01346oam 2200409 450 991070404830332120180426124842.0(CKB)5470000002437172(OCoLC)1030746594(OCoLC)995470000002437172(EXLCZ)99547000000243717220180406d2013 ua 0engurmn|||||||||txtrdacontentcrdamediacrrdacarrierThe 3D Elevation Program summary for California /William J. Carswell, JrReston, VA :U.S. Department of the Interior, U.S. Geological Survey,2013.1 online resource (2 unnumbered pages) color illustrations, color mapFact sheet ;2013-3056"November 2013."Includes bibliographical references (page 2).3D Elevation Program Digital elevation modelsCaliforniaThree-dimensional imagingCaliforniaDigital elevation modelsThree-dimensional imagingCarswell William J.1387067Geological Survey (U.S.),GPOGPOGPOBOOK9910704048303321The 3D Elevation Program3436533UNINA06407nam 2200757 a 450 991013104540332120240516071034.0978661317504597812831750431283175045978047082831104708283159780470825174047082517097804708251810470825189(CKB)3460000000003402(EBL)711821(OCoLC)729726196(SSID)ssj0000476999(PQKBManifestationID)12141550(PQKBTitleCode)TC0000476999(PQKBWorkID)10502330(PQKB)11752915(MiAaPQ)EBC711821(Au-PeEL)EBL711821(CaPaEBR)ebr10484787(CaONFJC)MIL317504(Perlego)1012501(EXLCZ)99346000000000340220101203d2011 uy 0engur|n|---|||||txtccrInterpretation of organic spectra /by Yong-Cheng Ning1st ed.Hoboken, N.J. Wiley20111 online resource (426 p.)Description based upon print version of record.9780470825167 0470825162 Includes bibliographical references and index.Interpretation of Organic Spectra; Contents; Foreword; Preface; 1 Interpretation of 1H NMR Spectra; 1.1 Chemical Shift; 1.1.1 Conception of Chemical Shift; 1.1.2 Factors Affecting Chemical Shifts; 1.2 Coupling Constant J; 1.2.1 Coupling Effect and Coupling Constant J; 1.2.2 Discussion of Coupling Constants According to their Kinds; 1.3 Chemical Equivalence and Magnetic Equivalence; 1.3.1 Chemical Equivalence; 1.3.2 Magnetic Equivalence; 1.3.3 Classification of 1H Spectra; 1.4 Characteristics of the 1H Spectra of Some Functional Groups; 1.4.1 Substituted Phenyl Ring1.4.2 Substituted Heteroaromatic Ring1.4.3 Normal Long-chain Alkyl Group; 1.4.4 Carbonyl Compounds; 1.4.5 Reactive Hydrogen Atom; 1.4.6 Compounds Containing Fluorine or Phosphor Atoms; 1.5 Interpretation of 1H NMR Spectra; 1.5.1 Find Impurity Peaks, Pay Attention to the Solvent Applied; 1.5.2 Calculation of the Unsaturation Number of the Unknown Compound; 1.5.3 Determination of the Number of Hydrogen Atoms Corresponding to Every Peak Set in the 1H Spectrum; 1.5.4 Determination of Functional Groups of the Unknown Compound; 1.5.5 Analysis of Coupling Splittings of Peak Sets1.5.6 Combination of Possible Structural Units1.5.7 Assignment of the 1H spectrum According to the Deduced Structure; 1.5.8 Checking of the Deduced Structure; 1.6 Examples of 1H Spectrum Interpretation; Reference; 2 Interpretation of 13C NMR Spectra; 2.1 Characteristics and Advantages of the 13C NMR Spectra; 2.2 The Main Parameter of the 13C Spectrum is the Chemical Shift; 2.3 Chemical Shift Values of Common Functional Groups and Main Factors Affecting Chemical Shift Values; 2.3.1 Alkanes and their Derivatives; 2.3.2 Cycloalkanes and their Derivatives; 2.3.3 Alkylenes and their Derivatives2.3.4 Benzene and its Derivatives2.3.5 Carbonyl Groups; 2.4 Determination of the Carbon Atom Orders; 2.5 Steps for 13C NMR Spectrum Interpretation; 2.5.1 Recognizing Impurity Peaks and Identifying Solvent Peaks; 2.5.2 Calculation of the Unsaturation Number of the Unknown Compound; 2.5.3 Consideration of Chemical Shift Values of Peaks; 2.5.4 Determination of Carbon Atom Orders; 2.5.5 Postulation of Possible Functional Groups; 3 Interpretation of 2D NMR Spectra; 3.1 General Knowledge about 2D NMR Spectra; 3.2 Homonuclear Shift Correlation Spectroscopy, COSY (H, H-COSY)3.3 Heteronuclear Shift Correlation Spectroscopy3.4 Long-Range Heteronuclear Shift Correlation Spectroscopy; 3.5 NOESY and ROESY; 3.6 Total Correlation Spectroscopy, TOCSY; References; 4 Interpretation of Mass Spectra; 4.1 Basic Knowledge of Organic Mass Spectrometry; 4.1.1 Mass Spectra; 4.1.2 Ionization in Organic Mass Spectrometry; 4.1.3 Ion Types in Organic Mass Spectrometry; 4.2 Isotopic Ion Clusters in Mass Spectra; 4.3 Interpretation of EI MS; 4.3.1 Determination of Molecular Ion Peak; 4.3.2 Interpretation of Fragment Ion Peaks; 4.3.3 Interpretation of Rearrangement Ion Peaks4.3.4 Complex Cleavages of Alicyclic Compounds"Although there are a number of books in this field, most of them lack an introduction of comprehensive analysis of MS and IR spectra, and others do not provide up-to-date information like tandem MS. This book fills the gap. The merit of this book is that the author will not only introduce knowledge for analyzing nuclear magnetic resonance spectra including 1H spectra (Chapter 1), 13C spectra (Chapter 2) and 2D NMR spectra (Chapter 3), he also arms readers systemically with knowledge of Mass spectra (including EI MS spectra and MS spectra by using soft ionizations) (Chapter 4) and IR spectra (Chapter 5). In each chapter the author presents very practical application skills by providing various challenging examples. The last chapter (Chapter 6) provides the strategy, skills and methods on how to identify an unknown compound through a combination of spectra. Based on nearly 40 years researching and teaching experience, the author also proposes some original and creative ideas, which are very practical for spectral interpretation"--Provided by publisher."The merit of this book is that the author will not only introduce knowledge for analyzing nuclear magnetic resonance spectra including 1H spectra (Chapter 1), 13C spectra (Chapter 2) and 2D NMR spectra (Chapter 3), he also arms readers systemically with knowledge of Mass spectra (including EI MS spectra and MS spectra by using soft ionizations) (Chapter 4) and IR spectra (Chapter 5)"--Provided by publisher.Spectrum analysisOrganic compoundsAnalysisSpectrum analysis.Organic compoundsAnalysis.543/.5SCI078000bisacshNing Yong-Cheng518792MiAaPQMiAaPQMiAaPQBOOK9910131045403321Interpretation of organic spectra1990761UNINA