LEADER 04929nam 2200745 450 001 9910132191903321 005 20200520144314.0 010 $a1-118-69570-4 010 $a1-118-68249-1 010 $a1-118-69571-2 035 $a(CKB)3710000000138588 035 $a(EBL)1712954 035 $a(SSID)ssj0001225462 035 $a(PQKBManifestationID)11673835 035 $a(PQKBTitleCode)TC0001225462 035 $a(PQKBWorkID)11269940 035 $a(PQKB)11321268 035 $a(OCoLC)889314789 035 $a(MiAaPQ)EBC1712954 035 $a(DLC) 2014004528 035 $a(Au-PeEL)EBL1712954 035 $a(CaPaEBR)ebr10902336 035 $a(CaONFJC)MIL633681 035 $a(OCoLC)881571476 035 $a(PPN)189859598 035 $a(EXLCZ)993710000000138588 100 $a20140815h20142014 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 00$aStructure from diffraction methods /$fedited by Duncan W. Bruce, Dermot O'Hare, Richard I. Walton 210 1$aWest Sussex, England :$cJohn Wiley & Sons, Ltd.,$d2014. 210 4$dİ2014 215 $a1 online resource (705 p.) 225 1 $aInorganic Materials Series 300 $aDescription based upon print version of record. 311 $a1-119-95322-7 320 $aIncludes bibliographical references and index. 327 $aCover; Inorganic Materials Series; Title Page; Copyright; Inorganic Materials Series Preface; Preface; List of Contributors; Chapter 1: Powder Diffraction; 1.1 INTRODUCTION; 1.2 THE SIMILARITIES AND DIFFERENCES BETWEEN SINGLE-CRYSTAL XRD AND POWDER XRD; 1.3 QUALITATIVE ASPECTS OF POWDER XRD: 'FINGERPRINTING' OF CRYSTALLINE PHASES; 1.4 QUANTITATIVE ASPECTS OF POWDER XRD: SOME PRELIMINARIES RELEVANT TO CRYSTAL STRUCTURE DETERMINATION; 1.5 STRUCTURE DETERMINATION FROM POWDER XRD DATA; 1.6 SOME EXPERIMENTAL CONSIDERATIONS IN POWDER XRD; 1.7 POWDER NEUTRON DIFFRACTION VERSUS POWDER XRD 327 $a1.8 VALIDATION OF PROCEDURES AND RESULTS IN STRUCTURE DETERMINATION FROM POWDER XRD DATA1.9 MORE DETAILED CONSIDERATION OF THE APPLICATION OF POWDER XRD AS A 'FINGERPRINT' OF CRYSTALLINE PHASES; 1.10 EXAMPLES OF THE APPLICATION OF POWDER XRD IN CHEMICAL CONTEXTS; 1.11 CONCLUDING REMARKS; References; Chapter 2: X-Ray and Neutron Single-Crystal Diffraction; 2.1 Introduction; 2.2 Solid-State Fundamentals; 2.3 Scattering and Diffraction; 2.4 Experimental Methods; 2.5 STRUCTURE SOLUTION; 2.6 Structure Refinement; 2.7 Problem Structures, Special Topics, Validation and Interpretation 327 $aSoftware AcknowledgementsReferences; Chapter 3: PDF Analysis of Nanoparticles; 3.1 INTRODUCTION; 3.2 PAIR DISTRIBUTION FUNCTION; 3.3 DATA COLLECTION STRATEGIES; 3.4 DATA TREATMENT; 3.5 EXAMPLES; 3.6 COMPLEMENTARY TECHNIQUES; References; Chapter 4: Electron Crystallography; 4.1 INTRODUCTION; 4.2 CRYSTAL DESCRIPTION; 4.3 ELECTRON MICROSCOPY; 4.4 ELECTRON DIFFRACTION; 4.5 IMAGING; 4.6 THE EC METHOD OF SOLVING CRYSTAL STRUCTURES; 4.7 OTHER TEM TECHNIQUES; 4.8 CONCLUSION; References; ACKNOWLEDGMENT; Chapter 5: Small-Angle Scattering; 5.1 INTRODUCTION; 5.2 GENERAL PRINCIPLES OF SAS 327 $a5.3 INSTRUMENTAL SET-UP FOR SAXS5.4 INSTRUMENTAL SET-UP FOR SANS; 5.5 ADDITIONAL REQUIREMENTS FOR SAS; 5.6 APPLICATION OF SAS METHODS; 5.7 CONCLUSION; Acknowledgements; References; Index; End User License Agreement 330 $a"Part of the highly successful Inorganic Materials Series, this new title deals with recent advances in the characterisation of crystalline materials. This very timely volume complements the Series which has so far focused on particular classes of materials (synthesis, structures, chemistry and properties) by introducing and reviewing state-of-art techniques for materials characterisation.Written by experts from around the world, methods reviewed include spectroscopic, diffraction and surface techniques that examine the structure of materials on all length scales, from local atomic structure to long-range crystallographic order"--$cProvided by publisher. 330 $a"Part of the successful Inorganic Materials Series, this is a unique collection of books which provide an up-to-date review of key aspects of materials chemistry"--$cProvided by publisher. 410 0$aInorganic materials series. 606 $aMolecular structure 606 $aX-rays$xDiffraction 606 $aInorganic compounds$xSpectra 615 0$aMolecular structure. 615 0$aX-rays$xDiffraction. 615 0$aInorganic compounds$xSpectra. 676 $a541/.22 686 $aTEC021000$2bisacsh 702 $aBruce$b Duncan W. 702 $aO'Hare$b Dermot 702 $aWalton$b Richard I. 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910132191903321 996 $aStructure from diffraction methods$91920122 997 $aUNINA