LEADER 05281nam 2200637 a 450 001 9910143426303321 005 20170815113117.0 010 $a1-280-44819-9 010 $a9786610448197 010 $a0-470-32598-4 010 $a0-471-91458-4 010 $a0-471-91456-8 035 $a(CKB)1000000000354904 035 $a(EBL)257226 035 $a(OCoLC)71522742 035 $a(SSID)ssj0000250983 035 $a(PQKBManifestationID)11939228 035 $a(PQKBTitleCode)TC0000250983 035 $a(PQKBWorkID)10247029 035 $a(PQKB)10812536 035 $a(MiAaPQ)EBC257226 035 $a(EXLCZ)991000000000354904 100 $a20051121d2006 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 10$aStatic headspace-gas chromatography$b[electronic resource] $etheory and practice /$fBruno Kolb and Leslie S. Ettre 205 $a2nd ed. 210 $aHoboken, N.J. $cWiley$dc2006 215 $a1 online resource (377 p.) 300 $aDescription based upon print version of record. 311 $a0-471-74944-3 320 $aIncludes bibliographical references and index. 327 $aStatic Headspace-Gas Chromatography; Contents; Preface; Preface to the First Edition; List of Acronyms and Symbols; 1 General Introduction; 1.1 Principles of Headspace Analysis; 1.2 Types of Headspace Analysis; 1.2.1 Principles of Static HS-GC; 1.2.2 Principles of Dynamic HS-GC; 1.2.2.1 The Trap; 1.2.2.2 The Water Problem; 1.2.2.3 The Flow Problem; 1.2.2.4 The Time Problem; 1.2.2.5 Comparison of Static HS-GC with P&T; 1.3 The Evolution of the HS-GC Methods; 1.4 HS-GS Literature; 1.5 Regulatory Methods Utilizing (Static) HS-GC; References; 2 Theoretical Background of HS-GC and Its Applications 327 $a2.1 Basic Theory of Headspace Analysis2.2 Basic Physicochemical Relationships; 2.3 Headspace Sensitivity; 2.3.1 Influence of Temperature on Vapor Pressure and Partition Coefficient; 2.3.1.1 Enhancement of Lower Boiling Compounds; 2.3.2 Influence of Temperature on Headspace Sensitivity for Compounds with Differing Partition Coefficients; 2.3.3 Influence of Sample Volume on Headspace Sensitivity for Compounds with Differing Partition Coefficients; 2.3.3.1 Sample-to-Sample Reproducibility; 2.3.4 Changing the Sample Matrix by Varying the Activity Coefficient; 2.4 Headspace Linearity 327 $a2.5 Duplicate Analyses2.6 Multiple Headspace Extraction (MHE); 2.6.1 Principles of MHE; 2.6.2 Theoretical Background of MHE; 2.6.3 Simplified MHE Calculation; References; 3 The Technique of HS-GC; 3.1 Sample Vials; 3.1.1 Vial Types; 3.1.2 Selection of the Vial Volume; 3.1.3 Vial Cleaning; 3.1.4 Wall Adsorption Effects; 3.2 Caps; 3.2.1 Pressure on Caps; 3.2.2 Safety Closures; 3.3 Septa; 3.3.1 Septa Types; 3.3.2 Septum Blank; 3.3.3 Should a Septum Be Pierced Twice?; 3.3.3.1 Closed-Vial versus Open-Vial Sample Introduction Technique; 3.4 Thermostatting; 3.4.1 Influence of Temperature 327 $a3.4.2 Working Modes3.5 The Fundamental Principles of Headspace Sampling Systems; 3.5.1 Systems Using Gas Syringes; 3.5.2 Solid Phase Microextraction (SPME); 3.5.2.1 Comparison of the Sensitivities in HS-SPME and Direct Static HS-GC; 3.5.3 Balanced Pressure Sampling Systems; 3.5.4 Pressure/Loop Systems; 3.5.5 Conditions for Pressurization Systems; 3.5.6 Volume of the Headspace Gas Sample; 3.5.6.1 Sample Volume with Gas Syringes; 3.5.6.2 Sample Volume with Loop Systems; 3.5.6.3 Sample Volume with the Balanced Pressure System; 3.6 Use of Open-Tubular (Capillary) Columns 327 $a3.6.1 Properties of Open-Tubular Columns for Gas Samples3.6.2 Headspace Sampling with Split or Splitless Introduction; 3.6.3 Comparison of Split and Splitless Headspace Sampling; 3.6.4 Band Broadening During Sample Introduction; 3.6.5 Influence of Temperature on Band Broadening; 3.6.5.1 Conclusions; 3.6.6 The Combination of Different Columns and Detectors; 3.7 Enrichment Techniques in HS-GC; 3.7.1 Systems for Cryogenic Trapping; 3.7.1.1 Trapping by Cryogenic Condensation; 3.7.1.2 Trapping by Cryogenic Focusing; 3.7.1.3 Influence of Temperature on Cryogenic Focusing 327 $a3.7.1.4 Comparison of the Various Techniques of Cryogenic Trapping 330 $aThe only reference to provide both current and thorough coverage of this important analytical techniqueStatic headspace-gas chromatography (HS-GC) is an indispensable technique for analyzing volatile organic compounds, enabling the analyst to assay a variety of sample matrices while avoiding the costly and time-consuming preparation involved with traditional GC.Static Headspace-Gas Chromatography: Theory and Practice has long been the only reference to provide in-depth coverage of this method of analysis. The Second Edition has been thoroughly updated to reflect the most recent 606 $aGas chromatography 608 $aElectronic books. 615 0$aGas chromatography. 676 $a543.85 676 $a543/.85 700 $aKolb$b Bruno$0729196 701 $aEttre$b Leslie S$015263 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910143426303321 996 $aStatic headspace gas-chromatography$91427730 997 $aUNINA LEADER 03251nam 22006735 450 001 9910254802503321 005 20250311150759.0 010 $a9783319559292 010 $a331955929X 024 7 $a10.1007/978-3-319-55929-2 035 $a(CKB)3710000001418525 035 $a(MiAaPQ)EBC4894555 035 $a(DE-He213)978-3-319-55929-2 035 $a(Perlego)3496773 035 $a(EXLCZ)993710000001418525 100 $a20170630d2017 u| 0 101 0 $aeng 135 $aurcnu|||||||| 181 $2rdacontent 182 $2rdamedia 183 $2rdacarrier 200 10$aEmotions and The Body in Buddhist Contemplative Practice and Mindfulness-Based Therapy $ePathways of Somatic Intelligence /$fby Padmasiri de Silva 205 $a1st ed. 2017. 210 1$aCham :$cSpringer Nature Switzerland :$cImprint: Palgrave Macmillan,$d2017. 215 $a1 online resource (144 pages) 225 1 $aPalgrave Pivot 311 08$a9783319559285 311 08$a3319559281 320 $aIncludes bibliographical references and indexes. 330 $aThis book represents an outstanding contribution to the field of somatic psychology. It focuses on the relationship between body and emotions, and on the linkages between mindfulness-based emotion studies and neuroscience. The author discusses the awakening of somatic intelligence as a journey through pain and trauma management, the moral dimensions of somatic passions, and the art and practice of embodied mindfulness. Issues such as the emotions and the body in relation to Buddhist contemplative practice, against the background of the most recent findings of current neuroscience, are expanded in the book. A broad review of the Darwinian-Jamesian heritage on emotion studies is a unique contribution to the tradition of the somatogenic strands of emotions, and provides a contrasting focus to the ideogenic emotions in Sigmund Freud. 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