBC469354 035 $a(PPN)243094213 035 $a(EXLCZ)991000000000376280 100 $a20750907d1978 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 00$aInorganic syntheses$hVolume XVIII$b[electronic resource] /$feditor-in-chief Daryle H. Busch 210 $aNew York $cWiley$d1978 215 $a1 online resource (260 p.) 225 0 $aInorganic syntheses ;$v18 300 $aDescription based upon print version of record. 311 $a0-471-03393-6 320 $aIncludes bibliographical references and and index. 327 $aINORGANIC SYNTHESES; CONTENTS; Notice to Contributors.; Toxic Substances.; Chapter One MACROCYCLIC LIGANDS AND THEIR METAL COMPLEXES; 1. 5,7,7,12,14,14-Hexamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene (5,7,7,12,14,14-Me6[14]-4,11-diene-1,4,8,11-N4) Complexes; A. 5,7,7,12,14,14-Hexamethyl-1,4,8,11-tetraazacyclotetraceca-4,11-diene Bis(trifluoromethanesulfonate).; B. 5,7,7,12,14,14-Hexamethyl-1,4,8,11-tetraazacyclotetraceca-4,11-diene Diperchlorate; C. [meso- and racemic-(5,7,7,12,14,14-hexamethyl-1,2,8,11-tetraazacyclotetradeca-4,11-diene)] nickel(II) Perchlorate 327 $aD. Bis(acetonitrile)(5,7,7,12,14,14-hexamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene)iron(II) Trifluoromethanesulfonate2. 5,5,7,12,12,14-Hexamethyl-1,4,8,11-tetraazacyclotetradecane (5,5,7,12,12,14-Me6[14]ane-1,4,8,11-N4) Complexes; A. meso- and racernic-(5,5,7,12,12,14-Hexamethyl-1,4,8,11-tetraazacyclotetradecane) Hydrate; B. [meso-(5,5,7,12,12,14-Hexamethyl-1,4,8,11-tetraazacyclotetradecane)]-nickel(II) Perchlorate; C. Dibromo [rneso-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetra-decane)] cobalt(III) Perchlorate 327 $aD. Bis(acetonitrile) [meso-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclo tetradecane)] iron(II) Trifluoromethanesulfonate3. 2,12-Dimethyl-3,7,11,17-tetraazabicyclo[11.3.1] heptadeca-1(17),2,11,13,15-pentaene (2,6-Me2-2',6':3,5-Pyo[14]-1,3,6-triene-1,4,7,11-N4) Complexes; A. (2,12-Dimethyl-3,7,11,17-tetraazabicyclo[11.3.11] heptadeca-1(17),2,11,13,15-pentaene)nickel(II) Perchlorate; B. Bromo(2,12-dimethyl-3,7,11,17-tetraazabicyclo[11.3.11] heptadeca-1(17),2,11,13,15-pentaene)cobalt(II) Bromide Monohydrate 327 $aC. Dibromo(2,12-dimethyl-3,7,11,17-tetraazabicyclo[11.3.11] heptadeca-1(17),2,11,13,15-pentaene)cobalt(III) Bromide Monohydrate4. 2,3,9,10-Tetramethyl-1,4,8,11-tetraazacyclotetradeca-1,3,8,10-tetraene(2,3,9,10-Me4[14]-1,3,8,10-tetraene-1,4,8,11-N4) Complexes; A. (2,3,9,10-Tetramethyl-1,4,8,11-tetraazacyclotetradeca-1,3,8,10-tetraene)nickel(II) Perchlorate; B. Bis(isothiocyanato)(2,3,9,10-tetramethyl-1,4,8,11-tetraazacyclotetradeca-1,3,8,10-tetraene)nickel(II); C. Dibromo(2,3,9,10-tetramethyl-1,4,8,11-tetraazacyclotetradeca-1,3,8,10-tetraene)cobalt(III) Bromide 327 $a5. 2,3-Dimethyl-1,4,8,11-tetraazacyclotetradeca-1,3-diene(2,3-Me2[14]-1,3-diene-1,4,8,11-N4)ComplexesA. (2,3-Dimethyl-1,4,8,11-tetraazacyclotetradeca-1,3-diene)nickel(II) Tetrachlorozincate(2-); B. Dibromo(2,3-dimethyl-1,4,8,11-tetraazacyclotetradeca-1,3-diene)-cobalt(III) Perchlorate; 6. Tetrabenzo[b,f,j,n][1,5,9,13] tetraazacyclohexadecine(2,3; 6,7; 10,11; 14,15-Bzo[16] octaene-1,5,9,13-N4) Complexes; A. (Tetrabenzo[b,f,j,n][1,5,9,13] tetraazacyclohexadecine)nickel(II) Perchlorate; B. Bis(isothiocyanato)(tetrabenzo[b,f,j,n][1,5,9,13] tetraazacyclohexadecine)nickel(II) 327 $aC. (Tetrabenzo[b,f,j,n][1,5,9,13] tetraazacyclohexadecine)copper(II) Nitrate 330 $aThe volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested. 410 0$aInorganic Syntheses 606 $aInorganic compounds$xSynthesis 606 $aChemistry, Inorganic 615 0$aInorganic compounds$xSynthesis. 615 0$aChemistry, Inorganic. 676 $a541.39 676 $a541/.39 701 $aBusch$b Daryle H$g(Daryle Hadley),$f1928-$0911774 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910144313403321 996 $aInorganic syntheses$92041745 997 $aUNINA