LEADER 00771nam0-22002771i-450 001 990005058440403321 005 20230123082515.0 035 $a000505844 035 $aFED01000505844 035 $a(Aleph)000505844FED01 100 $a19990530g19539999km-y0itay50------ba 101 0 $aita 102 $aIT 105 $ay-------001yy 200 1 $aSaggi$eCon una noterella$ePoliziano - Parini - Alfieri...$fGiuseppe De Robertis 205 $a2.a ed. 210 $aFirenze$cLe Monnier$d1953 215 $a207 p.$d19 cm 700 1$aDe Robertis,$bGiuseppe$f<1888-1963>$0151750 801 0$aIT$bUNINA$gRICA$2UNIMARC 901 $aBK 912 $a990005058440403321 952 $aIX DR 4$bFil.Mod. 15285$fFLFBC 959 $aFLFBC 996 $aSaggi$9131165 997 $aUNINA LEADER 05433nam 2200733 a 450 001 9910966468803321 005 20240514235038.0 010 $a9786613680785 010 $a9781280770012 010 $a1280770015 010 $a9780123855411 010 $a0123855411 035 $a(CKB)2670000000193862 035 $a(EBL)943706 035 $a(OCoLC)796466990 035 $a(SSID)ssj0000676098 035 $a(PQKBManifestationID)12229126 035 $a(PQKBTitleCode)TC0000676098 035 $a(PQKBWorkID)10677010 035 $a(PQKB)10833114 035 $a(Au-PeEL)EBL943706 035 $a(CaPaEBR)ebr10571152 035 $a(CaONFJC)MIL368078 035 $z(PPN)18257153X 035 $a(PPN)170601595 035 $a(FR-PaCSA)88811767 035 $a(MiAaPQ)EBC943706 035 $a(FRCYB88811767)88811767 035 $a(EXLCZ)992670000000193862 100 $a20120413d2012 uy 0 101 0 $aeng 135 $aurcn||||||||| 181 $ctxt 182 $cc 183 $acr 200 10$aGas chromatography /$fColin F. Poole 205 $a1st ed. 210 $aAmsterdam ;$aBoston $cElsevier$d2012 215 $a1 online resource (753 p.) 300 $aDescription based upon print version of record. 311 08$a9780123855404 311 08$a0123855403 320 $aIncludes bibliographical references and index. 327 $aFront Cover; Gas Chromatography; Copyright; Contents; Contributors; Chapter 1 - Milestones in the Development of Gas Chromatography; 1.1.INTRODUCTION; 1.2.THE INVENTION OF GAS CHROMATOGRAPHY; 1.3.EARLY INSTRUMENTATION; 1.4.EARLY COLUMN DEVELOPMENTS; 1.5.INTERFACING GLASS CAPILLARY COLUMNS TO INJECTORS AND DETECTORS; 1.6.THE HINDELANG CONFERENCES AND THE FUSED-SILICA COLUMN; 1.7.INCREASING SOPHISTICATION OF INSTRUMENTATION; 1.8.DECLINE IN THE EXPERTISE OF THE AVERAGE GAS CHROMATOGRAPHER; References; Chapter 2 - Theory of Gas Chromatography; 2.1.INTRODUCTION 327 $a2.2.NOMENCLATURE AND OTHER CONVENTIONS 2.3.GENERAL DEFINITIONS; 2.4.SOLUTE-COLUMN INTERACTION; 2.5.PROPERTIES OF AN IDEAL GAS; 2.6.FLOW OF IDEAL GAS IN OPEN CIRCULAR TUBES; 2.7.MIGRATION AND ELUTION PARAMETERS OF THE SOLUTES; 2.8.PEAK SPACING AND REVERSAL OF PEAK ORDER; 2.9.PEAK WIDTH; 2.10.OPTIMIZATION; References; Chapter 3 - Column Technology: Open Tubular Columns; 3.1.INTRODUCTION; 3.2.OVERVIEW OF THE FUSED SILICA DRAWING PROCESS; 3.3.THE PREFORM - RAW MATERIAL; 3.4.SURFACE CHEMISTRY; 3.5.DRAWING OF THE CAPILLARY FROM THE PREFORM; 3.6.PROTECTIVE COATING; 3.7.ALTERNATIVE PROTECTIVE COATINGS 327 $a3.8. CLEAN ROOM ENVIRONMENT 3.9.QUALITY MONITORING; 3.10.OBSERVATIONS ON HANDLING OF FUSED-SILICA CAPILLARY TUBING; 3.11.COLUMN TECHNOLOGY - COATING THE STATIONARY PHASE; 3.12.STATIONARY PHASES; 3.13.COATING TECHNIQUES; 3.14.COLUMN TECHNOLOGY - QUALITY EVALUATION; 3.15.COLUMN TECHNOLOGY - SUMMARY; References; Chapter 4- Packed Columns for Gas-Liquid and Gas-Solid Chromatography; 4.1.INTRODUCTION; 4.2.GAS-LIQUID CHROMATOGRAPHY; 4.3.GAS-SOLID CHROMATOGRAPHY; References; Chapter 5 - Gas-Solid Chromatography (PLOT Columns); 5.1.ALUMINA ADSORBENTS; 5.2.MOLECULAR SIEVES; 5.3.POROUS POLYMERS 327 $a5.4.CARBON ADSORBENTS 5.5.OTHER ADSORBENTS; References; Chapter 6- Classification and Selection of Open-Tubular Columns for Analytical Separations; 6.1.INTRODUCTION; 6.2.STATIONARY-PHASE CLASSIFICATION; 6.3.POROUS-LAYER OPEN-TUBULAR COLUMNS; 6.4.TEMPERATURE-PROGRAMMED SEPARATIONS; 6.5.STATIONARY-PHASE SELECTIVITY TUNING; References; Chapter 7 - Multidimensional and Comprehensive Gas Chromatography; 7.1.INTRODUCTION; 7.2.A GRAPHICAL REPRESENTATION OF 2D GC SEPARATIONS; 7.3 .BACK FLUSHING 2D GC; 7.4.HEART CUTTING 2D GC; 7.5.COMPREHENSIVE 2D GC; 7.6.CONCLUSIONS; References 327 $aChapter 8 - Sample Introduction Methods 8.1.INTRODUCTION; 8.2.CHOOSING A SAMPLE INTRODUCTION SYSTEM; 8.3.SUPPORTING DEVICES; 8.4.THE COLD ON-COLUMN INJECTOR; 8.5.THE FLASH VAPORIZATION INJECTOR; 8.6.THE SPLIT/SPLITLESS INJECTOR; 8.7.THE PROGRAMMABLE TEMPERATURE VAPORIZING (PTV) INJECTOR; 8.8.THE GAS SAMPLING VALVE; 8.9.THE LIQUID SAMPLING VALVE; References; Chapter 9 - Head space-Gas Chromatography; 9.1.INTRODUCTION AND HISTORY; 9.2.FUNDAMENTALS OF HEAD SPACE EXTRACTION; 9.3.INSTRUMENTATION AND PRACTICE; 9.4.METHOD DEVELOPMENT CONSIDERATIONS; 9.5.CONCLUSIONS; References 327 $aChapter 10- Thermal Desorption for Gas Chromatography 330 $aThis title provides comprehensive coverage of modern gas chromatography including theory, instrumentation, columns, and applications addressing the needs of advanced students and professional scientists in industry and government laboratories. Chapters are written by recognized experts on each topic. Each chapter offers a complete picture with respect to its topic so researchers can move straight to the information they need without reading through a lot of background information.Individual chapters written by recognized experts The big picture of gas chromatography 606 $aGas chromatography 606 $aChromatographic analysis 615 0$aGas chromatography. 615 0$aChromatographic analysis. 676 $a543/.85 676 $a543.85 700 $aPoole$b Colin F$015291 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910966468803321 996 $aGas chromatography$94336155 997 $aUNINA