05433nam 2200733 a 450 991096646880332120240514235038.097866136807859781280770012128077001597801238554110123855411(CKB)2670000000193862(EBL)943706(OCoLC)796466990(SSID)ssj0000676098(PQKBManifestationID)12229126(PQKBTitleCode)TC0000676098(PQKBWorkID)10677010(PQKB)10833114(Au-PeEL)EBL943706(CaPaEBR)ebr10571152(CaONFJC)MIL368078(PPN)18257153X(PPN)170601595(FR-PaCSA)88811767(MiAaPQ)EBC943706(FRCYB88811767)88811767(EXLCZ)99267000000019386220120413d2012 uy 0engurcn|||||||||txtccrGas chromatography /Colin F. Poole1st ed.Amsterdam ;Boston Elsevier20121 online resource (753 p.)Description based upon print version of record.9780123855404 0123855403 Includes bibliographical references and index.Front Cover; Gas Chromatography; Copyright; Contents; Contributors; Chapter 1 - Milestones in the Development of Gas Chromatography; 1.1.INTRODUCTION; 1.2.THE INVENTION OF GAS CHROMATOGRAPHY; 1.3.EARLY INSTRUMENTATION; 1.4.EARLY COLUMN DEVELOPMENTS; 1.5.INTERFACING GLASS CAPILLARY COLUMNS TO INJECTORS AND DETECTORS; 1.6.THE HINDELANG CONFERENCES AND THE FUSED-SILICA COLUMN; 1.7.INCREASING SOPHISTICATION OF INSTRUMENTATION; 1.8.DECLINE IN THE EXPERTISE OF THE AVERAGE GAS CHROMATOGRAPHER; References; Chapter 2 - Theory of Gas Chromatography; 2.1.INTRODUCTION2.2.NOMENCLATURE AND OTHER CONVENTIONS 2.3.GENERAL DEFINITIONS; 2.4.SOLUTE-COLUMN INTERACTION; 2.5.PROPERTIES OF AN IDEAL GAS; 2.6.FLOW OF IDEAL GAS IN OPEN CIRCULAR TUBES; 2.7.MIGRATION AND ELUTION PARAMETERS OF THE SOLUTES; 2.8.PEAK SPACING AND REVERSAL OF PEAK ORDER; 2.9.PEAK WIDTH; 2.10.OPTIMIZATION; References; Chapter 3 - Column Technology: Open Tubular Columns; 3.1.INTRODUCTION; 3.2.OVERVIEW OF THE FUSED SILICA DRAWING PROCESS; 3.3.THE PREFORM - RAW MATERIAL; 3.4.SURFACE CHEMISTRY; 3.5.DRAWING OF THE CAPILLARY FROM THE PREFORM; 3.6.PROTECTIVE COATING; 3.7.ALTERNATIVE PROTECTIVE COATINGS3.8. CLEAN ROOM ENVIRONMENT 3.9.QUALITY MONITORING; 3.10.OBSERVATIONS ON HANDLING OF FUSED-SILICA CAPILLARY TUBING; 3.11.COLUMN TECHNOLOGY - COATING THE STATIONARY PHASE; 3.12.STATIONARY PHASES; 3.13.COATING TECHNIQUES; 3.14.COLUMN TECHNOLOGY - QUALITY EVALUATION; 3.15.COLUMN TECHNOLOGY - SUMMARY; References; Chapter 4- Packed Columns for Gas-Liquid and Gas-Solid Chromatography; 4.1.INTRODUCTION; 4.2.GAS-LIQUID CHROMATOGRAPHY; 4.3.GAS-SOLID CHROMATOGRAPHY; References; Chapter 5 - Gas-Solid Chromatography (PLOT Columns); 5.1.ALUMINA ADSORBENTS; 5.2.MOLECULAR SIEVES; 5.3.POROUS POLYMERS5.4.CARBON ADSORBENTS 5.5.OTHER ADSORBENTS; References; Chapter 6- Classification and Selection of Open-Tubular Columns for Analytical Separations; 6.1.INTRODUCTION; 6.2.STATIONARY-PHASE CLASSIFICATION; 6.3.POROUS-LAYER OPEN-TUBULAR COLUMNS; 6.4.TEMPERATURE-PROGRAMMED SEPARATIONS; 6.5.STATIONARY-PHASE SELECTIVITY TUNING; References; Chapter 7 - Multidimensional and Comprehensive Gas Chromatography; 7.1.INTRODUCTION; 7.2.A GRAPHICAL REPRESENTATION OF 2D GC SEPARATIONS; 7.3 .BACK FLUSHING 2D GC; 7.4.HEART CUTTING 2D GC; 7.5.COMPREHENSIVE 2D GC; 7.6.CONCLUSIONS; ReferencesChapter 8 - Sample Introduction Methods 8.1.INTRODUCTION; 8.2.CHOOSING A SAMPLE INTRODUCTION SYSTEM; 8.3.SUPPORTING DEVICES; 8.4.THE COLD ON-COLUMN INJECTOR; 8.5.THE FLASH VAPORIZATION INJECTOR; 8.6.THE SPLIT/SPLITLESS INJECTOR; 8.7.THE PROGRAMMABLE TEMPERATURE VAPORIZING (PTV) INJECTOR; 8.8.THE GAS SAMPLING VALVE; 8.9.THE LIQUID SAMPLING VALVE; References; Chapter 9 - Head space-Gas Chromatography; 9.1.INTRODUCTION AND HISTORY; 9.2.FUNDAMENTALS OF HEAD SPACE EXTRACTION; 9.3.INSTRUMENTATION AND PRACTICE; 9.4.METHOD DEVELOPMENT CONSIDERATIONS; 9.5.CONCLUSIONS; ReferencesChapter 10- Thermal Desorption for Gas ChromatographyThis title provides comprehensive coverage of modern gas chromatography including theory, instrumentation, columns, and applications addressing the needs of advanced students and professional scientists in industry and government laboratories. Chapters are written by recognized experts on each topic. Each chapter offers a complete picture with respect to its topic so researchers can move straight to the information they need without reading through a lot of background information.Individual chapters written by recognized experts The big picture of gas chromatographyGas chromatographyChromatographic analysisGas chromatography.Chromatographic analysis.543/.85543.85Poole Colin F15291MiAaPQMiAaPQMiAaPQBOOK9910966468803321Gas chromatography4336155UNINA