1.

Record Nr.

UNINA9911020017003321

Titolo

High-throughput screening in heterogeneous [i.e. chemical] catalysis / / edited by Alfred Hagemeyer, Peter Strasser, Anthony F. Volpe, Jr

Pubbl/distr/stampa

Weinheim ; ; [Great Britain], : Wiley-VCH, c2004

ISBN

9781280519659

1280519657

9783527604104

3527604103

Descrizione fisica

1 online resource (341 p.)

Altri autori (Persone)

HagemeyerAlfred

StrasserPeter

VolpeAnthony F

Disciplina

541.395

Soggetti

Heterogeneous catalysis

Catalysis

Lingua di pubblicazione

Inglese

Formato

Materiale a stampa

Livello bibliografico

Monografia

Note generali

Description based upon print version of record.

Nota di bibliografia

Includes bibliographical references and index.

Nota di contenuto

High-Throughput Screening in Heterogeneous Catalysis; Foreword; Preface; Contents; List of Contributors; 1 Impact of High-Throughput Screening Technologies on Chemical Catalysis; 1.1 Introduction; 1.2 Application of HT-R&D Methods in Heterogeneous Catalysis; 1.3 Application of HT-R&D Methods in Homogeneous Catalysis; 1.4 Conclusions; 1.5 References; 2 Mastering the Challenges of Catalyst Screening in High-Throughput Experimentation for Heterogeneously Catalyzed Gas-phase Reactions; 2.1 Challenges Connected to Catalyst Screening in Gas-phase Catalysis; 2.2 Preparative Aspects

2.3 Analytical Aspects2.3.1 Stage I Screening; 2.3.2 Stage II Screening; 2.3.3 King-System: Saving Analysis Time via Intelligent Use of Analysis Techniques; 2.4 Case Studies of Selected Examples in Gas-phase Catalysis in Stage II Screening; 2.4.1 Bulk Chemicals and Intermediates: Partial Oxidation; 2.4.2 Refinery Catalysis: High-pressure Reactions; 2.4.3 Environmental Catalysis: DeNOx Catalysis; 2.5 The Challenge of Ultrahigh-Throughput Screening; 2.5.1 Catalyst Synthesis: the Split & Pool Principle; 2.5.2 Catalyst Testing: Integrated Reactor Formats as



Critical Key Components

2.6 Summary and Outlook2.7 References; 3 High-Throughput Workflow Development: Strategies and Examples in Heterogeneous Catalysis; 3.1 Introduction; 3.2 High-Throughput Methods; 3.2.1 DOE - Designing Experiments Based on Statistics; 3.2.2 Constrained Optimization - Independent Variables; 3.2.3 Constrained Optimization - Dependent Variables; 3.2.4 Methods to Include Synthesis Hardware Constraints; 3.2.5 Process Simulation for Hardware Bottleneck Identification; 3.3 Workflow Components; 3.3.1 Primary Synthesis; 3.3.2 Primary Synthesis: Wafer-based Sol-gel and Evaporative Synthesis

3.3.3 Primary Synthesis: Wafer-based Impregnation Synthesis3.3.4 Primary Screening: Scanning Mass Spectrometer; 3.3.5 Primary Screening: Massively Parallel Microfluidic Reactor; 3.3.6 Secondary Synthesis: Bulk Impregnation; 3.3.7 Secondary Synthesis: Bulk Evaporation/Precipitation; 3.3.8 Secondary Synthesis: Hydrothermal; 3.3.9 Secondary Screening: 48-Channel Fixed-bed Reactor; 3.3.10 High-Throughput Catalyst Characterization; 3.3.11 Tertiary Screening; 3.4 Example: Ethane to Ethylene; 3.5 Example: Ethane to Acetic Acid; 3.6 Example: Propane to Acrylonitrile; 3.7 Summary; 3.8 References

4 Integrated Microreactor Set-ups for High-Throughput Screening and Methods for the Evaluation of "Low-density" Screening Data4.1 Introduction; 4.1.1 Pellet-type and Ceramic Reactors; 4.1.2 Multiple Microchannel Array Reactors; 4.1.3 Chip-type Reactors; 4.1.4 Well-type Reactors; 4.2 Steady-state Reactor Set-ups; 4.2.1 Methanol Steam Reforming; 4.2.2 Propane Steam Reforming; 4.2.3 Catalytic Methane Combustion and Methods for Sample Preparation; 4.2.3.1 Wet Chemical Procedure (Washcoating/Flow Impregnation); 4.2.3.2 Experimental and Discussion; 4.3 Transient-state Reactor Set-ups

4.3.1 Introduction

Sommario/riassunto

Alfred Hagemeyer received his diploma degrees in chemistry, 1985, and physics, 1987, from the university of Dortmund, Germany, did his Ph.D. at the Max-Planck-Institute fuer Polymerforschung in Mainz, Germany, 1987-1989, was postdoc at the university of Bologna, Italy, 1990, was employed at BASF, corporate research, ammonia laboratory, Ludwigshafen, Germany, 1991-1996, and at Hoechst/Aventis, corporate research, department of heterogeneous catalysis, Frankfurt, Germany, 1996-1998, and joined Symyx Technologies, heterogeneous catalysis group, Santa Clara, CA, in 1998 where he is a Distinguished



2.

Record Nr.

UNINA9910253977603321

Autore

Ding Tao

Titolo

Power System Operation with Large Scale Stochastic Wind Power Integration : Interval Arithmetic Based Analysis and Optimization Methods / / by Tao Ding

Pubbl/distr/stampa

Singapore : , : Springer Singapore : , : Imprint : Springer, , 2017

ISBN

981-10-2561-4

Edizione

[1st ed. 2017.]

Descrizione fisica

1 online resource (XVII, 217 p. 70 illus., 64 illus. in color.)

Collana

Springer Theses, Recognizing Outstanding Ph.D. Research, , 2190-5053

Disciplina

621.312136

Soggetti

Renewable energy resources

Energy systems

Mathematical optimization

Energy policy

Renewable and Green Energy

Energy Systems

Optimization

Energy Policy, Economics and Management

Lingua di pubblicazione

Inglese

Formato

Materiale a stampa

Livello bibliografico

Monografia

Note generali

"Doctoral Thesis accepted by Tsinghua University, Beijing, China."

Nota di bibliografia

Includes bibliographical references at the end of each chapters.

Nota di contenuto

Introduction -- Mathematics for Interval Algebra and Optimization -- The Research and Application of Interval Power Flow -- Interval Economic Dispatch and The Tackling of Infeasible Model -- Robust Interval Economic Dispatch and The Price of Robustness -- Acceleration Strategies for Large-scale Economic Dispatch Models -- Conclusions and Prospects.

Sommario/riassunto

This book addresses the uncertainties of wind power modeled as interval numbers and assesses the physical modeling and methods for interval power flow, interval economic dispatch and interval robust economic dispatch. In particular, the optimization models are set up to address these topics and the state-of-the-art methods are employed to efficiently solve the proposed models. Several standard IEEE test systems as well as real-world large-scale Polish power systems have been tested to verify the effectiveness of the proposed models and



methods. These methods can be further applied to other research fields that are involved with uncertainty.