1.

Record Nr.

UNIPARTHENOPE000003369

Autore

Vilar, Pierre

Titolo

Oro e moneta nella storia : 1450-1920 / Pierre Vilar

Pubbl/distr/stampa

Bari : Laterza, 1971

Descrizione fisica

496 p. : ill. ; 21 cm

Collana

Collezione storica

Disciplina

332.49

Lingua di pubblicazione

Italiano

Formato

Materiale a stampa

Livello bibliografico

Monografia

2.

Record Nr.

UNISA996390608603316

Autore

Wright Thomas, M.A., of St. Peters Colledge in Cambridge

Titolo

The glory of God's revenge against the bloody and detestable sins of murther and adultery [[electronic resource] ] : express'd in thirty modern tragical histories. To which are annexed, The triumphs of friendship and chastity, in some illustrious examples. By Thomas Wright, M.A. of St. Peters Colledge in Cambridge

Pubbl/distr/stampa

London, : printed by Tho. Moore, for Benjamin Crayle at the Lamb in Fleet-street, MDCLXXXV[1685]

Descrizione fisica

[12], 240, 247-338, [2] p., [1] leaf of plates

Soggetti

Adultery

Murder

Lingua di pubblicazione

Inglese

Formato

Materiale a stampa

Livello bibliografico

Monografia

Note generali

With an additional, engraved title page.

With a final advertisment leaf.

Text and register are continuous despite pagination.

"The glory of God's revenge against the licentious and detestable sin of adultery. .. Book II." has a separate title page on p.155; "The triumphs



of friendship and chastity." has a separate title page on p. 275; pagination and register are continuous.

Copy tightly bound.

Reproduction of the original in the Harvard University Library.

Sommario/riassunto

eebo-0062

3.

Record Nr.

UNINA9910143567103321

Autore

Snyder Lloyd R

Titolo

High-performance gradient elution : the practical application of the linear-solvent-strength model / / Lloyd R. Snyder, John W. Dolan

Pubbl/distr/stampa

Hoboken, NJ, : John Wiley, c2007

ISBN

1-280-72143-X

9786610721436

0-470-05552-9

0-470-05551-0

Descrizione fisica

1 online resource (491 p.)

Altri autori (Persone)

DolanJohn W

Disciplina

543/.84

Soggetti

High performance liquid chromatography

Lingua di pubblicazione

Inglese

Formato

Materiale a stampa

Livello bibliografico

Monografia

Note generali

Description based upon print version of record.

Nota di bibliografia

Includes bibliographical references and index.

Nota di contenuto

HIGH-PERFORMANCE GRADIENT ELUTION; CONTENTS; PREFACE; GLOSSARY OF SYMBOLS AND TERMS; 1 INTRODUCTION; 1.1 The "General Elution Problem" and the Need for Gradient Elution; 1.2 Other Reasons for the Use of Gradient Elution; 1.3 Gradient Shape; 1.4 Similarity of Isocratic and Gradient Elution; 1.4.1 Gradient and Isocratic Elution Compared; 1.4.2 The Linear-Solvent-Strength Model; 1.5 Computer Simulation; 1.6 Sample Classification; 1.6.1 Sample Compounds of Related Structure ("Regular Samples"); 1.6.2 Sample Compounds of Unrelated Structure ("Irregular" Samples); 2 GRADIENT ELUTION FUNDAMENTALS

2.1 Isocratic Separation2.1.1 Retention; 2.1.2 Peak Width and Plate Number; 2.1.3 Resolution; 2.1.4 Role of Separation Conditions; 2.1.4.1 Optimizing Retention [Term a of Equation (2.7)]; 2.1.4.2 Optimizing



Selectivity α [Term b of Equation (2.7)]; 2.1.4.3 Optimizing the Column Plate Number N [Term c of Equation (2.7)]; 2.2 Gradient Separation; 2.2.1 Retention; 2.2.1.1 Gradient and Isocratic Separation Compared for "Corresponding" Conditions; 2.2.2 Peak Width; 2.2.3 Resolution; 2.2.3.1 Resolution as a Function of Values of S for Two Adjacent Peaks ("Irregular" Samples)

2.2.3.2 Using Gradient Elution to Predict Isocratic Separation2.2.4 Sample Complexity and Peak Capacity; 2.3 Effect of Gradient Conditions on Separation; 2.3.1 Gradient Steepness b: Change in Gradient Time; 2.3.2 Gradient Steepness b: Change in Column Length or Diameter; 2.3.3 Gradient Steepness b: Change in Flow Rate; 2.3.4 Gradient Range Δø: Change in Initial Percentage B (ø(0)); 2.3.5 Gradient Range Δø: Change in Final %B (ø(f)); 2.3.6 Effect of a Gradient Delay; 2.3.6.1 Equipment Dwell Volume; 2.3.7 Effect of Gradient Shape (Nonlinear Gradients)

2.3.8 Overview of the Effect of Gradient Conditions on the Chromatogram2.4 Related Topics; 2.4.1 Nonideal Retention in Gradient Elution; 2.4.2 Gradient Elution Misconceptions; 3 METHOD DEVELOPMENT; 3.1 A Systematic Approach to Method Development; 3.1.1 Separation Goals (Step 1 of Fig. 3.1); 3.1.2 Nature of the Sample (Step 2 of Fig. 3.1); 3.1.3 Initial Experimental Conditions; 3.1.4 Repeatable Results; 3.1.5 Computer Simulation: Yes or No?; 3.1.6 Sample Preparation (Pretreatment); 3.2 Initial Experiments; 3.2.1 Interpreting the Initial Chromatogram (Step 3 of Fig. 3.1)

3.2.1.1 "Trimming" a Gradient Chromatogram3.2.1.2 Possible Problems; 3.3 Developing a Gradient Separation: Resolution versus Conditions; 3.3.1 Optimizing Gradient Retention k* (Step 4 of Fig. 3.1); 3.3.2 Optimizing Gradient Selectivity α* (Step 5 of Fig. 3.1); 3.3.3 Optimizing the Gradient Range (Step 6 of Fig. 3.1); 3.3.3.1 Changes in Selectivity as a Result of Change in k*; 3.3.4 Segmented (Nonlinear) Gradients (Step 6 of Fig. 3.1 Continued); 3.3.5 Optimizing the Column Plate Number N* (Step 7 of Fig. 3.1); 3.3.6 Column Equilibration Between Successive Sample Injections

3.3.7 Fast Separations

Sommario/riassunto

Gradient elution demystifiedOf the various ways in which chromatography is applied today, few have been as misunderstood as the technique of gradient elution, which presents many challenges compared to isocratic separation. When properly explained, however, gradient elution can be less difficult to understand and much easier to use than often assumed.Written by two well-known authorities in liquid chromatography, High-Performance Gradient Elution: The Practical Application of the Linear-Solvent-Strength Model takes the mystery out of the practice of gradient elution and helps r