05149nam 2200625Ia 450 99621797570331620230421044537.01-281-75873-697866117587383-527-61563-63-527-61562-8(CKB)1000000000375885(EBL)482364(OCoLC)261224152(SSID)ssj0000183549(PQKBManifestationID)11179826(PQKBTitleCode)TC0000183549(PQKBWorkID)10195893(PQKB)11742837(MiAaPQ)EBC482364(EXLCZ)99100000000037588519941025d1995 uy 0engur|n|---|||||txtccrIon chromatography[electronic resource] /Joachim Weiss ; [translator, Jörg Mönig]2nd ed.Weinheim ;New York VCHc19951 online resource (479 p.)Description based upon print version of record.3-527-28698-5 Includes bibliographical references (p. [443]-453) and index.Ion Chromatography; Contents; 1 Introduction; 1.1 Historical Perspective; 1.2 Types of Ion Chromatography; 1.3 The Ion Chromatographic System; 1.4 Advantages of Ion Chromatography; 1.5 Selection of Separation and Detection Systems; 2 Theory of Chromatography; 2.1 Chromatographic Terms; 2.2 Parameters for Assessing the Quality of a Separation; 2.3 Column Efficiency; 2.4 The Concept of Theoretical Plates (van Deemter Theory); 2.5 van Deemter Curves in Ion Chromatography; 3 Ion-Exchange Chromatography (HPIC); 3.0 General Remarks; 3.1 The Ion-Exchange Process; 3.2 Thermodynamic Aspects3.3 Anion Exchange Chromatography3.3.1 Stationary Phases; 3.3.1.1 Polymer-Based Anion Exchangers; 3.3.1.2 Latex-Agglomerated Anion Exchangers; 3.3.1.3 Silica-Based Anion Exchangers; 3.3.1.4 Other Materials for Anion Separations; 3.3.2 Eluents for Anion Exchange Chromatography; 3.3.3 Suppressor Systems in Anion Exchange Chromatography; 3.3.4 Ion-Exchange Chromatography of Inorganic Anions; 3.3.4.1 General Parameters Affecting Retention; 3.3.4.2 Experimental Parameters Affecting Retention when Applying Suppressor Systems3.3.4.3 Experimental Parameters Affecting Retention when Applying Direct Conductivity Detection3.3.4.4 Polarizable Anions; 3.3.5 Ion-Exchange Chromatography of Organic Anions; 3.3.5.1 Organic Acids; 3.3.5.2 Polyvalent Anions; 3.3.5.3 Carbohydrates; 3.3.5.4 Oligosaccharides Derived from Glycoproteins; 3.3.6 Gradient Elution Techniques in Anion Exchange Chromatography; 3.4 Cation Exchange Chromatography; 3.4.1 Stationary Phases; 3.4.1.1 Polymer-Based Cation Exchangers; 3.4.1.2 Latexed Cation Exchangers; 3.4.1.3 Silica-Based Cation Exchangers; 3.4.2 Eluents in Cation Exchange Chromatography3.4.3 Suppressor Systems in Cation Exchange Chromatography3.4.4 Cation Exchange Chromatography of Alkali Metals, Alkaline-Earth Metals, and Amines; 3.4.5 Analysis of Heavy and Transition Metals; 3.4.5.1 Basic Theory; 3.4.5.2 Analysis of Heavy and Transition Metals by Direct Conductivity Detection; 3.4.5.3 Analysis of Heavy and Transition Metals with Spectrophotometric Detection; 3.4.6 Analysis of Polyamines; 4 Ion-Exclusion Chromatography (HPICE); 4.1 The Ion-Exclusion Process; 4.2 Stationary Phases; 4.3 Eluents for Ion-Exclusion Chromatography4.4 Suppressor Systems in Ion-Exclusion Chromatography4.5 Analysis of Inorganic Acids; 4.6 Analysis of Organic Acids; 4.7 HPICE/HPIC-Coupling; 4.8 Analysis of Alcohols and Aldehydes; 4.9 Analysis of Amino Acids; 4.9.1 Separation of Amino Acids; 4.9.2 Detection of Amino Acids; 4.9.3 Sample Preparation; 5 Ion-Pair Chromatography (MPIC); 5.1 Survey of Existing Retention Models; 5.2 Suppressor Systems in Ion-Pair Chromatography; 5.3 Experimental Parameters that Affect Retention; 5.3.1 Type and Concentration of Lipophilic Counter Ions in the Mobile Phase5.3.2 Type and Concentration of the Organic ModifierThis all-new edition of the highly successful first edition contains a wealth of up-to-date information on this major analytical technique. Ion-exchange, ion-exclusion, and ion-pair chromatography are treated together with their detection methods, and a discussion of quantitative analysis is also given. The complete range of application possibilities of this technique is described and illustrated with numerous chromatograms. Special chapters are featured on applications in environmental analysis, clinical chemistry as well as in the food and beverage industry. From reviews of previous Ion exchange chromatographyChromatographic analysisIon exchange chromatography.Chromatographic analysis.543.0893543.82Weiss Joachim882859MiAaPQMiAaPQMiAaPQBOOK996217975703316Ion chromatography2860590UNISA