05492nam 2200673Ia 450 991013976180332120230721022729.01-282-34957-097866123495770-470-74810-90-470-74809-5(CKB)1000000000793109(EBL)454319(OCoLC)609843806(SSID)ssj0000303312(PQKBManifestationID)11228539(PQKBTitleCode)TC0000303312(PQKBWorkID)10275197(PQKB)11599910(MiAaPQ)EBC454319(Au-PeEL)EBL454319(CaPaEBR)ebr10323387(CaONFJC)MIL234957(EXLCZ)99100000000079310920090423d2009 uy 0engur|n|---|||||txtccrMiniaturization of analytical systems[electronic resource] principles, designs and applications /Angel Rios, Alberto Escarpa, Bartolomé SimonetHoboken, N.J. Wiley20091 online resource (385 p.)Description based upon print version of record.0-470-06110-3 Includes bibliographical references and index.Miniaturization of Analytical Systems: Principles, Designs and Applications; Contents; Preface; 1 Miniaturization in Analytical Chemistry; 1.1 Introduction; 1.2 Miniaturization as One of the Critical Trends in Modern Analytical Chemistry; 1.3 Evolution in the Field of Analytical Miniaturization; 1.4 Classification of Miniaturized Analytical Systems and Definition of Terms; 1.5 Theory of Miniaturization; 1.6 Features of Miniaturized Analytical Systems; 1.7 Incidences of Miniaturization in the Analytical Process; 1.7.1 Miniaturization of the Steps of the Analytical Process1.7.2 Integrated (Micro)systems for the Performance of the Entire Analytical Process1.8 Outlook; References; 2 Tools for the Design of Miniaturized Analytical Systems; 2.1 Introduction; 2.2 Miniaturized Analytical Processes: The Downsizing and Integrating Phenomena; 2.2.1 Transport within Microfluidic Systems; 2.2.2 Microsystem Design from Transport Parameter Information; 2.3 Microfluidic Devices; 2.3.1 Microvalves; 2.3.2 Moving Liquids in Miniaturized Systems; 2.3.3 Mixers; 2.3.4 Volume-dispensing and Sample-introduction Devices; 2.3.5 Detection Systems for Analytical Microsystems2.4 Microtechnology2.4.1 Computer Simulations in Microfluidics; 2.4.2 Micromachining; 2.4.3 Packaging of Microsystems; 2.5 MEMS and NEMS; 2.5.1 Fabrication and Characterization; 2.5.2 Functionalization; 2.5.3 Detection Methods; 2.6 Outlook; References; 3 Automation and Miniaturization of Sample Treatment; 3.1 Introduction; 3.2 Simplification of Sample Treatment: Microextraction Techniques; 3.2.1 Calibration in Microextraction Processes; 3.2.2 Solid Phase Microextraction (SPME) Techniques; 3.2.3 Liquid Phase Microextraction (LPME) Techniques3.2.4 Comparison of Solid and Liquid Phase Microextraction Techniques3.3 Simplification of Sample Treatment: Continuous Flow Systems; 3.3.1 Coupling to Gas Chromatography; 3.3.2 Coupling to Liquid Chromatography; 3.3.3 Coupling to Capillary Electrophoresis (CE); References; 4 Miniaturized Systems for Analytical Separations I: Systems Based on a Hydrodynamic Flow; 4.1 Introduction; 4.2 The Earliest Example of Miniaturization of a Gas Chromatograph and Some Other Developments; 4.3 Capillary Liquid Chromatography (CLC); 4.4 Liquid Chromatography on Microchips; 4.4.1 The Agilent HPLC Chip4.4.2 Other Approaches to Microchip HPLC4.4.3 Some Selected Applications; References; 5 Miniaturized Systems for Analytical Separations II: Systems Based on Electroosmotic Flow (EOF); 5.1 Introduction; 5.2 CE on the Microchip Format; 5.3 Modes and Theories of CE Microchips; 5.4 Microfabrication Techniques; 5.4.1 Microfabrication of Glass CE Microchips; 5.4.2 Microfabrication of Polymer CE Microchips; 5.5 Basic Fluidic Manipulation/Motivation: Electrokinetic Injection and Separation Protocols; 5.6 Electrochromatography in Microchip Format: Designs and Applications5.7 Comparison of Hydrodynamic and Electroosmotic Flow-driven Miniaturized SystemsThe book describes a general vision of the miniaturization of the analytical systems, including their principles, designs and applications. Through ten chapters the different aspects characterizing the miniaturized systems are developed. Thus, the two first chapters include the basic concepts behind miniaturization in analytical chemistry, as well as the mechanical and electronic tools needed for designing and fabricating miniaturized analytical systems. Chapters 3 to 6 represent the core of the book, as they take as the basis the analytical process and deal with the miniaturization of sampleChemistry, AnalyticMiniature electronic equipmentChemistry, Analytic.Miniature electronic equipment.543543.22Ríos Castro Angel923199Escarpa Miguel Alberto1968-923200Simonet Bartolomé923201MiAaPQMiAaPQMiAaPQBOOK9910139761803321Miniaturization of analytical systems2071599UNINA