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1. |
Record Nr. |
UNINA9910144281403321 |
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Autore |
Rosowsky Andre |
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Titolo |
Seven-membered heterocyclic compounds containing oxygen and sulfur [[electronic resource] /] / edited by Andre Rosowsky |
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Pubbl/distr/stampa |
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New York, : Wiley-Interscience, 1972 |
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ISBN |
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1-282-30171-3 |
9786612301711 |
0-470-18696-8 |
0-470-18845-6 |
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Edizione |
[99th ed.] |
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Descrizione fisica |
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1 online resource (982 p.) |
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Collana |
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Chemistry of heterocyclic compounds ; ; v. 26 |
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Altri autori (Persone) |
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Disciplina |
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547.592 |
547/.59/05 |
547/.592 |
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Soggetti |
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Lingua di pubblicazione |
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Formato |
Materiale a stampa |
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Livello bibliografico |
Monografia |
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Note generali |
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Description based upon print version of record. |
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Nota di bibliografia |
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Includes bibliographical references. |
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Nota di contenuto |
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THE CHEMISTRY OF HETEROCYCLIC COMPOUNDS A SERIES OF MONOGRAPHS; Preface; Contents; Tables; I. Oxepins and Reduced Oxepins; A. OXEPINS; 1. Theoretical Interest; 2. Preparation; 3. Physical Properties; a. Infrared Absorption; b. Ultraviolet Absorption; c. Nuclear Magnetic Resonance; d. Thermodynamic Properties; 4. Chemical Reactions; a. Addendum; B. DIHYDROOXEPINS; 1. Introduction; 2. Preparation; 3. Physical Properties; a. Infrared Absorption; b. Ultraviolet Absorption; c. Nuclear Magnetic Resonance; 4. Chemical Reactions; C. TETRAHYDROOXEPINS; 1. Introduction; 2. Preparation |
3. Physical Propertiesa. Infrared Absorption; b. Nuclear Magnetic Resonance; 4. Chemical Reactions; D. HEXAHYDROOXEPINS (OXEPANS); 1. Preparation; a. Hexamethylene Oxide; b. Substituted Oxepans; (1) Ring Closure Reactions; (2) Ring Expansion Reactions; (3) Two-Component Reactions; 2. Physical Properties of Hexamethylene Oxide; 3. Chemical Reactions of Hexamethylene Oxide; 4. Preparation and Reactions of Cyclic Acetals, Ketals, and Related Compounds; E. TABLES; I-1. Oxepins and Reduced Oxepins; F. REFERENCES; II. Oxepin Ring |
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Systems Containing Two Rings; A. FUSED RINGS SYSTEMS |
1. 2-Oxabicyclo[5.1.0]octanes2. 2-Oxabicyclo[5.2.0]nonanes; 3. 2H-Cyclopent[b]oxepins; 4. 2H-Cyclopent[d]oxepins; 5. Furo[3,4-b]oxepins; 6. Furo[3,4-d]oxepins; 7. 2H-Oxepino[2,3-b]pyrroles; 8. Thieno[3,4-d]oxepins; 9.1-Benzoxepins; a. Synthesis, Chemical Reactions, and Physical Properties of the Parent Compound; b. Synthesis and Chemical Reactions of Dihydro-l-benzoxepins; c. Synthesis and Chemical Reactions of Tetrahydro-l- benzoxepins; d. Synthesis and Chemical Reactions of Other Reduced 1-Benzoxepins; e. Physicochemical Properties of 2,3,4,5-Tetrahydro-1- benzoxepins; 10.2-Benzoxepins |
11. 3-BenzoxepinsB. SPIRANS; 1. 1,7-Dioxaspiro[5.6]dodecanes; 2. 1,4,6-Trioxaspiro[4.6]undecanes; C. BRIDGED SYSTEMS; 1. 2-Oxabicyclo[3.2.2]nonanes; 2. 3-Oxabicyclo[3.2.2]nonanes; 3. 9-Oxabicyclo[3.3.2]decanes; 4. 11-Oxabicyclo[4.4.1]undecanes; a. Partly or Fully Saturated Derivatives; b. 1,6-Oxido[10]annulenes; 5. 3-Oxa-6,7-dithiabicyclo[3.2.2]nonanes; D. TABLES; II-1. Uv Data and Bromination Rate of 2,3,4,5-Tetrahydro-l-benzoxepins and Lower Ring Homologs; II-2. Solvolysis Kinetics of 7-Chloromethyl-2,3,4,5-tetrahydro-l- benzoxepin and Lower Ring Homologs |
II-3. Uv Data and Bromination Rate of 2,3,4,5-Tetrahydro-l- benzoxepin-2-carboxylic Acid and Lower Ring HomologsII-4. Uv Data and Molecular Geometry of 2,3,4,5-Tetrahydro-2-(N,N-dimethylamino)methyl-1-benzoxepin Methobromide and Lower Ring Homologs; II-5. l-Benzoxepins; II-6. 2-Benzoxepins; II-7. 3-Benzoxepins; E. REFERENCES; III. Oxepin Ring Systems Containing Three Rings; A. FUSED RING SYSTEMS; 1. Cyclopenta[5.6]pyrano[4,3-b]oxepins; 2. 8H-1,3-Dioxolo[4,5-h][3]benzoxepins; 3. Dibenz[b,d]oxepins; 4. Dibenz[b,e]oxepins; 5. Dibenz[b,f]oxepins; 6. Dibenz[c,e]oxepins |
a. Dibenz[c,e]oxepin-5,7-diones (Diphenic Anhydrides) |
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Sommario/riassunto |
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Chemistry of Heterocyclic Compounds publishes articles, letters to the Editor, reviews, and minireviews on the synthesis, structure, reactivity, and biological activity of heterocyclic compounds including natural products. The journal covers investigations in heterocyclic chemistry taking place in scientific centers of all over the world, including extensively the scientific institutions in Russia, Ukraine, Latvia, Lithuania and Belarus. |
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2. |
Record Nr. |
UNISA996215538503316 |
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Autore |
Joglekar Anand M |
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Titolo |
Industrial statistics [[electronic resource] ] : practical methods and guidance for improved performance / / Anand M. Joglekar |
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Pubbl/distr/stampa |
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ISBN |
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1-282-68662-3 |
9786612686627 |
0-470-58414-9 |
0-470-58412-2 |
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Descrizione fisica |
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1 online resource (283 p.) |
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Disciplina |
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Soggetti |
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Process control - Statistical methods |
Quality control - Statistical methods |
Experimental design |
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Lingua di pubblicazione |
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Formato |
Materiale a stampa |
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Livello bibliografico |
Monografia |
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Note generali |
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Description based upon print version of record. |
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Nota di bibliografia |
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Includes bibliographical references and index. |
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Nota di contenuto |
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INDUSTRIAL STATISTICS; CONTENTS; PREFACE; 1. BASIC STATISTICS: HOW TO REDUCE FINANCIAL RISK?; 1.1. Capital Market Returns; 1.2. Sample Statistics; 1.3. Population Parameters; 1.4. Confidence Intervals and Sample Sizes; 1.5. Correlation; 1.6. Portfolio Optimization; 1.7. Questions to Ask; 2. WHY NOT TO DO THE USUAL t-TEST AND WHAT TO REPLACE IT WITH?; 2.1. What is a t-Test and what is Wrong with It?; 2.2. Confidence Interval is Better Than a t-Test; 2.3. How Much Data to Collect?; 2.4. Reducing Sample Size; 2.5. Paired Comparison; 2.6. Comparing Two Standard Deviations |
2.7. Recommended Design and Analysis Procedure 2.8. Questions to Ask; 3. DESIGN OF EXPERIMENTS: IS IT NOT GOING TO COST TOO MUCH AND TAKE TOO LONG?; 3.1. Why Design Experiments?; 3.2. Factorial Designs; 3.3. Success Factors; 3.4. Fractional Factorial Designs; 3.5. Plackett-Burman Designs; 3.6. Applications; 3.7. Optimization Designs; 3.8. Questions to Ask; 4. WHAT IS THE KEY TO DESIGNING ROBUST PRODUCTS AND PROCESSES?; 4.1. The Key to Robustness; 4.2. Robust Design Method; 4.3. Signal-to-Noise Ratios; 4.4. Achieving Additivity; 4.5. Alternate Analysis Procedure; 4.6. Implications for R&D |
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4.7. Questions to Ask 5. SETTING SPECIFICATIONS: ARBITRARY OR IS THERE A METHOD TO IT?; 5.1. Understanding Specifications; 5.2. Empirical Approach; 5.3. Functional Approach; 5.4. Minimum Life Cycle Cost Approach; 5.5. Questions to Ask; 6. HOW TO DESIGN PRACTICAL ACCEPTANCE SAMPLING PLANS AND PROCESS VALIDATION STUDIES?; 6.1. Single-Sample Attribute Plans; 6.2. Selecting AQL and RQL; 6.3. Other Acceptance Sampling Plans; 6.4. Designing Validation Studies; 6.5. Questions to Ask; 7. MANAGING AND IMPROVING PROCESSES: HOW TO USE AN AT-A-GLANCE-DISPLAY?; 7.1. Statistical Logic of Control Limits |
7.2. Selecting Subgroup Size 7.3. Selecting Sampling Interval; 7.4. Out-of-Control Rules; 7.5. Process Capability and Performance Indices; 7.6. At-A-Glance-Display; 7.7. Questions to Ask; 8. HOW TO FIND CAUSES OF VARIATION BY JUST LOOKING SYSTEMATICALLY?; 8.1. Manufacturing Application; 8.2. Variance Components Analysis; 8.3. Planning for Quality Improvement; 8.4. Structured Studies; 8.5. Questions to Ask; 9. IS MY MEASUREMENT SYSTEM ACCEPTABLE AND HOW TO DESIGN, VALIDATE, AND IMPROVE IT?; 9.1. Acceptance Criteria; 9.2. Designing Cost-Effective Sampling Schemes |
9.3. Designing a Robust Measurement System 9.4. Measurement System Validation; 9.5. Repeatability and Reproducibility (R&R) Study; 9.6. Questions to Ask; 10. HOW TO USE THEORY EFFECTIVELY?; 10.1. Empirical Models; 10.2. Mechanistic Models; 10.3. Mechanistic Model for Coat Weight CV; 10.4. Questions to Ask; 11. QUESTIONS AND ANSWERS; 11.1. Questions; 11.2. Answers; APPENDIX: TABLES; REFERENCES; INDEX |
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Sommario/riassunto |
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HELPS YOU FULLY LEVERAGE STATISTICAL METHODS TO IMPROVE INDUSTRIAL PERFORMANCE Industrial Statistics guides you through ten practical statistical methods that have broad applications in many different industries for enhancing research, product design, process design, validation, manufacturing, and continuous improvement. As you progress through the book, you'll discover some valuable methods that are currently underutilized in industry as well as other methods that are often not used correctly. With twenty-five years of teaching and consulting experience, author Anand Jogleka |
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