04538nam 2200721 a 450 991097166300332120220712133127.097866131710789781283171076128317107497800809201530080920152(CKB)2670000000074980(EBL)670206(OCoLC)727648625(SSID)ssj0000492006(PQKBManifestationID)12174850(PQKBTitleCode)TC0000492006(PQKBWorkID)10478798(PQKB)11109751(Au-PeEL)EBL670206(CaPaEBR)ebr10483481(CaONFJC)MIL317107(PPN)182574601(PPN)170599825(FR-PaCSA)88812116(MiAaPQ)EBC670206(FRCYB88812116)88812116(EXLCZ)99267000000007498020100715d2011 uy 0engurcn|||||||||txtccrGas chromatography and mass spectrometry a practical guide /O. David Sparkman, Zelda E. Penton, Fulton G. Kitson2nd ed.Boston Elsevier20111 online resource (633 p.)Description based upon print version of record.9780080438016 0080438016 9780123736284 0123736285 Includes bibliographical references and index.The fundamentals of GC/MS -- Introduction and history -- Gas chromatography -- The gc/ms interface -- Mass spectrometry instrumentation -- Mass spectral data interpretation -- Quantitation with GC/MS -- GC conditions, derivatization, and mass spectral interpretation -- Of specific compound types -- Acids -- Alcohols -- Aldehydes -- Amides -- Amines -- Amino acid -- Common contaminants -- Drugs and their metabolites -- Esters -- Ethers -- Fluorinated compounds -- Gases -- Glycols -- Halogenated compounds (other than fluorinated) -- Hydrocarbons -- Isocyanates -- Ketones -- Nitriles -- Nitroaromatics -- Nitrogen-containing heterocyclics -- Nucleosides (TMS derivatives) -- Pesticides -- Phenols -- Phosphorus compounds -- Plasticizers and other polymer additives (including phthalates) -- Prostaglandins (MO-TMS derivatives) -- Solvents and their impurities -- Steroids -- Sugars (monosaccharides) -- Sulfur compounds -- Appendices -- A definitions of terms related to gas chromatography -- B definitions of terms related to mass spectrometry -- C atomic masses and isotope abundances -- X+1 and x+2 values for ions containing atoms of C and H based on -- Isotope contributions -- E isotope peak patterns for ions containing atoms of Cl and/or Br -- F steps to follow in the determination of an elemental composition -- Based on isotope peak intensity ratios -- G derivatization in GC/MS -- H points of comparison of LC/MS vs GC/MS -- I list of available EI mass spectral databases -- J information required for reporting a GC/MS analysis -- K third-party software for use with GC/MS -- GC installation and maintenance -- Troubleshooting common GC problems -- N maintenance, operating tips, and troubleshooting for mass spectrometers -- O mixtures for determining mass spectral resolution -- P cross-index chart for GC stationary phases -- Q ions for determining unknown structures.The second edition of Gas Chromatography and Mass Spectrometry: A Practical Guide follows the highly successful first edition by F.G. Kitson, B.S. Larsen, and C.N. McEwen (1996), which was designed as an indispensable resource for GC/MS practitioners regardless of whether they are a novice or well experienced. The Fundamentals section has been extensively reworked from the original edition to give more depth of an understanding of the techniques and science involved with GC/MS. Even with this expansion, the original brevity and simple didactic style has been retained. Information onGas chromatographyMass spectrometryGas chromatography.Mass spectrometry.543/.85543.85Sparkman O. David(Orrin David),1942-447425Penton Zelda1798142Kitson Fulton G67140MiAaPQMiAaPQMiAaPQBOOK9910971663003321Gas chromatography and mass spectrometry4340770UNINA