05151nam 2200649Ia 450 991014431340332120170810192827.01-282-30559-X97866123055970-470-13249-30-470-13284-1(CKB)1000000000376280(EBL)469354(OCoLC)808668866(SSID)ssj0000299761(PQKBManifestationID)11947457(PQKBTitleCode)TC0000299761(PQKBWorkID)10241577(PQKB)10927561(MiAaPQ)EBC469354(PPN)243094213(EXLCZ)99100000000037628020750907d1978 uy 0engur|n|---|||||txtccrInorganic synthesesVolume XVIII[electronic resource] /editor-in-chief Daryle H. BuschNew York Wiley19781 online resource (260 p.)Inorganic syntheses ;18Description based upon print version of record.0-471-03393-6 Includes bibliographical references and and index.INORGANIC SYNTHESES; CONTENTS; Notice to Contributors.; Toxic Substances.; Chapter One MACROCYCLIC LIGANDS AND THEIR METAL COMPLEXES; 1. 5,7,7,12,14,14-Hexamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene (5,7,7,12,14,14-Me6[14]-4,11-diene-1,4,8,11-N4) Complexes; A. 5,7,7,12,14,14-Hexamethyl-1,4,8,11-tetraazacyclotetraceca-4,11-diene Bis(trifluoromethanesulfonate).; B. 5,7,7,12,14,14-Hexamethyl-1,4,8,11-tetraazacyclotetraceca-4,11-diene Diperchlorate; C. [meso- and racemic-(5,7,7,12,14,14-hexamethyl-1,2,8,11-tetraazacyclotetradeca-4,11-diene)] nickel(II) PerchlorateD. Bis(acetonitrile)(5,7,7,12,14,14-hexamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene)iron(II) Trifluoromethanesulfonate2. 5,5,7,12,12,14-Hexamethyl-1,4,8,11-tetraazacyclotetradecane (5,5,7,12,12,14-Me6[14]ane-1,4,8,11-N4) Complexes; A. meso- and racernic-(5,5,7,12,12,14-Hexamethyl-1,4,8,11-tetraazacyclotetradecane) Hydrate; B. [meso-(5,5,7,12,12,14-Hexamethyl-1,4,8,11-tetraazacyclotetradecane)]-nickel(II) Perchlorate; C. Dibromo [rneso-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetra-decane)] cobalt(III) PerchlorateD. Bis(acetonitrile) [meso-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclo tetradecane)] iron(II) Trifluoromethanesulfonate3. 2,12-Dimethyl-3,7,11,17-tetraazabicyclo[11.3.1] heptadeca-1(17),2,11,13,15-pentaene (2,6-Me2-2',6':3,5-Pyo[14]-1,3,6-triene-1,4,7,11-N4) Complexes; A. (2,12-Dimethyl-3,7,11,17-tetraazabicyclo[11.3.11] heptadeca-1(17),2,11,13,15-pentaene)nickel(II) Perchlorate; B. Bromo(2,12-dimethyl-3,7,11,17-tetraazabicyclo[11.3.11] heptadeca-1(17),2,11,13,15-pentaene)cobalt(II) Bromide MonohydrateC. Dibromo(2,12-dimethyl-3,7,11,17-tetraazabicyclo[11.3.11] heptadeca-1(17),2,11,13,15-pentaene)cobalt(III) Bromide Monohydrate4. 2,3,9,10-Tetramethyl-1,4,8,11-tetraazacyclotetradeca-1,3,8,10-tetraene(2,3,9,10-Me4[14]-1,3,8,10-tetraene-1,4,8,11-N4) Complexes; A. (2,3,9,10-Tetramethyl-1,4,8,11-tetraazacyclotetradeca-1,3,8,10-tetraene)nickel(II) Perchlorate; B. Bis(isothiocyanato)(2,3,9,10-tetramethyl-1,4,8,11-tetraazacyclotetradeca-1,3,8,10-tetraene)nickel(II); C. Dibromo(2,3,9,10-tetramethyl-1,4,8,11-tetraazacyclotetradeca-1,3,8,10-tetraene)cobalt(III) Bromide5. 2,3-Dimethyl-1,4,8,11-tetraazacyclotetradeca-1,3-diene(2,3-Me2[14]-1,3-diene-1,4,8,11-N4)ComplexesA. (2,3-Dimethyl-1,4,8,11-tetraazacyclotetradeca-1,3-diene)nickel(II) Tetrachlorozincate(2-); B. Dibromo(2,3-dimethyl-1,4,8,11-tetraazacyclotetradeca-1,3-diene)-cobalt(III) Perchlorate; 6. Tetrabenzo[b,f,j,n][1,5,9,13] tetraazacyclohexadecine(2,3; 6,7; 10,11; 14,15-Bzo[16] octaene-1,5,9,13-N4) Complexes; A. (Tetrabenzo[b,f,j,n][1,5,9,13] tetraazacyclohexadecine)nickel(II) Perchlorate; B. Bis(isothiocyanato)(tetrabenzo[b,f,j,n][1,5,9,13] tetraazacyclohexadecine)nickel(II)C. (Tetrabenzo[b,f,j,n][1,5,9,13] tetraazacyclohexadecine)copper(II) NitrateThe volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.Inorganic SynthesesInorganic compoundsSynthesisChemistry, InorganicInorganic compoundsSynthesis.Chemistry, Inorganic.541.39541/.39Busch Daryle H(Daryle Hadley),1928-911774MiAaPQMiAaPQMiAaPQBOOK9910144313403321Inorganic syntheses2041745UNINA