04989nam 2200673Ia 450 991087673130332120200520144314.01-280-54194-697866105419420-471-65367-50-471-65368-3(CKB)111090529069414(EBL)183854(SSID)ssj0000179658(PQKBManifestationID)11177655(PQKBTitleCode)TC0000179658(PQKBWorkID)10138030(PQKB)10643124(MiAaPQ)EBC183854(OCoLC)85820551(PPN)243218214(EXLCZ)9911109052906941420750907d2004 uy 0engur|n|---|||||txtccrInorganic synthesesVolume 34 /editor-in-chief John R. ShapleyNew York [etc.] Wiley [etc.]20041 online resource (284 p.)Inorganic Syntheses ;v.68Description based upon print version of record.0-471-64750-0 Includes bibliographical references and index.INORGANIC SYNTHESES Volume 34; PREFACE; NOTICE TO CONTRIBUTORS AND CHECKERS; TOXIC SUBSTANCES AND LABORATORY HAZARDS; CONTENTS; Chapter One MAIN GROUP COMPOUNDS; 1. Diborane(4) Compounds; A. Tetrakis(dimethylamino)diborane(4), B(2)(NMe(2))(4); B. 1,2-Dichloro-1,2-bis(dimethylamino)diborane(4), B(2)Cl(2)(NMe(2))(2); C. 2,2'-Bis(1,3,2-benzodioxaborole), B(2)(1,2-O(2)C(6)H(4))(2); 2. Sodium Tetrakis(3,5-bis(trifluoromethyl)phenyl)borate, Na[B(3,5-(CF(3))(2)C(6)H(3))(4)]; 3. Anionic Tris- and Bis(diphenylphosphinomethyl)boratesA. Tetrabutylammonium Phenyltris(diphenylphosphinomethyl)borate, [(n)Bu(4)N][PhB(CH(2)PPh(2))(3)]B. Tetrabutylammonium Diphenylbis(diphenylphosphinomethyl)borate, [(n)Bu(4)N][Ph(2)B(CH(2)PPh(2))(2)]; C. Thallium Phenyltris(diphenylphosphinomethyl)borate, [PhB(CH(2)PPh(2))(3)]Tl; 4. Six-Coordinate Aluminum Cations Based on Salen Ligands; A. Chloro-1,2-bis(2-hydroxybenzylideneimino)ethanealuminum, Al(Salen)Cl; B. Diaqua-1,2-bis(2-hydroxybenzylideneimino)ethanealuminum Chloride, [Al(Salen)(H(2)O)(2)]ClC. Dimethanol-1,2 bis-(2-hydroxy-3,5-bis(tert-butyl)benzylideneimino) Aluminum Chloride, [Al(Salen(t)Bu)(MeOH)(2)]ClD. Dimethanol-1,2-bis(2-hydroxy-3,5-bis(tert-butyl)benzylideneimino)ethanealuminum Tetraphenylborate, [Al((t)BuSalen)(MeOH)(2)][BPh(4)]; E. Dimethanol-1,2-bis(2-hydroxy-3,5-bis(tert-butyl)benzylideneimino)ethanealuminum para-Toluenesulfonate, [Al((t)BuSalen)(MeOH)(2)][OTs]; F. Bis(tetrahydrofuran)-1,2-bis(2-hydroxy-3,5-bis(tert-butyl)benzylideneimino)ethanealuminum Tetraphenylborate, [Al((t)BuSalen)(THF)(2)][BPh(4)]; 5. Tabular a-Alumina; 6. Para-Substituted Aryl IsocyanidesA. 1,4-Diisocyanobenzene, p-CNC(6)H(4)NCB. 1,4-Diisocyano-2,5-dimethylbenzene, p-CN(C(6)H(2)(CH(3))(2))NC; C. 1-Isocyano-4-methoxybenzene, p-CN(C(6)H(4))OCH(3); D. Bis(1,4-diisocyanobenzene)bis(1,2-bis(diphenylphosphino)ethane)tungsten(0), W(dppe)(2)(CNC(6)H(4)NC)(2); 7. Unsymmetric Tripod Ligands Related to Tris(pyrazol-1-yl)methane; A. Bis(pyrazol-1-yl)methanone, (pz)(2)C=O; B. N-Methylimidazole-2-carbaldehyde, (mim)CHO; C. Bis(pyrazol-1-yl)(pyridin-2-yl)methane, (pz)(2)(py)CH; D. Bis(pyrazol-1-yl)(N-methylimidazol-2-yl)methane, (pz)(2)(mim)CH; 8. Difluorotriphenylarsenic(V), AsF(2)Ph(3)9. Tetramethylammonium Salts of Superoxide and PeroxynitriteA. Tetramethylammonium Superoxide, [N(CH(3))(4)]O(2); B. Tetramethylammonium Peroxynitrite, [N(CH(3))(4)][ONOO]; 10. Tellurium-Nitrogen Compounds; A. Lithium tert-Butylamide, Li[HN(t)Bu]; B. Bis(m-tert-butylimido)-bis(tert-butylimido)ditellurium, (t)BuNTe(m-N(t)Bu)(2)TeN(t)Bu; C. Bis{dilithium[tris(tert-butylimido)tellurite]}, {Li(2)[Te(N(t)Bu)(3)]}(2); Chapter Two ORGANOMETALLIC AND COORDINATION COMPLEXES; 11. Addition Compounds of Dibromodioxomolybdenum(VI); A. Stock Solution of MoO(2)Br(2)(H(2)O)(2) in Diethyl EtherB. Diaquadibromodioxomolybdenum(VI) Diglyme Complex, MoO(2)Br(2)(H(2)O)(2)·diglymeThis series provides inorganic chemists with detailed and foolproof procedures for the preparation of important and timely compounds. Volume 34 continues to report such procedures with an up-to-date selection of contributions by internationally-recognized researchers, including the following:Inorganic SynthesesInorganic compoundsSynthesisChemistry, InorganicInorganic compoundsSynthesis.Chemistry, Inorganic.541.39541/.39547.2Shapley John R1761563American Chemical Society.MiAaPQMiAaPQMiAaPQBOOK9910876731303321Inorganic syntheses4201089UNINA