LEADER 05407nam 2200745 450 001 9910140280303321 005 20220603150946.0 010 $a3-527-64938-7 010 $a3-527-64936-0 010 $a3-527-64939-5 035 $a(CKB)2670000000534442 035 $a(EBL)1642423 035 $a(SSID)ssj0001211610 035 $a(PQKBManifestationID)11795726 035 $a(PQKBTitleCode)TC0001211610 035 $a(PQKBWorkID)11202770 035 $a(PQKB)11248112 035 $a(OCoLC)878139150 035 $a(MiAaPQ)EBC1642423 035 $a(Au-PeEL)EBL1642423 035 $a(CaPaEBR)ebr10845585 035 $a(CaONFJC)MIL578635 035 $a(OCoLC)871781076 035 $a(PPN)196495679 035 $a(EXLCZ)992670000000534442 100 $a20140318h20142014 uy 0 101 0 $aeng 135 $aurcnu|||||||| 181 $ctxt 182 $cc 183 $acr 200 10$aCalorimetry $efundamentals, instrumentation and applications /$fStefan M. Sarge, Gu?nther W. H. Ho?hne and Wolfgang Hemminger 205 $a2nd ed. 210 1$aWeinheim, Germany :$cWiley-VCH Verlag,$d2014. 210 4$dİ2014 215 $a1 online resource (300 p.) 300 $aDescription based upon print version of record. 311 $a3-527-32761-4 320 $aIncludes bibliographical references and index. 327 $aCalorimetry: Fundamentals, Instrumentation and Applications; Contents; Preface; List of Quantities and Units; Introduction: Calorimetry: Definition, Application Fields and Units; Definition of Calorimetry; Application Fields for Calorimetry; First Example from Life Sciences; Second Example from Material Science; Third Example from Legal Metrology; Units; Further Reading; References; Part One: Fundamentals of Calorimetry; 1 Methods of Calorimetry; 1.1 Compensation of the Thermal Effect; 1.1.1 Compensation by a Phase Transition; 1.1.2 Compensation by Electric Effects 327 $a1.2 Measurement of Temperature Differences 1.2.1 Measurement of Time-Dependent Temperature Differences; 1.2.2 Measurement of Local Temperature Differences; 1.2.2.1 First Example: Flow Calorimeter; 1.2.2.2 Second Example: Heat Flow Rate Calorimeter; 1.3 Summary of Measuring Principles; References; 2 Measuring Instruments; 2.1 Measurement of Amount of Substance; 2.1.1 Weighing; 2.1.2 Volume Measurement; 2.1.3 Pressure Measurement; 2.1.4 Flow Measurement; 2.2 Measurement of Electric Quantities; 2.3 Measurement of Temperatures; 2.3.1 Thermometers; 2.3.1.1 Liquid-in-Glass Thermometers 327 $a2.3.1.2 Gas Thermometers 2.3.1.3 Vapor Pressure Thermometers; 2.3.1.4 Resistance Thermometers; 2.3.1.5 Semiconductors; 2.3.1.6 Pyrometers; 2.3.2 Thermocouples; 2.4 Chemical Composition; References; 3 Fundamentals of Thermodynamics; 3.1 States and Processes; 3.1.1 Thermodynamic Variables (Functions of State); 3.1.2 Forms of Energy, Fundamental Form, and Thermodynamic Potential Function; 3.1.2.1 Fundamental Form; 3.1.2.2 Thermodynamic Potential Function; 3.1.3 Equilibrium; 3.1.4 Reversible and Irreversible Processes; 3.1.5 The Laws of Thermodynamics; 3.1.5.1 The Zeroth Law; 3.1.5.2 The First Law 327 $a3.1.5.3 The Second Law 3.1.5.4 The Third Law; 3.1.6 Measurement of Thermodynamic State Functions; 3.2 Phases and Phase Transitions; 3.2.1 Multiphase Systems; 3.2.2 Phase Transitions; 3.2.3 Gibbs Phase Rule; 3.2.4 Measurement of Variables of State during Phase Transitions; References; 4 Heat Transport Phenomena; 4.1 Heat Conduction; 4.2 Convection; 4.3 Heat Radiation; 4.4 Heat Transfer; 4.5 Entropy Increase during Heat Exchange; 4.6 Conclusions Concerning Calorimetry; References; 5 Surroundings and Operating Conditions; 5.1 The Isothermal Condition; 5.2 The Isoperibol Condition 327 $a5.3 The Adiabatic Condition 5.4 The Scanning Condition; Reference; 6 Measurements and Evaluation; 6.1 Consequences of Temperature Relaxation within the Sample; 6.1.1 First Example: Chemical Reaction; 6.1.2 Second Example: Biological System; 6.1.3 Third Example: First-Order Phase Transitions; 6.2 Typical Results from Different Calorimeters; 6.2.1 Adiabatic Calorimeters; 6.2.2 Isoperibol Calorimeters; 6.2.3 Differential Scanning Calorimeters; 6.3 Reconstruction of the True Sample Heat Flow Rate from the Measured Function; 6.3.1 Reconstruction of the Temperature Field for Negative Times 327 $a6.3.2 The Convolution Integral and Its Validity 330 $aClearly divided into three parts, this practical book begins by dealing with all fundamental aspects of calorimetry. The second part looks at the equipment used and new developments. The third and final section provides measurement guidelines in order to obtain the best results. The result is optimized knowledge for users of this technique, supplemented with practical tips and tricks. 606 $aCalorimeters 606 $aCalorimetry 606 $aCombustion$xMeasurement 606 $aThermal analysis 615 0$aCalorimeters. 615 0$aCalorimetry. 615 0$aCombustion$xMeasurement. 615 0$aThermal analysis. 676 $a535.6 700 $aSarge$b Stefan Mathias$0936559 702 $aHo?hne$b Gu?nther W. H. 702 $aHemminger$b Wolfgang 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910140280303321 996 $aCalorimetry$92109632 997 $aUNINA