LEADER 06099nam 2200673 450 001 9910139017803321 005 20231110213743.0 010 $a1-118-69079-6 010 $a1-118-69044-3 010 $a1-118-69059-1 035 $a(CKB)2550000001115787 035 $a(StDuBDS)AH25496819 035 $a(SSID)ssj0000981838 035 $a(PQKBManifestationID)11532542 035 $a(PQKBTitleCode)TC0000981838 035 $a(PQKBWorkID)10982934 035 $a(PQKB)10307982 035 $a(MiAaPQ)EBC1365055 035 $a(DLC) 2013019307 035 $a(Au-PeEL)EBL1365055 035 $a(CaPaEBR)ebr10756838 035 $a(CaONFJC)MIL516122 035 $a(OCoLC)843955907 035 $a(MiAaPQ)EBC7103948 035 $a(Au-PeEL)EBL7103948 035 $a(EXLCZ)992550000001115787 100 $a20130507h20142014 uy| 0 101 0 $aeng 135 $aur||||||||||| 181 $ctxt 182 $cc 183 $acr 200 10$aCrystals and crystallinity in polymers $ediffraction analysis of ordered and disordered crystals /$fClaudio De Rosa, Finizia Auriemma 210 1$aHoboken, New Jersey :$cWiley,$d[2014] 210 4$d2014 215 $a1 online resource (464 pages) 225 1 $aNew York Academy of Sciences 300 $aBibliographic Level Mode of Issuance: Monograph 311 $a0-470-17576-1 311 $a1-299-84871-0 320 $aIncludes bibliographical references and index. 327 $aMachine generated contents note: Chapter 1 Configuration and Conformation of Macromolecules in Polymer Crystals 1.1 Crystals of polymers 1.2 Constitution and configuration of crystalline polymers 1.3 Conformation 1.4 Relationships among internal parameters of macromolecules 1.5 Conformation of polymer chains in the crystalline state 1.6 Helical conformations in isotactic and syndiotactic polymers 1.7 Conformational energy calculations 1.8 Helical conformation and optical activity 1.9 Alternating copolymers 1.10 Polydienes 1.11 Non helical chain conformations of isotactic polymers References Chapter 1 Chapter 2 Packing of macromolecules in polymer crystals 2.1 General principles 2.2 The principle of density (entropy)-driven phase formation in polymers 2.3 Symmetry breaking 2.4 Impact of chain folding on crystal structure symmetry 2.5 Frustrated Polymer Crystal Structures 2.6 Chiral crystallization of polymers with helical chain conformations 2.7 Packing effects on the conformation of polymer chains in the crystals: the case of aliphatic polyamides References Chapter 2 Chapter 3 3.1 X-ray diffraction of semicrystalline polymers 3.2 Fourier synthesis and the phase problem in crystallography 3.3 X-ray fiber diffraction analysis 3.4 Determination of parameters of the unit cell and indexing of the diffraction pattern 3.5 Measure of the integrated intensities of the reflections and corrections for geometrical (Lorentz), polarization and absorption factors 3.6 Calculation of Structure Factors 3.7 Structural refinement 3.8 Form of diffraction pattern and broadening due to the Laue function References Chapter 3 Chapter 4 Defects and Disorder in Polymer Crystals 4.1 Classification of different types of structural disorder 4.2 Crystals with partial three-dimensional order (Class A)Disorder with three-dimensional periodicity maintained only for some characterizing points of the structure 4.3 Solid mesophases References Chapter 4 Chapter 5 Methods of Analysis of Diffuse Scattering from Disordered Structures of Polymers 5.1 Structural disorder and diffuse scattering 5.2 Methods of diffraction analysis from disordered crystals 5.3 Long Range Order in Disordered Lattices of Class A 5.4 Short Range Order in Disordered Crystals of Class A 5.5 Short Range Order in Disordered Crystals with Substitution type Disorder 5.6 Short Range vs Long Range Order in Disordered Crystals of Class B and C (Solid Mesophases) 5.7 Disordered Models with Perturbations Occurring over Continuous Ranges 5.8 Basic formulas for the calculation of X-ray Diffraction Intensity from Disordered Model Structures of Polymers 5.9 Examples of calculation of average diffracted intensity of structures disordered in one dimension 5.10 Integration method of diffraction intensity for cylindrically and spherical surfaces in the reciprocal space References Chapter 5 Chapter 6 Crystal habit 6.1 Basic remark 6.2 Rounded lateral habits 6.3 Chain folding, molecular orientation and sectorization 6.4 Twinning and secondary nucleation theory 6.5 Homoepitaxy, morphology, stem orientation and polymorphism References Chapter 6 Chapter 7 Influence of Crystal Defects and Structural Disorder on the Physical and Mechanical Properties of Polymeric Materials 7.1 Introduction 7.2 Stress induced phase transformations during deformation 7.3 Isotactic polypropylene 7.4 Syndiotactic Polypropylene References Chapter 7. 330 $a"Polymeric crystals are more complex in nature than other materials' crystal structures due to significant structural disorder present. In fact, they actually exist in a semicrystalline state where the crystals are embedded in an amorphous phase to create a highly interconnected network. Presenting an in-depth and current overview of polymer crystals, Crystals and Crystallinity in Polymers provides researchers, engineers, and graduate students with guidelines to help select the proper crystallization method, evaluate polymer crystallization data, determine which methods to utilize for particular cases, and understand the different analytical techniques utilized"--$cProvided by publisher. 410 0$aNew York Academy of Sciences 606 $aCrystalline polymers 606 $aCrystallization 615 0$aCrystalline polymers. 615 0$aCrystallization. 676 $a547/.7 686 $aTEC009010$2bisacsh 700 $aDe Rosa$b Claudio$0895929 701 $aAuriemma$b Finizia$0895930 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910139017803321 996 $aCrystals and crystallinity in polymers$92001574 997 $aUNINA LEADER 01590nas--2200373-n-450 001 990008948280403321 005 20240229084433.0 011 $a1040-8746 035 $a000894828 035 $aFED01000894828 035 $a(Aleph)000894828FED01 035 $a000894828 091 $2CNR$aP 00066592 100 $a20161109a19899999km-y0itaa50------ba 101 0 $aeng 102 $aUS 110 $aauu-------- 200 1 $aCurrent opinion in oncology 207 1$a1989- 210 $aPhiladelphia$cLippincott Williams and Wilkins 326 $aBimestrale 452 0$12001$aCurrent opinion in oncology (Online) 530 0 $aCurrent opinion in oncology 676 $a616.99/2/005 801 0$aIT$bACNP$c20090723 859 4 $uhttp://acnp.cib.unibo.it/cgi-ser/start/it/cnr/dc-p1.tcl?catno=915958&person=false&language=ITALIANO&libr=&libr_th=unina1$zBiblioteche che possiedono il periodico 901 $aSE 912 $a990008948280403321 958 $aBiblioteca Centrale della Facoltà di Medicina e Chirurgia di Napoli " Federico II "$b1996-1997;1999-2000;$c2000;$escaffale 6$fFMEBC 959 $aFMEBC 996 $aCurrent opinion in oncology$9797536 997 $aUNINA AP1 8 $6866-01$aNA206 Biblioteca Centrale della Facoltà di Medicina e Chirurgia di Napoli " Federico II "$bscaffale 6$eVia Sergio Pansini, 5, 80131 Napoli (NA)$m0817463408$m0817463465/08$nit AP2 40$aacnp.cib.unibo.it$nACNP Italian Union Catalogue of Serials$uhttp://acnp.cib.unibo.it/cgi-ser/start/it/cnr/df-p.tcl?catno=915958&language=ITALIANO&libr=&person=&B=1&libr_th=unina&proposto=NO