LEADER 04657nam 2200637Ia 450 001 9910144312303321 005 20170815160610.0 010 $a1-282-30540-9 010 $a9786612305405 010 $a0-470-13253-1 010 $a0-470-13288-4 035 $a(CKB)1000000000376284 035 $a(EBL)469519 035 $a(OCoLC)808668852 035 $a(SSID)ssj0000299763 035 $a(PQKBManifestationID)11266121 035 $a(PQKBTitleCode)TC0000299763 035 $a(PQKBWorkID)10260929 035 $a(PQKB)10412729 035 $a(MiAaPQ)EBC469519 035 $a(PPN)243151349 035 $a(EXLCZ)991000000000376284 100 $a20750907d1983 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 00$aInorganic syntheses$hVolume 22$b[electronic resource] /$feditor-in-chief, Smith L. Holt, Jr 210 $aNew York $cMcGraw Hill$d1983 215 $a1 online resource (298 p.) 225 0 $aInorganic syntheses ;$v22 300 $aDescription based upon print version of record. 311 $a0-471-88887-7 320 $aIncludes bibliographical references and and index. 327 $aINORGANIC SYNTHESES Volume 22; CONTENTS; Chapter One SOLID STATE; 1. Ternary Chlorides and Bromides of the Rare Earth Elements; A. AIRE2IIIX7: Cesium Praesodymium Chloride (CsPr2Cl7) and Postassium Dysprosium Chloride (KDy2Cl7); B. AI3RE2IIIX9, AI2REIIIX5, AI3REIIX6: The Cesium Lutetium Chlorides, Cs3Lu2Cl9, Cs2LuCl5, Cs3LuCl6; 2. Quaternary Chlorides and Bromides of the Rare Earth Elements: Elpasolites AI2BIREIIIX6 (r(AI)>r(BI)); A. Cesium Lithium Thulium Chloride, (Cs2LiTmCl6); B. Other Chloro- and Bromo elpasolites; 3. Tantalum as a High-Temperature Container Material for Reduced Halides 327 $a4. Cesium Scandium(II) TrichlorideA. Synthesis with CsCl; B. Synthesis with Cs3Sc2Cl9; 5. Zirconium Monochloride and Monobromide; A. Synthesis with Zirconium Foil; B. Synthesis Using Zirconium Turnings; 6. Lanthanum Triiodide (And Other Rare Earth Metal Triiodides); A. Synthesis Using Hgl2; B. Synthesis from the Elements; 7. Lanthanum Diiodide; 8. Trichlorides of Rare Earth Elements. Yttrium, and Scandium; 9. Single Crystal Growth of Oxides by Skull Melting: The Case of Magnetite (Fe3O4; 10. Lithium Nitride, Li3N; A. Polycrystalline Material; B. Single Crystals of Li3N 327 $a11. The Alkali Ternary Oxides AXCoO2 and AXCrO2 (A = Na, K)A. Sodium Cobalt Oxides: NaxCoO2 (x < 1); B. Potassium Cobalt Oxide Bronzes: K0.50CoO2, K0.67CoO2; C. Potassium Cobalt Oxide: KCoO2; D. Potassium Chromium Oxide: KCrO2; E. Potassium Chromium Oxide Bronzes: KxCrO2; 12. Zeolite Molecular Sieves; A. Zeolite A2; B. Zeolite Y3; C. TMA Offretite4; D. ZSM-5; 13. Lead Ruthenium Oxide, Pb2 [Ru2-xPb4x+]O6.5; 14. Calcium Manganese Oxide. Ca2Mn3O8; 15. Synthesis of Silver Tetratungstate; 16. Cadmium Mixed Chalcogenides and Layers of Cadmium (Mixed); A. Cadmium Selenide Telluride (CdSe0.65Te0.35) 327 $aB. Cadmium Selenide Thin Layers on TitaniumC. Cadmium Selenide Telluride Layers on Molybdenum; 17. Layered Intercalation Compounds; A. Charge-Transfer-Type Intercalation Compounds: FeOCl(Pyridine derivative)1/n; B. Grafted-Type Compound from FeOCl; C. The Organic Intercalates of HTiNbO5; 18. Iron Titanium Hydride (FeTiH1.94); 19. Aluminum Lanthanum Nickel Hydride; Chapter Two TRANSITION METAL COMPLEXES AND COMPOUNDS; 20. Purification of Copper(I) Iodide; 21. Cobalt(III) Amine Complexes with Coordinated Trifluoromethanesulfonate 327 $aA. Pentammine(trifluoromethanesulfonato)cobalt(III) Trifluoromethanesulfonate, [Co(NH3)5OSO2CF3](CF3SO3)2B. cis-Bis(1,2-ethylenediarnine)di(trifluoromethanesulfonato )- cobalt(III) Trifluoromethanesulfonate, cis-[Co(en2)(OSO2CF3)2](CF3SO3); C. fac-Tris(trifluoromethanesulfonato)[N-(2-aminoethyl)-1,2-ethanediamine]cobalt(III), Co(dien)(OSO2CF3)3; 22. 2,9-Dimethyl-3,10-diphenyl-1,4,8,11-tetraazacyclotetradeca-1,3,8,10-tetraene, (Me2Ph2 [14]-1,3,8,10-tetraeneN4) Complexes 327 $aA. Bis(acetonitrile)(2,9-dimethyl-3,10-diphenyl-1,4,8,11-tetraazacyclotetradeca-1,3,8,10-tetraene)iron(II) Hexafluorophosphate 410 0$aInorganic Syntheses 606 $aInorganic compounds$xSynthesis 606 $aChemistry, Inorganic 615 0$aInorganic compounds$xSynthesis. 615 0$aChemistry, Inorganic. 676 $a541.39 676 $a541/.39 701 $aHolt$b Smith L.$f1938-$0984005 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910144312303321 996 $aInorganic syntheses$92246820 997 $aUNINA