LEADER 05708nam 2200757 450 001 9910132159203321 005 20230803072840.0 010 $a1-118-90779-5 010 $a1-118-90792-2 010 $a1-118-90791-4 035 $a(CKB)3710000000218272 035 $a(EBL)1765098 035 $a(SSID)ssj0001289002 035 $a(PQKBManifestationID)11774762 035 $a(PQKBTitleCode)TC0001289002 035 $a(PQKBWorkID)11294572 035 $a(PQKB)10873027 035 $a(OCoLC)868150756 035 $a(MiAaPQ)EBC1765098 035 $a(DLC) 2014001128 035 $a(Au-PeEL)EBL1765098 035 $a(CaPaEBR)ebr10907560 035 $a(CaONFJC)MIL637330 035 $a(PPN)196496918 035 $a(EXLCZ)993710000000218272 100 $a20140820h20142014 uy 0 101 0 $aeng 135 $aurcnu|||||||| 181 $ctxt 182 $cc 183 $acr 200 00$aHigh throughput analysis for food safety /$fedited by Perry G. Wang, Mark F. Vitha, Jack F. Kay 210 1$aHoboken, New Jersey :$cWiley,$d2014. 210 4$d©2014 215 $a1 online resource (300 p.) 225 1 $aChemical Analysis ;$v179 225 1 $aTHEi Wiley ebooks 300 $aIncludes index. 311 $a1-118-39630-8 320 $aIncludes bibliographical references at the end of each chapters and index. 327 $aHigh-Throughput Analysis for Food Safety; Contents; Preface; Contributors; Chapter 1: Introduction: Basic Principles of Assays to be Covered, Sample Handling, and Sample Processing; 1.1 Introduction; 1.1.1 Current Situation and Challenges of Food Safety and Regulations; 1.1.2 Residues and Matrices of Food Analysis and High-Throughput Analysis; 1.1.3 Food Safety Classifications; 1.1.4 "High Throughput" Definition; 1.1.5 Scope of the Book; 1.2 Advanced Sample Preparation Techniques; 1.2.1 Automation of Weighing and Preparing Standard Solutions; 1.2.2 QuEChERS 327 $a1.2.3 Swedish Extraction Technique (SweEt) and Other Fast Sample Preparation Methods 1.2.4 Turbulent Flow Chromatography; 1.2.5 Pressurized Liquid Extraction; 1.2.6 Automated 96- and 384-Well Formatted Sample Preparation as well as Automated SPE Workstations; 1.2.7 Solid-Phase Microextraction; 1.2.8 Microextraction by Packed Sorbent; 1.2.9 Liquid Extraction Surface Analysis; 1.2.10 Headspace GC; 1.2.11 Summary; 1.3 Future Perspectives; Acknowledgment; References; Chapter 2: Survey of Mass Spectrometry-Based High-Throughput Methods in Food Analysis; 2.1 Introduction 327 $a2.2 Techniques Employing Chromatographic Separation 2.2.1 Gas Chromatography-Mass Spectrometry; 2.2.2 Liquid Chromatography-Mass Spectrometry; 2.3 Direct Techniques; 2.3.1 Matrix-Assisted Laser Desorption/ Ionization-Mass Spectrometry; 2.3.2 Headspace (Solid-Phase Microextraction)- Mass Spectrometry E-Nose; 2.3.3 Ambient Desorption/Ionization-Mass Spectrometry; 2.4 Concluding Remarks; Acknowledgments; References; Chapter 3: Quality Systems, Quality Control Guidelines and Standards, Method Validation, and Ongoing Analytical Quality Control; 3.1 Introduction; 3.1.1 Quality System Design 327 $a3.1.2 Procedures 3.1.3 Roles and Responsibilities; 3.1.4 Quality Manual; 3.1.5 Document Control; 3.1.6 Control of Records; 3.1.7 Audits; 3.1.8 Validation of Methodology; 3.1.9 Staff Competency; 3.1.10 Internal Quality Control; 3.1.11 Method Performance Criteria; 3.2 Qualitative Screening Methods; 3.2.1 Selectivity of Mass Spectrometry-Based Methods; 3.2.2 Confirmatory Methods; 3.2.3 Validation of Qualitative Screening Multiresidue Methods for Pesticide Residues in Foods; 3.3 Elements of the Analytical Workflow; 3.3.1 Sample Preparation; 3.3.2 Effects of Sample Processing 327 $a3.3.3 Extraction Efficiency 3.4 Initial Method Validation; 3.5 Ongoing Analytical Quality Control; 3.5.1 Internal Quality Control; 3.5.2 Proficiency Testing; 3.6 Validation of Qualitative Screening Multiresidue Methods for Veterinary Drug Residues in Foods; 3.6.1 EU Legislation Covering Method Validation for Veterinary Drug Screening; 3.6.2 Determination of Specificity/Selectivity and Detection Capability (CCß) Using the Classical Approach; 3.6.3 Establishment of a Cutoff Level and Calculation of CC?; 3.6.4 Determination of the Applicability; 3.7 Conclusions; References 327 $aChapter 4: Deliberate Chemical Contamination and Processing Contamination 330 $aThis book focuses on high-throughput analyses for food safety. Because of the contributors domestic and international expertise from industry and government the book appeals to a wider audience. It includes the latest development in rapid screening, with a particular emphasis on the growing use and applicability of a variety of stand-alone mass spectrometry methods as well as using mass spectrometry in hyphenated techniques such as gas chromatograph mass spectrometry (GC-MS) and liquid chromatography mass spectrometry (LC-MS). Readers will be educated to the field of food safety and rapid test 410 0$aChemical analysis ;$v179. 410 0$aTHEi Wiley ebooks. 606 $aFood$xSafety measures 606 $aFood$xSafety measures$xGovernment policy 606 $aFood adulteration and inspection 615 0$aFood$xSafety measures. 615 0$aFood$xSafety measures$xGovernment policy. 615 0$aFood adulteration and inspection. 676 $a363.19/26 702 $aWang$b Perry G. 702 $aVitha$b Mark F. 702 $aKay$b Jack F. 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910132159203321 996 $aHigh throughput analysis for food safety$92125653 997 $aUNINA