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1. |
Record Nr. |
UNISA996204172303316 |
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Autore |
Gerhards Petra |
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Titolo |
GC/MS in der klinischen Chemie [[electronic resource] /] / Petra Gerhards ... [et al.] |
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Pubbl/distr/stampa |
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Weinheim, Germany, : VCH, 1997 |
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ISBN |
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1-282-02150-8 |
9786612021503 |
3-527-62434-1 |
3-527-62435-X |
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Descrizione fisica |
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1 online resource (242 p.) |
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Disciplina |
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Soggetti |
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Gas chromatography |
Mass spectrometry |
Chemistry, Analytic |
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Lingua di pubblicazione |
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Formato |
Materiale a stampa |
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Livello bibliografico |
Monografia |
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Note generali |
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Description based upon print version of record. |
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Nota di bibliografia |
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Includes bibliographical references and index. |
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Nota di contenuto |
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GC/MS in der klinischen Chemie; Inhalt; Teil I Analytische Grundlagen der Gaschromatographie und der Massenspektrometrie; 1 Physikalische Grundlagen und Aufbau; 1.1 Adsorption; 1.2 Verteilung; 1.3 Aufbau eines gaschromatographischen Systems; 2 Injektion und Headspace-Technik; 2.1 Injektion; 2.1.1 Splitlose Injektion; 2.1.2 Split-Injektion; 2.1.3 Temperaturprogrammierte Injektion; 2.1.4 On-Column-Injektion; 2.2 Headspace-Technik; 2.2.1 Statische Headspace; 2.2.2 Dynamische Headspace; 3 Säulen und Trägergas; 3.1 Gepackte Säulen; 3.2 Kapillarsäulen; 3.3 Stationäre Phasen; 3.4 Filmdicke |
3.5 Trägergas4 GC-Detektoren und Massenspektrometrie; 4.1 Selektivität; 4.2 Flammenionisationsdetektor (FID); 4.3 Electron Capture Detector (ECD); 4.4 Massenspektrometrie; 4.4.1 Aufbau und Funktionsweise eines Quadrupol-Massenspektrometers; 4.4.2 Detektion; 4.4.3 Probenaufgabe - GC/MS-Interface; 4.4.4 Der Totalionenstrom (TIC); 4.4.5 Selected Ion Monitoring (SIM); 4.4.6 Auswertung; 5 Quantifizierung; 5.1 Interne Standardmethode; 5.2 Standardaddition; 5.3 Externe Eichung; 5.4 Quantifizierung im |
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Splitmodus; 5.5 Nachweisgrenzen; Literatur zu Teil I; Teil II Drogenscreening |
6 Epidemiologie des Drogen- und Arzneimittelmißbrauchs6.1 Einleitung; 6.2 Spezifische Daten und Trends; 6.2.1 Opioide/Opiate; 6.2.1.1 Heroin; 6.2.1.2 Codein; 6.2.1.3 Dihydrocodein (DHC); 6.2.1.4 Methadon; 6.2.1.5 Tramadol; 6.2.1.6 Tilidin; 6.2.1.7 Andere zentral wirksame Analgetika; 6.2.2 Periphere Analgetika; 6.2.3 Benzodiazepine; 6.2.3.1 Diazepam; 6.2.3.2 Flunitrazepam; 6.2.3.3 Bromazepam; 6.2.4 Barbiturate; 6.2.5 Andere Schlaf- und Suchtmittel; 6.2.5.1 Clomethiazol; 6.2.5.2 Antihistaminika; 6.2.6 Amphetamine und verwandte Substanzen; 6.2.6.1 Substanzen der Drogenszene |
6.2.6.2 Psychoanaleptika und Antihypotonika6.2.6.3 Anorektika; 6.2.7 Designer-Drogen; 6.2.8 Cannabis; 6.2.9 Cocain; 6.2.10 Weitere Halluzinogene; 6.2.10.1 Lysergsäurediethylamid (LSD); 6.2.10.2 Andere Indol-Derivate; 6.2.10.3 Mescalin; 6.2.10.4 Muskatnuß; 6.2.10.5 Piperidin-Derivate; 6.2.10.6 Fliegenpilz; 6.2.10.7 Biperiden; 6.2.11 Schnüffelstoffe; 7 Probenvorbereitungsverfahren für die Drogenanalytik; 7.1 Historie der Probenvorbereitung; 7.2 Prinzip der Festphasenextraktion; 7.2.1 Praktischer Teil; 7.2.1.1 Probenvorbereitung für die Matrix Urin |
7.2.1.2 Probenvorbereitung für die Matrix Vollblut7.3 Flüssig-Flüssig-Extraktion (FFE); 7.4 Vergleich zwischen FPE und FFE; 8 Drogenscreening aus Urin mit GC/MS; 8.1 Allgemeines zum Drogenscreening am Urin; 8.1.1 Abgrenzung des Drogenscreenings zu anderen Screening-Verfahren; 8.1.2 Probenmaterial; 8.1.3 Manipulationsmöglichkeiten; 8.1.4 Immunologische Analyseverfahren; 8.1.4.1 Immunologische Tests auf Einzelsubstanzen und Stoffgruppen; 8.1.4.2 Gängige immunologische Testprinzipien (Auswahl); 8.1.5 Chromatographische Verfahren; 8.1.5.1 Gaschromatographie mit massenspektrometrischer Detektion |
8.1.5.2 Hochleistungsflüssigkeitschromatographie mit Diodenarraydetektion (HPLC/DAD) |
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Sommario/riassunto |
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Die GC/MS erfüllt die gesetzlichen Forderungen nach immer empfindlicheren und aussagekräftigeren Verfahren in der klinischen Analytik. Speziell im Drogenscreening werden die Ergebnisse der immunologischen Verfahren mit Hilfe der GC/MS abgesichert. Anwender im klinischen Labor erhalten mit diesem Buch einen schnellen Einstieg in die GC/MS Analytik.Die Beschreibung aktueller Themen der klinischen Analytik in einfacher und praxisgerechter Form sowie die nötigen Begleitinformationen aus anderen Fachgebieten helfen, Zusammenhänge zu verstehen und in die Praxis umzusetzen. Anhand praxisgerec |
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2. |
Record Nr. |
UNINA9910782754003321 |
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Autore |
Solovyov Vladimir Sergeyevich <1853-1900.> |
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Titolo |
Freedom, faith, and dogma [[electronic resource] ] : essays by V.S. Soloviev on Christianity and Judaism / / edited, translated, and with an introduction by Vladimir Wozniuk |
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Pubbl/distr/stampa |
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Albany, NY, : State University of New York Press, c2008 |
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ISBN |
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0-7914-7796-7 |
1-4356-9453-8 |
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Descrizione fisica |
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Altri autori (Persone) |
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Disciplina |
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Soggetti |
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Christianity and other religions - Relations - Judaism |
Judaism - Relations - Christianity |
Christianity |
Judaism |
Russia Religion 19th century |
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Lingua di pubblicazione |
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Formato |
Materiale a stampa |
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Livello bibliografico |
Monografia |
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Note generali |
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Bibliographic Level Mode of Issuance: Monograph |
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Nota di bibliografia |
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Includes bibliographical references (p. 233-240) and indexes. |
"Supplemental listing of Soloviev's relevant writings": p. 241. |
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Nota di contenuto |
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On spiritual authority in Russia -- On the ecclesiastical question concerning the old Catholics -- The Jews and the Christian question -- New Testament Israel -- The teaching of the Twelve Apostles -- The Talmud and the recent polemical literature concerning it in Austria and Germany -- On counterfeits -- On the decline of the medieval worldview -- When did the Hebrew prophets live? -- Byzantinism and Russia -- The secret of progress. |
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3. |
Record Nr. |
UNINA9910734821803321 |
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Autore |
Dudek Micha (Lawyer) |
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Titolo |
Courtroom Power Distance Dynamics / / by Michał Dudek, Mateusz Stępień |
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Pubbl/distr/stampa |
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Cham : , : Springer International Publishing : , : Imprint : Springer, , 2021 |
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ISBN |
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Edizione |
[1st ed. 2021.] |
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Descrizione fisica |
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1 online resource (xii, 295 pages) : illustrations |
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Collana |
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Law and Visual Jurisprudence, , 2662-4540 ; ; 3 |
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Disciplina |
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Soggetti |
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Law - Philosophy |
Law - History |
Theories of Law, Philosophy of Law, Legal History |
Philosophy of Law |
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Lingua di pubblicazione |
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Formato |
Materiale a stampa |
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Livello bibliografico |
Monografia |
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Nota di bibliografia |
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Includes bibliographical references. |
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Nota di contenuto |
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1 Introduction -- 2 Courts, Courtrooms and Power Distance -- 3 Judge-Witness Courtroom Power Distance Dynamics -- 4 Subjective Power Distance and Opinions on Judges -- 5 Conclusion. |
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Sommario/riassunto |
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The book presents a comprehensive reconceptualization of Geert Hofstede’s well-known concept of power distance, applying the theory to the specific case of judge–witness courtroom interactions in Polish regional courts. In the light of the detailed critique of Hofstede’s original approach to power distance, the book first carefully develops a three-level concept of power distance, including personal preferences concerning the realization of power relations (subjective level); rules, practices and spatio-architectural arrangements underlying power relations (organizational level); and individual demeanors that can, in practice, increase or decrease the asymmetry between parties to a power relation (interactional level). This reconceptualization provides a universal conceptual apparatus that is applicable to various social settings, but the authors have used it in extensive qualitative and quantitative research focused on courtroom interactions. After laying thetheoretical foundations, the book details the elements of judge–witness courtroom interactions (both verbal and non-verbal) that contribute to establishing power distance between judge and witness. |
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These were identified over 6 months of observational research conducted in 2018 in the Kraków regional courts. Lastly, the book addresses the issue of the relationship between the subjective level of power distance and opinions that laypeople can have concerning a judge’s demeanor in the courtroom environment. To do so, it describes specific quantitative research that involved the creation of original film clips depicting witness questioning by the judge in a courtroom in three power distance situations. Offering a coherent framework for examining various interpersonal relations in legal contexts and illustrating how the framework can be applied on the courtroom interactions example, the book will appeal to a wide range of legal practitioners and academics. It also allows scientists outside the legal field to gain a new and broad understanding of power distance that they can easily apply in their respective fields. Furthermore, it provides non-academics with insights into courtroom interactional dynamics, as exemplified by the discussion of Polish judicial practice. |
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