Preparation of thin film Pd membranes for H2 separation from synthesis gas and detailed design of a permeability testing unit / / M. Bientinesi and L. Petarca

• Record Nr.: UNINA9910967943103321
• Autore: Bientinesi M (Miguel), <1950->
• Pubbl/distr/stampa: New York, : Nova Science Publishers, c2010
• ISBN: 1-61122-688-0
• Edizione: [1st ed.]
• Descrizione fisica: 1 online resource (94 p.)
• Collana: Chemical engineering methods and technology
• Altri autori (Persone): PetarcaL <1945-> (Luca)
• Disciplina: 665.8/1
• Soggetti: Hydrogen - Separation; Palladium; Membranes (Technology); Gasoline, Synthetic
• Lingua di pubblicazione: Inglese
• Formato: Materiale a stampa
• Livello bibliografico: Monografia
• Note generali: Description based upon print version of record.
• Nota di bibliografia: Includes bibliographical references (p. [71]-74) and index.
• Nota di contenuto: Intro -- PREPARATION OF THIN FILM PD MEMBRANES FOR H2 SEPARATION FROM SYNTHESIS GAS AND DETAILED DESIGN OF A PERMEABILITY TESTING UNIT -- PREPARATION OF THIN FILM PD MEMBRANES FOR H2 SEPARATION FROM SYNTHESIS GAS AND DETAILED DESIGN OF A PERMEABILITY TESTING UNIT -- CONTENTS -- PREFACE -- Chapter 1 INTRODUCTION -- 1.1. HYDROGEN AS AN ENERGY CARRIER -- 1.2. CURRENT PRODUCTION METHODS AND USES -- 1.3. SYNGAS FOR HYDROGEN PRODUCTION -- 1.4. SEPARATION OF HYDROGEN FROM SYNTHESIS GAS -- 1.4.1. Pressure Swing Adsorption -- 1.4.2. Membrane Separation -- 1.5. FUNDAMENTALS OF HYDROGEN MEMBRANE SEPARATION TECHNOLOGY -- 1.5.1. Dense Polymeric Membranes -- 1.5.2. Dense Metallic Membranes -- 1.5.3. Microporous Ceramic Membranes -- 1.5.4. Dense Ceramic Membranes -- 1.5.5. Composite Membranes -- Chapter 2 PALLADIUM MEMBRANES -- 2.1. PURE PALLADIUM AND PALLADIUM ALLOYS MEMBRANES -- 2.2. POROUS SUPPORTS -- 2.3. PALLADIUM FILM DEPOSITION TECHNIQUES -- 2.3.1. Chemical Vapor Deposition -- 2.3.2. Spray Pyrolysis -- 2.3.3. Sputter Deposition -- 2.3.4. Electroplating -- 2.3.5. Electroless Plating -- 2.3.6. Pd-Alloy Deposition via ELP -- 2.4. PALLADIUM MEMBRANES CHARACTERIZATION -- Chapter 3 EXPERIMENTAL -- 3.1. METALLIC ; POROUS SUPPORTS -- 3.2. SUPPORTS ABRASION AND CLEANING -- 3.3. SURFACE OXIDATION -- 3.4. SENSITIZATION AND ACTIVATION -- 3.5. ELECTROLESS PLATING -- 3.5.1. Bath Composition -- 3.5.2. Disc ELP Equipment -- 3.5.3. Tube ELP Equipment -- 3.5.4. Vacuum Electroless Plating -- 3.6. MORPHOLOGY CHARACTERIZAION -- 3.7. NITROGEN LOW PRESSURE PERMEATION TEST -- Chapter 4 RESULT AND DISCUSSION -- 4.1. POROUS SUPPORTS -- 4.2. SUPPORT ABRASION AND ETCHING -- 4.2. SURFACE OXIDATION -- 4.3. PALLADIUM DEPOSITION -- 4.4. TUBULAR MEMBRANES NITROGEN PERMEABILITY -- Chapter 5 PERMEABILITY TEST EXPERIMENTAL SET-UP -- 5.1. INTRODUCTION.; 5.2. EXPERIMENTAL SET-UP -- 5.3. SELECTED EQUIPMENT -- 5.4. PERMEATION CELLS AND OTHER EQUIPMENT -- Chapter 6 CONCLUSION -- ACKNOWLEDGEMENTS -- REFERENCES -- INDEX -- Blank Page.
• Sommario/riassunto: In this text, palladium films were deposited above stainless steel porous supports using the electroless plating (ELP) technique. Two different geometry (disc sheet and tubes) were used. Finally, in this book, the detailed design of a permeability testing unit is reported.