Record Nr.

UNINA9910480150003321

Autore

Haines P.J

Titolo

Thermal Methods of Analysis [[electronic resource] ] : Principles, Applications and Problems / / by P.J. Haines

Pubbl/distr/stampa


Dordrecht : , : Springer Netherlands : , : Imprint : Springer, , 1995

ISBN

94-011-1324-6

Edizione

[1st ed. 1995.]

Descrizione fisica

1 online resource (XII, 286 p.)

Disciplina

543

Soggetti

Analytical chemistry

Chemistry

Analytical Chemistry

Chemistry/Food Science, general

Lingua di pubblicazione

Inglese

Formato

Materiale a stampa

Livello bibliografico

Monografia

Note generali

Bibliographic Level Mode of Issuance: Monograph

Nota di contenuto

1 Introduction to thermal methods -- 1.1 Introduction -- 1.2 Historical development -- 1.3 Definitions -- 1.4 Computers and thermal methods -- 1.5 Factors affecting thermal analysis results -- 1.6 Simultaneous and complementary techniques -- 1.7 Problems -- References -- General Bibliography -- 2 Thermogravimetry -- 2.1 Introduction -- 2.2 Historical -- 2.3 Definition of thermogravimetry -- 2.4 Apparatus -- 2.5 Kinetics of reactions -- 2.6 Applications of thermogravimetry -- 2.7 Controlled rate thermogravimetry and Hi-Res• TGA -- 2.8 Problems -- References -- 3 Differential thermal analysis and differential scanning calorimetry -- 3.1 Introduction -- 3.2 Historical -- 3.3 Definitions -- 3.4 Apparatus -- 3.5 Theory of DTA and DSC -- 3.6 Heat flux DSC -- 3.7 Power-compensated DSC -- 3.8 Calibration -- 3.9 Applications -- 3.11 Problems -- References -- 4 Thermomechanical, dynamic mechanical and associated methods -- 4.1 Introduction -- 4.2 Definitions -- 4.3 Thermomechanical analysis -- 4.4 Dynamic mechanical analysis -- 4.5 Dielectric thermal analysis -- 4.6 Thermally stimulated current analysis and relaxation map analysis -- 4.7 Problems -- References -- 5 Simultaneous techniques and product analysis -- 5.1 Introduction -- 5.2 Simultaneous thermal analysis -- 5.3 Evolved gas analysis -- 5.4 Detection and identification of evolved gases -- 5.5 Infrared and simultaneous TA-infrared -- 5.6

Infrared product analysis -- 5.7 Thermomicroscopy -- 5.8 X-ray methods -- 5.9 Electron microscopy and associated techniques -- 5.10 Conclusion -- 5.11 Less common thermal analysis techniques -- 5.12 Problems -- References -- 6 Problem solving and applications of thermal methods -- List of examples -- Problems/Solutions -- 6.1 Inorganic materials -- 6.2 Polymeric materials -- 6.3 Fine chemicals and pharmaceuticals -- 6.4 Other materials -- References -- Appendix: Solutions to problems in Chapters 1-5.

Sommario/riassunto

The wide range of applications of thermal methods of analysis in measuring physical properties, studying chemical reactions and determining the thermal behaviour of samples is of interest to academics and to industry. These applications prompted the writing of this book, in the hope that the descriptions, explanations and examples given would be of help to the analyst and would stimulate the investigation of other thermal techniques. Thermal studies are a fascinating means of examining the samples and the problems brought to us by colleagues, students and clients. If time allows, watching crystals change on a hot-stage microscope, or measuring the properties and changes on a DSC or TG or any thermal instrument can be a rewarding activity, besides providing valuable analytical information. This book started from a series of lectures delivered at Kingston University and at meetings of the Thermal Methods Group of the United Kingdom. The collaboration and information supplied to all the contribu tors by colleagues and instrument manufacturers is most gratefully ack nowledged, as are the valuable contributions made at meetings of the International Confederation for Thermal Analysis and Calorimetry (ICT AC) and at the European Symposia on Thermal Analysis and Calorimetry (ESTAC).

Record Nr.

UNISA996397566903316

Autore

Millington Edward <d. 1703.>

Titolo

A collection of curious pictures, viz. paintings and limnings, by the best masters. Will be sold by auction on Monday the 15th, and Tuesday the 16th of this instant September 1690. at the Barbadoes Coffe-House in Exchange-Alley. over against the Royal-Exchange, in Cornhil [[electronic resource] ] : The sale beginning precisely at four of the clock each afternoon. By Edward Millington. Catalogues of which are distributed by Mr. Gilliflower in Westminster-Hall: Mr. Nott in the Pall Mall: Mr. Bently in Russel-street, Covent-Garden: Mr. Wilkinson in Fleet-street: Mr. Hargrave, at the Kings Head, over against Furnivals-Inn in Holborn: Mr; [sic] Miller, at the Acorn, in St. Paul's Church yard: and Mr. Crouch over against the Royal-Exchange, in Cornhil, booksellers

Pubbl/distr/stampa


[London, : s.n., 1690]

Descrizione fisica

[2], 6 p

Soggetti

Art auctions - England - London

Art - England - Catalogs