LEADER 05010nam 22005295 450 001 9910789202403321 005 20230907121049.0 010 $a94-011-1324-6 024 7 $a10.1007/978-94-011-1324-3 035 $a(CKB)3400000000121728 035 $a(SSID)ssj0000933281 035 $a(PQKBManifestationID)11508105 035 $a(PQKBTitleCode)TC0000933281 035 $a(PQKBWorkID)10890862 035 $a(PQKB)10505826 035 $a(DE-He213)978-94-011-1324-3 035 $a(MiAaPQ)EBC3566196 035 $a(PPN)237956268 035 $a(EXLCZ)993400000000121728 100 $a20121227d1995 u| 0 101 0 $aeng 135 $aurnn#008mamaa 181 $ctxt 182 $cc 183 $acr 200 10$aThermal Methods of Analysis $ePrinciples, Applications and Problems /$fby P.J. Haines$b[electronic resource] 205 $a1st ed. 1995. 210 1$aDordrecht :$cSpringer Netherlands :$cImprint: Springer,$d1995. 215 $a1 online resource (XII, 286 p.) 300 $aBibliographic Level Mode of Issuance: Monograph 311 $a0-7514-0050-5 327 $a1 Introduction to thermal methods -- 1.1 Introduction -- 1.2 Historical development -- 1.3 Definitions -- 1.4 Computers and thermal methods -- 1.5 Factors affecting thermal analysis results -- 1.6 Simultaneous and complementary techniques -- 1.7 Problems -- References -- General Bibliography -- 2 Thermogravimetry -- 2.1 Introduction -- 2.2 Historical -- 2.3 Definition of thermogravimetry -- 2.4 Apparatus -- 2.5 Kinetics of reactions -- 2.6 Applications of thermogravimetry -- 2.7 Controlled rate thermogravimetry and Hi-Res? TGA -- 2.8 Problems -- References -- 3 Differential thermal analysis and differential scanning calorimetry -- 3.1 Introduction -- 3.2 Historical -- 3.3 Definitions -- 3.4 Apparatus -- 3.5 Theory of DTA and DSC -- 3.6 Heat flux DSC -- 3.7 Power-compensated DSC -- 3.8 Calibration -- 3.9 Applications -- 3.11 Problems -- References -- 4 Thermomechanical, dynamic mechanical and associated methods -- 4.1 Introduction -- 4.2 Definitions -- 4.3 Thermomechanical analysis -- 4.4 Dynamic mechanical analysis -- 4.5 Dielectric thermal analysis -- 4.6 Thermally stimulated current analysis and relaxation map analysis -- 4.7 Problems -- References -- 5 Simultaneous techniques and product analysis -- 5.1 Introduction -- 5.2 Simultaneous thermal analysis -- 5.3 Evolved gas analysis -- 5.4 Detection and identification of evolved gases -- 5.5 Infrared and simultaneous TA-infrared -- 5.6 Infrared product analysis -- 5.7 Thermomicroscopy -- 5.8 X-ray methods -- 5.9 Electron microscopy and associated techniques -- 5.10 Conclusion -- 5.11 Less common thermal analysis techniques -- 5.12 Problems -- References -- 6 Problem solving and applications of thermal methods -- List of examples -- Problems/Solutions -- 6.1 Inorganic materials -- 6.2 Polymeric materials -- 6.3 Fine chemicals and pharmaceuticals -- 6.4 Other materials -- References -- Appendix: Solutions to problems in Chapters 1-5. 330 $aThe wide range of applications of thermal methods of analysis in measuring physical properties, studying chemical reactions and determining the thermal behaviour of samples is of interest to academics and to industry. These applications prompted the writing of this book, in the hope that the descriptions, explanations and examples given would be of help to the analyst and would stimulate the investigation of other thermal techniques. Thermal studies are a fascinating means of examining the samples and the problems brought to us by colleagues, students and clients. If time allows, watching crystals change on a hot-stage microscope, or measuring the properties and changes on a DSC or TG or any thermal instrument can be a rewarding activity, besides providing valuable analytical information. This book started from a series of lectures delivered at Kingston University and at meetings of the Thermal Methods Group of the United Kingdom. The collaboration and information supplied to all the contribu­ tors by colleagues and instrument manufacturers is most gratefully ack­ nowledged, as are the valuable contributions made at meetings of the International Confederation for Thermal Analysis and Calorimetry (ICT AC) and at the European Symposia on Thermal Analysis and Calorimetry (ESTAC). 606 $aAnalytical chemistry 606 $aChemistry 606 $aAnalytical Chemistry$3https://scigraph.springernature.com/ontologies/product-market-codes/C11006 606 $aChemistry/Food Science, general$3https://scigraph.springernature.com/ontologies/product-market-codes/C00004 615 0$aAnalytical chemistry. 615 0$aChemistry. 615 14$aAnalytical Chemistry. 615 24$aChemistry/Food Science, general. 676 $a543 700 $aHaines$b P.J$4aut$4http://id.loc.gov/vocabulary/relators/aut$0314643 906 $aBOOK 912 $a9910789202403321 996 $aThermal methods of analysis$9192740 997 $aUNINA LEADER 01408oam 2200445zu 450 001 9910138921603321 005 20241212215807.0 010 $a9781424449262 010 $a142444926X 010 $a9781424449286 010 $a1424449286 035 $a(CKB)2400000000002870 035 $a(SSID)ssj0000453070 035 $a(PQKBManifestationID)12201911 035 $a(PQKBTitleCode)TC0000453070 035 $a(PQKBWorkID)10472170 035 $a(PQKB)11642585 035 $a(NjHacI)992400000000002870 035 $a(EXLCZ)992400000000002870 100 $a20160829d2009 uy 101 0 $aeng 135 $aur||||||||||| 181 $ctxt 182 $cc 183 $acr 200 10$a2009 IEEE International Symposium on Modeling, Analysis and Simulation of Computer and Telecommunication Systems 210 31$a[Place of publication not identified]$cIEEE$d2009 215 $a1 online resource 300 $aBibliographic Level Mode of Issuance: Monograph 311 08$a9781424449279 311 08$a1424449278 606 $aDigital computer simulation$vCongresses 615 0$aDigital computer simulation 676 $a001.640184 702 $aIEEE Staff 801 0$bPQKB 906 $aPROCEEDING 912 $a9910138921603321 996 $a2009 IEEE International Symposium on Modeling, Analysis and Simulation of Computer and Telecommunication Systems$92506562 997 $aUNINA